Ultra-high performance liquid chromatographic method for the determination of polycyclic aromatic hydrocarbons in a passive environmental sampler

Purcaro, Giorgia; Moret, S.; Bučar-Miklavčič, M.; Conte, L. S.

doi:10.1002/jssc.201100922

Article (Scientific journals)

Ultra-high performance liquid chromatographic method for the determination of polycyclic aromatic hydrocarbons in a passive environmental sampler

Purcaro, Giorgia; Moret, S.; Bučar-Miklavčič, M. et al.

2012 • In Journal of Separation Science, 35 (8), p. 922-928

Peer Reviewed verified by ORBi

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https://hdl.handle.net/2268/231147

DOI
10.1002/jssc.201100922

PubMed
22589152

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Keywords :

Environmental contamination; Passive sampler; Polycyclic aromatic hydrocarbon (PAH); Ultra-high performance liquid chromatography (UHPLC); Acenaphthene; Chromatographic methods; Elution temperature; Fluorenes; Limits of detection; Limits of quantification; Passive samplers; Performance criterion; Polycyclic aromatic hydrocarbons(PAHs); Regression coefficient; Solid-phase extraction; Ultra-high performance; Chromatographic analysis; Chromatography; High performance liquid chromatography; Polyethylene terephthalates; Synthetic fibers; Polycyclic aromatic hydrocarbons; Chromatography, High Pressure Liquid; Limit of Detection; Polycyclic Hydrocarbons, Aromatic; Solid Phase Extraction; Temperature

Abstract :

[en] Polycyclic aromatic hydrocarbons (PAHs) are ubiquitous compounds released in the environment by different sources. The aim of the present work was to validate a solid-phase extraction (SPE) and a rapid ultra-high performance liquid chromatographic (UHPLC) method for the analysis of PAHs in a passive environmental sampler, namely a Dacron® (the commercial name of a synthetic fiber based on polyethylene terephthalate) textile. The elution temperature was optimized to improve the resolution of early-eluted compounds, namely acenaphthene (Ac) and fluorene (F). The UHPLC method lasts about 10 min and showed good linearity for all the 16 PAHs considered, with regression coefficients over 0.99. Recoveries, limits of detection (LODs), and limits of quantification (LOQs) of the SPE method were well within the performance criteria fixed by the Regulation n. 836/2011, namely 0.3 and 0.9 μg/kg, respectively. © 2012 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

Disciplines :

Chemistry
Environmental sciences & ecology

Author, co-author :

Purcaro, Giorgia ; Université de Liège - ULiège > Agronomie, Bio-ingénierie et Chimie (AgroBioChem) > Chimie des agro-biosystèmes

Moret, S.; Dipartimento di Scienze Degli Alimenti, Università di Udine, via Sondrio 2, Udine 33100, Italy

Bučar-Miklavčič, M.; LABS LCC, Institute for Ecology, Olive Oil and Control, Izola, Slovenia

Conte, L. S.; Dipartimento di Scienze Degli Alimenti, Università di Udine, via Sondrio 2, Udine 33100, Italy

Language :

English

Title :

Ultra-high performance liquid chromatographic method for the determination of polycyclic aromatic hydrocarbons in a passive environmental sampler

Publication date :

2012

Journal title :

Journal of Separation Science

ISSN :

1615-9306

eISSN :

1615-9314

Publisher :

Wiley, Weinheim, Germany

Volume :

Issue :

Pages :

922-928

Peer reviewed :

Peer Reviewed verified by ORBi

Available on ORBi :

since 11 January 2019

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Bibliography

Lee, M. L., Novotny, M. V., Bartle, K. D., Analytical Chemistry of Polycyclic Aromatic Compounds, Academic Press, New York 1981.
IARC, Monographs on the Evaluation of Carcinogenic Risks of Chemicals to Humans, Overall Evaluation of Carcinogenicity: An updating of IARC Monographs, vol. 1-42, (Suppl. 7), International Agency for Research on Cancer, World Health Organization, Lyon 1987.
Grimmer, G., Pott, F., in Environmental Carcinogenesis: Polycyclic Aromatic Hydrocarbons (Ed.: Grimmer, G.), CRC Press, Inc., Boca Raton, FL 1983, pp. 61-128.
Grob, K., Biedermann, M., Caramaschi, A., Pacciarelli, B., J. High Resolut. Chromatogr. 1991, 14, 33-39.
Simko, P., Khunova, V., Simon, P., Hruba, M., Int. J. Food Sci. Technol. 1995, 30, 807-812.
Moret, S., Grob, K., Conte, L. S., J. Chromatogr. A 1996, 750, 361-368.
Moret, S., Grob, K., Conte, L. S., Z. Lebensm. Unters. Forsch., A 1997, 204, 241-246.
Compendium Method TO-13A, US Environmental Protection Agency (EPA), Cincinnati, OH 1999.
European Union, Commission Regulation (EC) No 208/2005, Off. J. Eur. Comm. 2005, L34, 3-5.
European Union, Commission Recommendation (EC) No 2005/108/EC, Off. J. Eur. Comm. 2005, L34, 43-45.
European Commission, Opinion of the Scientific Committee on Food on the Risks to Human Health of Polycyclic Aromatic Hydrocarbons in Food., European Commission, Brussels 2002.
Expert Committee on Food Additives, Food and Agriculture Organization (FAO), Rome/World Health Organization (WHO), Summary and conclusions of the sixty-fourth meeting of the Joint FAO/WHO Expert Committee on Food Additives (JECFA), FAO, Geneva 2005.
European Food Safety Authority, EFSA J. 2008, 724, 1-114.
European Union, Commission Regulation (EC) No 835/2011, Off. J. Eur. Comm. 2011, L215, 4-8.
Gómez-Ruiz, J. A., Wenzl, T., Anal. Bioanal. Chem. 2009, 393, 1697-1707.
Ziegenhals, K., Hubschmann, H.-J., Speer, K., Jira, W., J. Sep. Sci. 2008, 31, 1779-1786.
Purcaro, G., Moret, S., Conte, L.S., J. Chromatogr. A 2007, 1176, 231-235.
Moret, S., Conte, L. S., J. Sep. Sci. 2002, 25, 96-100.
Manoli, E., Samara, C., Trends Anal. Chem. 1999, 18, 417-428.
Akpambang, V. O. E., Purcaro, G., Lajide, L., Amoo, I. A., Conte, L. S., Moret, S., Food Addit. Contam. 2009, 26 (7) 1096-1103.
Purcaro, G., Moret, S., Conte, L. S., J. Sep. Sci. 2008, 31, 3936-3944.
Simon, R., Palme, S., Anklam, E., Food Chem. 2007, 104, 876-887.
Welsch, T., Michalke, D., J. Chromatogr. A 2003, 1000, 935-951.
Gerber, F., Krummen, M., Potgeter, H., Roth, A., Siffrin, C., Spoendlin, C., J. Chromatogr. A 2004, 1036, 127-133.
Poppe, H., J. Chromatogr. A 1997, 778, 3-21.
Li, J., Hu, Y., Carr, P. W., Anal. Chem. 1997, 69, 3884-3888.
Guillarme, D., Russo, R., Rudaz, S., Bicchi, C., Veuthey, J. L., Curr. Pharm. Anal. 2007, 4, 221-229.
Lestremau, F., De Villiers, A., Lynen, F., Cooper, A., Szucs, R., Sandra, P., J. Chromatogr. A 2007, 1138, 120-131.
Tanaka, N., Kobayashi, H., Ishizuka, N., Minakuchi, H., Nakanishi, K., Hosoya, K., Ikegami, T., J. Chromatogr. A 2002, 965, 35-49.
Minakuchi, H., Nakanishi, K., Soga, N., Ishizuka, N., Tanaka, N., Anal. Chem. 1996, 68, 3498-3501.
MacNair, J. E., Lewis, K. C., Jorgenson, J. W., Anal. Chem. 1997, 69, 983-989.
MacNair, J. E., Patel, K. D., Jorgenson, J. W., Anal. Chem. 1999, 71, 700-708.
Patel, K. D., Jerkovich, A. D., Link J. C., Jorgenson, J. W., Anal. Chem. 2004, 76, 5777-5786.
Wu, N., Lippert, J. A., Lee, M. L., J. Chromatogr. A 2001, 911, 1-12.
Wren, S. A. C., Tchelitcheff, P., J. Chromatogr. A 2006, 1119, 140-146.
Deconinck, E., Sacré, P. Y., Baudewyns, S., Courselle, P., De Beer, J., J. Pharm. Biomed. Anal. 2011, 56 (2), 200-209.
Latorre-Moratalla, M.L., Bosch-Fusté, J., Lavizzari, T., Bover-Cid, S., Veciana-Nogués, M. T., Vidal-Carou, M. C., J. Chromatogr. A 2009, 1216, 7715-7720.
Liu, R., Hei, W., He, P., Li, Z., J. Chromatogr. B 2011, 879, 2416-2422.
Suomela, J.-P., Leskinen, H., Kallio, H., J. Agric. Food Chem. 2011, 59, 8095-8100.
Kim, J.-W., Isobe, T., Chang, K.-H., Amano, A., Maneja, R. H., Zamora, P. B., Siringan, F. P., Tanabe, S., Environ. Pollut. 2011, 159, 3653-3659
Gosetti, F., Chiuminatto, U., Mazzucco, E., Robotti, E., Calabrese, G., Gennaro, M.C., Marengo, E., J. Chromatogr. A 2011, 1218, 6308-6318.
Skert, N., Falomo, J., Giorgini, L., Acquavita, A., Capriglia, L., Grahonja, R., Miani, N., Water Air Soil Pollut. 2010, 206, 95-103.
Fiselier, K., Grob, K., Workshop: Mineral Oil Material in Food: Analytical methods, Occurrence and Evaluation" of EU-DG-SANCO and the Official Food Control Authority of Zurich, Zurich, Switzerland, September 17/18, 2008.
The Fitness for Purpose of Analytical Methods: A Laboratory Guide to Method Validation and Related Topics, EURACHEM Guide, First English edition 1.0-1998, LCG Ltd., Teddington 1998.
Draper, N., Smith, H., Applied Regression Analysis, Wiley, New York 1981.
de Villers, A., Lauer, H., Szucs, R., Goodall, S., Sandra, P., J. Chromatogr. A 2006, 1113, 84-91.