[en] Modulated differential scanning calorimetry, wide angle x-ray scattering, and environmental scanning electron microscopy were used to investigate the physical and morphological properties of chicory root inulin spray dried under different conditions. When the feed temperature increased up to 80 degrees C, the average degree of polymerization of the solubilized fraction increased, leading to a higher glass transition temperature (Tg). Above 80 degrees C, the samples were completely amorphous, and the Tg did not change. The starting material was semicrystalline, and the melting region was composed of a dual endotherm; the first peak subsided as the feed temperature increased up to a temperature of 70 degrees C, whereas above 80 degrees C, no melting peak was observed as the samples were completely amorphous. To a lesser extent, the inlet air temperature of 230 degrees C allowed a higher amorphous content of the samples than at 120-170 degrees C but induced a blow-out of the particles.
Disciplines :
Agriculture & agronomy
Author, co-author :
Ronkart, S. N.
Deroanne, C.
Paquot, Michel ; Université de Liège - ULiège > Gembloux Agro-Bio Tech > Gembloux Agro-Bio Tech
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Bibliography
C. Blecker, C. Fougnies, J.C. Van Herck, J.P. Chevalier and M. Paquot, J Agric Food Chem 50, 1602-1607 (2002).
M.B. Roberfroid and N.M. Delzenne, Annu Rev Nutr 18, 117-143 (1998).
C. Blecker, J.P. Chevalier, J.C. Van Herck, C. Fougnies, C. Deroanne and M. Paquot, Recent Research Developments in Agricultural & Food Chemistry 5, 125-131 (2001).
D.E. Oakley, Chem Eng Prog 93, 48-54 (1997).
O.C. Chidavaenzi, G. Buckton, F. Koosha and R. Pathak, Int J Pharm 159, 67-74 (1997).
M. Sugimoto, T. Maejima, S. Narisawa, K. Matsubara and H. Yoshino, Int J Pharm 296, 64-72 (2005).
R. Surana, A. Pyne and R. Suryanarayanan, Pharm Res 21, 1167-1176 (2004).
R. Parker and S.G. Ring, J Cereal Sci 34, 1-17 (2001).
J.J. Fitzpatrick, K. Barry, P.S.M. Cerqueira, T. Iqbal, J. O'Neill and Y.H. Roos, Int Dairy J 17, 383-392 (2007).
S.N. Ronkart, M. Paquot, C. Fougnies, C. Deroanne, J.C. Van Herck and C. Blecker, Talanta 70, 1006-1010 (2006).
C. Blecker, J.P. Chevalier, C. Fougnies, J.C. Van Herck, C. Deroanne C. and M. Paquot, J Therm Anal Cal 71, 215-224 (2003).
S. Ronkart, C. Blecker, C. Fougnies, J.C. Van Herck, J. Wouters and M. Paquot, Carbohyd Polym 63, 210-217 (2006).
H. Xu, B. Seyhan Ince and P. Cebe, J Polym Sci Pol Phys 41, 3026-3036 (2003).
E.Y. Shalaev and G. Zografi, The concept of structure in amorphous solids from the perspective of the pharmaceutical sciences. In: Progress in Amorphous Food and Pharmaceutical Systems, edited by H. Levine (Royal Society of Chemistry, Cambridge, UK 2002), pp. 11-30.
E. Verdonck, K. Schaap, L.C. Thomas, Int J Pharm 192, 3-20 (1999).
M. Mathlouthi, A.L. Cholli, and J.L. Koenig, Carbohyd Res 147, 1-9 (1986).
J.F. Mano, J.L. Gómez Ribelles, N.M. Alves and M. Salmerón Sanchez, Polymer 46, 8258-8265 (2005).
Y. Roos and M. Karel, Biotechnol Prog 7, 49-53 (1991).
S.Y Hobbs and C.F. Pratt, Polymer 16, 462-465 (1975).
C. Fougnies, M. Dosière, M.H.J. Koch and J. Roovers, Macromolecules 31, 6266-6274 (1998).
E.M. Woo, Y.S. Sun and C.P. Yang, Prog Polym Sci 26, 945-983 (2001).
J. Plans, W.J. MacKnight and F.E. Karasz, Macromolecules 17, 810-814 (1984).
T Liu, Eur Polym J 39, 1311-1317 (2003).
P. Srimoaon, N. Dangseeyun and P. Supaphol, Eur. Polym. J. 40, 599-608 (2004).
C.L.M. Hébette, J.A. Delcour, M.H.J. Koch, K. Booten, R. Kleppinger, N. Mischenko and H. Reynaers, Carbohyd Res 310, 65-75 (1998).
Hébette C, Crystallisation, melting and gel formation of concentrated inulin-water systems. PhD thesis (K.U. Leuven, Belgium 2002).
R.H. Marchessault, T. Bleha, Y. Deslandes and J.F. Revol, Can J Chem 58, 2415-2422 (1980).
I. André, J.L. Putaux, H. Chanzy, F.R. Taravel, J.W. Timmermans and D. de Wit, Int J Biol Macromol 18, 195-204 (1996a).
I. André, K. Mazeau, I. Tvaroska, J.L. Putaux, W.T. Winter, F.R. Taravel and H. Chanzy, Macromolecules 29, 4626-4635 (1996b).
D.O. Corrigan, A.M. Healy and O.I. Corrigan, Int J Pharm 262, 125-137 (2003).
N.R. Rabbani and P.C. Seville, J Control Release 110, 130-140 (2005).
B.H. Graham, Food Austr 49, 184-185 (1997).
R.E.M. Verdurmen, P. Menn, J. Ritzert et al., Dry Technol 22, 1403-1461 (2004).
D.F. Bain, D.L. Munday and A. Smith, J Microencapsul 16, 453-474 (1999).
F. Iskandar, L. Gradon and K. Okuyama, J Colloid Interf Sci 265, 296-303 (2003).
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