Surface enhanced transmission Raman spectroscopy: Quantitative performances for impurity analysis in complex matrices

Horne, Julie; Beckers, Pierre; Sacre, Pierre-Yves; Francotte, Pierre; Caudron, Eric; Hubert, Philippe; Hubert, Cédric; De Bleye, Charlotte; Ziemons, Eric

doi:10.1016/j.jpba.2024.116469

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Surface enhanced transmission Raman spectroscopy: Quantitative performances for impurity analysis in complex matrices

Horne, Julie; Beckers, Pierre; Sacre, Pierre-Yves et al.

2024 • In Journal of Pharmaceutical and Biomedical Analysis

Peer Reviewed verified by ORBi

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https://hdl.handle.net/2268/321913

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10.1016/j.jpba.2024.116469

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Keywords :

Surface enhanced transmission Raman spectroscopy (SETRS); Analytical performances; Total error risk-based approach; complex matrix; impuriy; assay

Abstract :

[en] A transmission detection mode was investigated with SERS analyses (SETRS). A comparison between back- scattering and transmission detection modes was conducted to demonstrate the feasibility of performing SETRS analyses. The impact of various parameters on the SERS signal intensity such as sample volume, lens collection optic, laser beam size and laser power were then examined. The analytical performances of SETRS were further evaluated through the quantification of an impurity (4-aminophenol) ranging from 3 to 20 μg/mL in a com- mercial pharmaceutical product using a total error risk-based approach. To account for expected variability of routine analysis, 9 batches of silver nanoparticles suspensions were used and experiments were performed over 5 different days and by 2 operators. Univariate spectral analysis based on a quadratic regression was compared to a multivariate approach using a partial least square regression. The presented results demonstrated that SETRS can be used to determine an impurity in a complex matrix opening new perspectives for quantitative applications.

Research Center/Unit :

CIRM - Centre Interdisciplinaire de Recherche sur le Médicament - ULiège

Disciplines :

Pharmacy, pharmacology & toxicology

Author, co-author :

Horne, Julie ^✱; Université de Liège - ULiège > Unités de recherche interfacultaires > Centre Interdisciplinaire de Recherche sur le Médicament (CIRM)

Beckers, Pierre ^✱; Université de Liège - ULiège > Unités de recherche interfacultaires > Centre Interdisciplinaire de Recherche sur le Médicament (CIRM)

Sacre, Pierre-Yves ; Université de Liège - ULiège > Département de pharmacie > Chimie analytique

Francotte, Pierre ; Université de Liège - ULiège > Département de pharmacie > Chimie pharmaceutique

Caudron, Eric; University of Paris-Saclay [FR] > lipids > Analytical and biological systems

Hubert, Philippe ; Université de Liège - ULiège > Département de pharmacie > Chimie analytique

Hubert, Cédric ; Université de Liège - ULiège > Département de pharmacie > Chimie analytique

De Bleye, Charlotte ; Université de Liège - ULiège > Unités de recherche interfacultaires > Centre Interdisciplinaire de Recherche sur le Médicament (CIRM)

Ziemons, Eric ; Université de Liège - ULiège > Unités de recherche interfacultaires > Centre Interdisciplinaire de Recherche sur le Médicament (CIRM)

^✱ These authors have contributed equally to this work.

Language :

English

Title :

Surface enhanced transmission Raman spectroscopy: Quantitative performances for impurity analysis in complex matrices

Publication date :

11 September 2024

Journal title :

Journal of Pharmaceutical and Biomedical Analysis

ISSN :

0731-7085

eISSN :

1873-264X

Publisher :

Elsevier, Amsterdam, Netherlands

Peer reviewed :

Peer Reviewed verified by ORBi

Available on ORBi :

since 11 September 2024

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