Wang, S., Chen, X., Han, X., Hong, X., Li, X., Zhang, H., Li, M., Wang, Z., Zheng, A., A review of 3D printing Technology in Pharmaceutics: technology and applications, now and future. Pharmaceutics, 15, 2023, 416, 10.3390/pharmaceutics15020416.
Parulski, C., Bya, L.-A., Goebel, J., Servais, A.-C., Lechanteur, A., Evrard, B., Development of 3D printed mini-waffle shapes containing hydrocortisone for children's personalized medicine. Int. J. Pharm., 642, 2023, 123131, 10.1016/j.ijpharm.2023.123131.
Jørgensen, A.K., Ong, J.J., Parhizkar, M., Goyanes, A., Basit, A.W., Advancing non-destructive analysis of 3D printed medicines. Trends Pharmacol. Sci. 44 (2023), 379–393, 10.1016/j.tips.2023.03.006.
Yang, T.L., Szewc, J., Zhong, L., Leonova, A., Giebułtowicz, J., Habashy, R., Isreb, A., Alhnan, M.A., The use of near-infrared as process analytical technology (PAT) during 3D printing tablets at the point-of-care. Int. J. Pharm., 642, 2023, 123073, 10.1016/j.ijpharm.2023.123073.
Vankeirsbilck, T., Vercauteren, A., Baeyens, W., Van der Weken, G., Verpoort, F., Vergote, G., Remon, J.P., Applications of Raman spectroscopy in pharmaceutical analysis, TrAC. Trends Anal. Chem. 21 (2002), 869–877, 10.1016/S0165-9936(02)01208-6.
Tumuluri, V.S., Kemper, M.S., Lewis, I.R., Prodduturi, S., Majumdar, S., Avery, B.A., Repka, M.A., Off-line and on-line measurements of drug-loaded hot-melt extruded films using Raman spectroscopy. Int. J. Pharm. 357 (2008), 77–84, 10.1016/j.ijpharm.2008.01.036.
Saerens, L., Segher, N., Vervaet, C., Remon, J.P., De Beer, T., Validation of an in-line Raman spectroscopic method for continuous active pharmaceutical ingredient quantification during pharmaceutical hot-melt extrusion. Anal. Chim. Acta 806 (2014), 180–187, 10.1016/j.aca.2013.11.020.
Saerens, L., Dierickx, L., Lenain, B., Vervaet, C., Remon, J.P., Beer, T.D., Raman spectroscopy for the in-line polymer–drug quantification and solid state characterization during a pharmaceutical hot-melt extrusion process. Eur. J. Pharm. Biopharm. 77 (2011), 158–163, 10.1016/j.ejpb.2010.09.015.
Thiry, J., Lebrun, P., Vinassa, C., Adam, M., Netchacovitch, L., Ziemons, E., Hubert, P., Krier, F., Evrard, B., Continuous production of itraconazole-based solid dispersions by hot melt extrusion: Preformulation, optimization and design space determination. Int. J. Pharm. 515 (2016), 114–124, 10.1016/j.ijpharm.2016.10.003.
Krier, F., Mantanus, J., Sacré, P.-Y., Chavez, P.-F., Thiry, J., Pestieau, A., Rozet, E., Ziemons, E., Hubert, P., Evrard, B., PAT tools for the control of co-extrusion implants manufacturing process. Int. J. Pharm. 458 (2013), 15–24, 10.1016/j.ijpharm.2013.09.040.
Hubert, Ph., Nguyen-Huu, J.-J., Boulanger, B., Chapuzet, E., Chiap, P., Cohen, N., Compagnon, P.-A., Dewé, W., Feinberg, M., Lallier, M., Laurentie, M., Mercier, N., Muzard, G., Nivet, C., Valat, L., Harmonization of strategies for the validation of quantitative analytical procedures: a SFSTP proposal—part I. J. Pharm. Biomed. Anal. 36 (2004), 579–586, 10.1016/j.jpba.2004.07.027.
Hubert, Ph., Nguyen-Huu, J.-J., Boulanger, B., Chapuzet, E., Chiap, P., Cohen, N., Compagnon, P.-A., Dewé, W., Feinberg, M., Lallier, M., Laurentie, M., Mercier, N., Muzard, G., Nivet, C., Valat, L., Rozet, E., Harmonization of strategies for the validation of quantitative analytical procedures: a SFSTP proposal – part II. J. Pharm. Biomed. Anal. 45 (2007), 70–81, 10.1016/j.jpba.2007.06.013.
Chamberlain, R., Breitkreutz, J., Fischer, B., Drug content determination of low-dosed hot-melt extruded filaments using Raman spectroscopy. Pharm. Dev. Technol. 29 (2024), 258–264, 10.1080/10837450.2024.2323622.
Hubert, Ph., Nguyen-Huu, J.-J., Boulanger, B., Chapuzet, E., Cohen, N., Compagnon, P.-A., Dewé, W., Feinberg, M., Laurentie, M., Mercier, N., Muzard, G., Valat, L., Rozet, E., Harmonization of strategies for the validation of quantitative analytical procedures: a SFSTP proposal–Part III. J. Pharm. Biomed. Anal. 45 (2007), 82–96, 10.1016/j.jpba.2007.06.032.
I.H.T. Guideline, Validation of Analytical Procedures Q2 (R2), ICH Geneva Switz. https://pink.citeline.com/-/media/supporting-documents/pink-sheet/2022/04/p0422ema_21.pdf, 2022. (Accessed 26 May 2025)
Hydrocortisone - European Pharmacopoeia 11.8, (n.d.). https://pheur.edqm.eu/app/11-8/content/11-8/0335E.htm?highlight=on&terms%5B%5D=hydrocortisone (accessed May 26, 2025).
Afseth, N.K., Kohler, A., Extended multiplicative signal correction in vibrational spectroscopy, a tutorial. Chemom. Intel. Lab. Syst. 117 (2012), 92–99, 10.1016/j.chemolab.2012.03.004.
Kucheryavskiy, S., mdatools – R package for chemometrics. Chemom. Intel. Lab. Syst., 198, 2020, 103937, 10.1016/j.chemolab.2020.103937.
Manivannan, P., Kumar, R.T., Periyanayagasamy, V., Spectral analysis of hydrocortisone. J. Chem. Pharm. Sci. 2 (2009), 1–5.
Li, L., Liang, X., Xu, T., Xu, F., Dong, W., Rapid detection of six glucocorticoids added illegally to dietary supplements by combining TLC with spot-concentrated Raman scattering. Molecules, 23, 2018, 1504, 10.3390/molecules23071504.
Gracie, K., Pang, S., Jones, G.M., Faulds, K., Braybrook, J., Graham, D., Detection of cortisol in serum using quantitative resonance Raman spectroscopy. Anal. Methods 9 (2017), 1589–1594, 10.1039/C6AY03296F.
Rutledge, D.N., Jouan-Rimbaud Bouveresse, D., Independent components analysis with the JADE algorithm. TrAC Trends Anal. Chem. 50 (2013), 22–32, 10.1016/j.trac.2013.03.013.