[en] Headspace solid-phasemicroextraction is a solvent-free sample preparation technique
that is based on the equilibrium among a three-phase system, i.e., sample-headspacefiber.
A compromise between sensitivity and extraction time is usually needed to
optimize the sample throughput, especially when a large number of samples are analyzed,
as usually the case in cross-samples studies. This work explores the capability
of multiple-cumulative trapping solid-phase microextraction on the characterization
of the aroma profiling of olive oils, exploiting the automation capability of a novel
headspace autosampler. It was shown that multiple-cumulative solid-phase microextraction
has the potential to improve the overall sensitivity and burst the level of information
for cross-sample studies by using cumulative shorter extraction times.
Disciplines :
Food science Chemistry
Author, co-author :
Mascrez, Steven ; Université de Liège - ULiège > Département GxABT > Chimie des agro-biosystèmes
Purcaro, Giorgia ; Université de Liège - ULiège > Département GxABT > Chimie des agro-biosystèmes
Language :
English
Title :
Exploring multiple-cumulative trapping solid-phase microextraction for olive oil aroma profiling
Publication date :
May 2020
Journal title :
Journal of Separation Science
ISSN :
1615-9306
eISSN :
1615-9314
Publisher :
Wiley, Weinheim, Germany
Special issue title :
Special Issue: Emerging Thought Leaders in Separation Science
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Bibliography
Souza-Silva, É. A., Reyes-Garcés, N., Gómez-Ríos, G. A., Boyaci, E., Bojko, B., Pawliszyn, J., A critical review of the state of the art of solid-phase microextraction of complex matrices III. Bioanalytical and clinical applications. TrAC - Trends Anal. Chem. 2015, 71, 249–264.
Roszkowska, A., Miękus, N., Bączek, T., Application of solid-phase microextraction in current biomedical research. J. Sep. Sci. 2019, 42, 285–302.
Souza-Silva, É. A., Gionfriddo, E., Pawliszyn, J., A critical review of the state of the art of solid-phase microextraction of complex matrices I. Environmental analysis. TrAC - Trends Anal. Chem. 2015, 71, 236–248.
Llompart, M., Celeiro, M., García-Jares, C., Dagnac, T., Environmental applications of solid-phase microextraction. TrAC - Trends Anal. Chem. 2019, 112, 1–12.
Xu, C. H., Chen, G. S., Xiong, Z. H., Fan, Y. X., Wang, X. C., Liu, Y., Applications of solid-phase microextraction in food analysis. TrAC - Trends Anal. Chem. 2016, 80, 12–29.
Tranchida, P. Q., Maimone, M., Purcaro, G., Dugo, P., Mondello, L., The penetration of green sample-preparation techniques in comprehensive two-dimensional gas chromatography. TrAC - Trends Anal. Chem. 2015, 71, 74–84.
Tranchida, P. Q., Purcaro, G., Maimone, M., Mondello, L., Impact of comprehensive two-dimensional gas chromatography with mass spectrometry on food analysis. J. Sep. Sci. 2016, 39, 149–161.
Pawliszyn, J., Arthur, C. L., Solid phase microextraction with thermal desorption using fused silica optical fibers. Anal. Chem. 1990, 62, 2145–2148.
Pawliszyn, J., Theory of solid-phase microextraction. J. Chromatogr. Sci. 2000, 38, 270–278.
Górecki, T., Yu, X., Pawliszyn, J., Theory of analyte extraction by selected porous polymer SPME fibres. Analyst 1999, 124, 643–649.
Purcaro, G., Cordero, C., Liberto, E., Bicchi, C., Conte, L. S., Toward a definition of blueprint of virgin olive oil by comprehensive two-dimensional gas chromatography. J. Chromatogr. A 2014, 1334, 101–111.
Purcaro, G., Stefanuto, P. H., Franchina, F. A., Beccaria, M., Wieland-Alter, W. F., Wright, P. F., Hill, J. E., SPME-GC×GC-TOF MS fingerprint of virally-infected cell culture: Sample preparation optimization and data processing evaluation. Anal. Chim. Acta 2018, 1027, 158–167.
Stilo, F., Cordero, C., Sgorbini, B., Bicchi, C., Liberto, E., Highly informative fingerprinting of extra-virgin olive oil volatiles: the role of high concentration-capacity sampling in combination with comprehensive two-dimensional gas chromatography. Separations 2019, 6, 34.
Purcaro, G., Rees, C. A., Wieland-alter, W. F., Schneider, M. J., Wang, X., Stefanuto, P., Wright, P. F., Enelow, R. I., Hill, J. E., States, U., States, U., Volatile fingerprinting of human respiratory viruses. J. Breath Res. 2017, 12, 026015.
Purcaro, G., Rees, C. A., Melvin, J. A., Bomberger, J. M., Hill, J. E., Volatile fingerprinting of Pseudomonas aeruginosa and respiratory syncytial virus infection in an in vitro cystic fibrosis co-infection model. J. Breath Res. 2018, 12, 046001.
Sghaier, L., Vial, J., Sassiat, P., Thiebaut, D., Watiez, M., Breton, S., Rutledge, D. N., Cordella, C. B. Y., An overview of recent developments in volatile compounds analysis from edible oils: technique-oriented perspectives. Eur. J. Lipid Sci. Technol. 2016, 118, 1853–1879.
Psillakis, E., Yiantzi, E., Sanchez-Prado, L., Kalogerakis, N., Vacuum-assisted headspace solid phase microextraction: Improved extraction of semivolatiles by non-equilibrium headspace sampling under reduced pressure conditions. Anal. Chim. Acta 2012, 742, 30–36.
Psillakis, E., Mousouraki, A., Yiantzi, E., Kalogerakis, N., Effect of Henry's law constant and operating parameters on vacuum-assisted headspace solid phase microextraction. J. Chromatogr. A 2012, 1244, 55–60.
Yiantzi, E., Kalogerakis, N., Psillakis, E., Design and testing of a new sampler for simplified vacuum-assisted headspace solid-phase microextraction. Anal. Chim. Acta 2016, 927, 46–54.
Psillakis, E., Vacuum-assisted headspace solid-phase microextraction: a tutorial review. Anal. Chim. Acta 2017, 986, 12–24.
Mascrez, S., Psillakis, E., Purcaro, G., A multifaceted investigation on the effect of vacuum on the headspace solid-phase microextraction of extra-virgin olive oil. Anal. Chim. Acta 2020, 1103, 106–114.
Oliver-Pozo, C., Trypidis, D., Aparicio, R., Garciá-González, D. L., Aparicio-Ruiz, R., Implementing dynamic headspace with SPME sampling of virgin olive oil volatiles: optimization, quality analytical study, and performance testing. J. Agric. Food Chem. 2019, 67, 2086–2097.
Lipinski, J., Automated multiple solid phase micro extraction. An approach to enhance the limit of detection for the determination of pesticides in water. Fresenius. J. Anal. Chem. 2000, 367, 445–449.
Chin, S. T., Eyres, G. T., Marriott, P. J., Cumulative solid phase microextraction sampling for gas chromatography-olfactometry of Shiraz wine. J. Chromatogr. A 2012, 1255, 221–227.
Angerosa, F., Servili, M., Selvaggini, R., Taticchi, A., Esposto, S., Montedoro, G., Volatile compounds in virgin olive oil: occurrence and their relationship with the quality. J. Chromatogr. A 2004, 1054, 17–31.
Romero, I., García-González, D. L., Aparicio-Ruiz, R., Morales, M. T., Validation of SPME-GCMS method for the analysis of virgin olive oil volatiles responsible for sensory defects. Talanta 2015, 134, 394–401.
Aparicio, R., Morales, M. T., Aparicio-Ruiz, R., Tena, N., García-González, D. L., Authenticity of olive oil: Mapping and comparing official methods and promising alternatives. Food Res. Int. 2013, 54, 2025–2038.
IOC, Sensory Analysis of Olive Oil - Method for the Organoleptic Assessment of Virgin Olive Oil. International Olive Council, Madrid, Spain 2018.
Massart, D., Chemometrics : A Textbook. Elsevier Science, New York, NY 1988.
Smolinska, A., Hauschild, A.-C., Fijten, R. R. R., Dallinga, J. W., Baumbach, J., van Schooten, F. J., Current breathomics—a review on data pre-processing techniques and machine learning in metabolomics breath analysis. J. Breath Res. 2014, 8, 027105.
Stilo, F., Liberto, E., Reichenbach, S. E., Tao, Q., Bicchi, C., Cordero, C., Untargeted and targeted fingerprinting of extra virgin olive oil volatiles by comprehensive two-dimensional gas chromatography with mass spectrometry: challenges in long-term studies. J. Agric. Food Chem. 2019, 67, 5289–5302.
Oliver-Pozo, C., Aparicio-Ruiz, R., Romero, I., García-González, D. L., Analysis of volatile markers for virgin olive oil aroma defects by SPME-GC/FID: possible sources of incorrect data. J. Agric. Food Chem. 2015, 63, 10477–10483.
Mascrez, S., Psillakis, E., Purcaro, G., A multifaceted investigation on the effect of vacuum on the headspace solid-phase microextraction of extra-virgin olive oil. Anal. Chim. Acta 2019, https://doi.org/10.1016/j.aca.2019.12.053.
Magagna, F., Valverde-Som, L., Ruíz-Samblás, C., Cuadros-Rodríguez, L., Reichenbach, S. E., Bicchi, C., Cordero, C., Combined untargeted and targeted fingerprinting with comprehensive two-dimensional chromatography for volatiles and ripening indicators in olive oil. Anal. Chim. Acta 2016, 936, 245–258.
Trujillo-Rodríguez, M. J., Pino, V., Psillakis, E., Anderson, J. L., Ayala, J. H., Yiantzi, E., Afonso, A. M., Vacuum-assisted headspace-solid phase microextraction for determining volatile free fatty acids and phenols. investigations on the effect of pressure on competitive adsorption phenomena in a multicomponent system. Anal. Chim. Acta 2017, 962, 41–51.
Kolb, B., Ettre, L. E., Static Headspace-Gas Chromatography: Theory and Practice. Wiley-VHC, New York, NY 2006.
Cerretani, L., Salvador, M. D., Bendini, A., Fregapane, G., Relationship between sensory evaluation performed by Italian and spanish official panels and volatile and phenolic profiles of virgin olive oils. Chemosens. Percept. 2008, 1, 258–267.
Cavalli, J. F., Fernandez, X., Lizzani-Cuvelier, L., Loiseau, A. M., Comparison of static headspace, headspace solid phase microextraction, headspace sorptive extraction, and direct thermal desorption techniques on chemical composition of french olive oils. J. Agric. Food Chem. 2003, 51, 7709–7716.
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