Article (Scientific journals)
Characterization of the porous structure of biodegradable scaffolds obtained with supercritical CO2 as foaming agent
Léonard, Angélique; Calberg, Cédric; Kerckhofs, Greet et al.
2008In Journal of Porous Materials, 15 (4), p. 397-403
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Keywords :
biomaterial; scaffold; green technology; supercritical carbon dioxide; 3D reconstruction; supercritical CO2
Abstract :
[en] Poly(ε-caprolactone) foams were prepared, via a batch process, by using supercritical CO2 as foaming agent. Their porous structure was characterized through mercury porosimetry, helium and mercury pycnometry, scanning electron microscopy (SEM) and X-ray microtomography observations coupled with image analysis. The pore size distributions obtained by these two latter techniques show that the pore structure is more homogeneous when the foaming process is performed under a high CO2 saturation pressure (higher than 250 bars).
Research Center/Unit :
Center for Education and Research on Macromolecules (CERM)
Disciplines :
Materials science & engineering
Chemistry
Author, co-author :
Léonard, Angélique  ;  Université de Liège - ULiège > Département de chimie appliquée > Génie chimique - Procédés et développement durable
Calberg, Cédric ;  Université de Liège - ULiège > Department of Applied Chemistry > Laboratory of Industrial Chemistry
Kerckhofs, Greet ;  Universiteit Leuven (KUL) > Metallurgy and Materials Engineering
Wevers, Martine;  Universiteit Leuven (KUL) > Metallurgy and Materials Engineering
Jérôme, Robert ;  Université de Liège - ULiège > Department of Chemistry > Center for Education and Research on Macromolecules (CERM)
Pirard, Jean-Paul ;  Université de Liège - ULiège > Department of Applied Chemistry > Laboratory of Chemical Engineering
Germain, Albert ;  Université de Liège - ULiège > Department of Applied Chemistry > Laboratory of Industrial Chemistry
Blacher, Silvia ;  Université de Liège - ULiège > Department of Applied Chemistry > Laboratory of Chemical Engineering
Language :
English
Title :
Characterization of the porous structure of biodegradable scaffolds obtained with supercritical CO2 as foaming agent
Publication date :
August 2008
Journal title :
Journal of Porous Materials
ISSN :
1380-2224
eISSN :
1573-4854
Publisher :
Springer, Dordrecht, Netherlands
Volume :
15
Issue :
4
Pages :
397-403
Peer reviewed :
Peer Reviewed verified by ORBi
Funders :
F.R.S.-FNRS - Fonds de la Recherche Scientifique
The Ministry of the ‘‘Communauté française de Belgique’’, Belgium (Action de Recherche Concertée 00/05-265) and the Ministry of ‘‘Région Wallonne’’ (DGTRE), Belgium, in the frame of the W.D.U. and WINNOMAT programs
Commentary :
The original publication is available at http://www.springerlink.com/content/q031375562m60m8n/fulltext.pdf. The authors acknowledge Journal of Porous Materials (Springer) for allowing them to archive this paper.
Available on ORBi :
since 22 April 2013

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