Optimisation and validation of a generic method for the LC assay of six corticosteroids and salicylic acid in dermopharmaceutical forms

Marini Djang'Eing'A, Roland; Pantella, A.; Bimazubute, Marcel; Chiap, Patrice; Hubert, Philippe; Crommen, Jacques

doi:10.1007/BF02491657

Article (Scientific journals)

Optimisation and validation of a generic method for the LC assay of six corticosteroids and salicylic acid in dermopharmaceutical forms

Marini Djang'Eing'A, Roland; Pantella, A.; Bimazubute, Marcel et al.

2002 • In Chromatographia, 55 (5-6), p. 263-269

Peer Reviewed verified by ORBi

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https://hdl.handle.net/2268/1684

DOI
10.1007/BF02491657

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Keywords :

column liquid chromatography; corticosteroids; salicylic acid; dermatological formulations; method validation

Abstract :

[en] A generic method was developed for the liquid chromatographic (LC) assay of six corticosteroids and salicylic acid in different dermatological formulations containing methylparaben and propylparaben or sorbic acid as preservatives. An adequate separation was obtained using octadecylsilica as stationary phase and a mixture of acetonitrile (MeCN) and 25 mM phosphate buffer of pH 3.5 as mobile phase. Segmented gradient elution was applied from 30 to 45% of MeCN in 9.9 minutes, then from 45 to 96% in 19.0 minutes. UV detection was performed at 240 nm. The method was validated. Very good results were obtained with respect to linearity selectivity, precision and accuracy.

Disciplines :

Biochemistry, biophysics & molecular biology
Chemistry

Author, co-author :

Marini Djang'Eing'A, Roland ; Université de Liège - ULiège > Département de pharmacie > Chimie analytique

Pantella, A.

Bimazubute, Marcel

Chiap, Patrice ; Université de Liège - ULiège > Département de pharmacie > Analyse des médicaments

Hubert, Philippe ; Université de Liège - ULiège > Chimie analytique

Crommen, Jacques ; Université de Liège - ULiège > Département de pharmacie > Analyse des médicaments

Language :

English

Title :

Optimisation and validation of a generic method for the LC assay of six corticosteroids and salicylic acid in dermopharmaceutical forms

Publication date :

March 2002

Journal title :

Chromatographia

ISSN :

0009-5893

eISSN :

1612-1112

Publisher :

Vieweg, Wiesbaden, Germany

Volume :

Issue :

5-6

Pages :

263-269

Peer reviewed :

Peer Reviewed verified by ORBi

Available on ORBi :

since 07 April 2010

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