First synthesis of a '1,2-diquinone-calix[4]arene'. Interaction of its reduced form with Ag+

Vataj, Rame; Ridaoui, Hassan; Louati, Alain; Gabelica, Valérie; Steyer, Stéphane; Matt, Dominique

doi:10.1016/S0022-0728(01)00734-3

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First synthesis of a '1,2-diquinone-calix[4]arene'. Interaction of its reduced form with Ag+

Vataj, Rame; Ridaoui, Hassan; Louati, Alain et al.

2002 • In Journal of Electroanalytical Chemistry, 519 (1-2), p. 123–129

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https://hdl.handle.net/2268/798

DOI
10.1016/S0022-0728(01)00734-3

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Keywords :

calixarene; electrochemistry; calixdiquinone; silver(I) detection; mass spectrometry

Abstract :

[en] Electrochemical oxidation of 5,11,17,23-tetra-tert-butyl-25,26-bis(diphenylphosphinoylmethoxy)-27,28-dihydroxycalix[4]arene (3), a calixarene with two phosphoryl units appended on proximal positions, affords the corresponding '1,2-diquinonecalix[4]arene' (4). The formation of 4 results from nucleophilic attack of residual water on anodically generated diphenoxylium. cations. Preliminary voltammetric experiments in CH3CN on a platinum electrode showed that 4 is suitable for electrochemical detection of the silver metal cation. (C) 2002 Elsevier Science B.V. All rights reserved.

Disciplines :

Chemistry

Author, co-author :

Vataj, Rame

Ridaoui, Hassan

Louati, Alain

Gabelica, Valérie ; Université de Liège - ULiège > Chimie physique, spectrométrie de masse

Steyer, Stéphane

Matt, Dominique

Language :

English

Title :

First synthesis of a '1,2-diquinone-calix[4]arene'. Interaction of its reduced form with Ag+

Publication date :

2002

Journal title :

Journal of Electroanalytical Chemistry

ISSN :

0022-0728

Publisher :

Elsevier Science

Volume :

519

Issue :

1-2

Pages :

123–129

Peer reviewed :

Peer Reviewed verified by ORBi

Additional URL :

http://www.elsevier.com/locate/jelechem

Funders :

F.R.S.-FNRS - Fonds de la Recherche Scientifique [BE]

Commentary :

This is a postprint version of an article published in Journal of Electroanalytical Chemistry 519 (2002) 123–129.

Available on ORBi :

since 05 November 2008

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