Mg alloys; Friction stir processing; Metal matrix composites; Mechanical properties; Microstructures; LiMaRC - Liège Materials Research Center
Abstract :
[en] Short C fibres-Mg matrix composites have been produced by friction stir processing sandwiches made of a layer of C fabric stacked between two sheets of Mg alloy AZ31B or AZ91D. This novel processing technique can allow the easy production of large-scale metal matrix composites. The paper investigates the microstructure of FSPed C fibre-Mg composites in relation with the fragmentation of the C fibres during FSP and their influence on the tensile properties. 3D X-ray tomography reveals that the fibres orient like onion rings and are more or less fragmented depending on the local shear stress during the process. The fibre volume fraction can be increased from 2.3% to 7.1% by reducing the nugget volume, i.e. by using a higher advancing speed in AZ31B alloy or a stronger matrix alloy, like AZ91D alloy. A higher fibre volume fraction leads to a smaller grain size which brings about an increase of the composite yield strength by 15 to 25%. However, a higher fibre volume fraction also leads to a lower fracture strain. Fracture surface observations reveal that damage occurs by fibre/matrix decohesion along fibres oriented perpendicularly to the loading direction.
Disciplines :
Materials science & engineering
Author, co-author :
Mertens, Anne ; Université de Liège > Département d'aérospatiale et mécanique > Science des matériaux métalliques
Simar, Aude; Université Catholique de Louvain - UCL > Institute of Mechanics, Materials and Civil Engineering > IMAP
Adrien, Jérôme; Institut National des Sciences Appliquées de Lyon > MATEIS Laboratory
Maire, Eric; Institut National des Sciences Appliquées de Lyon > MATEIS Laboratory
Montrieux, Henri-Michel ; Université de Liège > Département d'aérospatiale et mécanique > Science des matériaux métalliques
Delannay, Francis; Université Catholique de Louvain - UCL > Institute of Mechanics, Materials and Civil Engineering > IMAP
Lecomte-Beckers, Jacqueline ; Université de Liège > Département d'aérospatiale et mécanique > Science des matériaux métalliques
Language :
English
Title :
Influence of Fibre Distribution and Grain Size on the Mechanical Behaviour of Friction Stir Processed Mg-C Composites
Publication date :
2015
Journal title :
Materials Characterization
ISSN :
1044-5803
Publisher :
Elsevier Science, New York, United States - New York
B.L. Mordike, and T. Ebert Magnesium properties - applications - potential Mater. Sci. Eng. A 302 2001 37 45
M.S. Yong, and A.J. Clegg Process optimisation for a squeeze cast magnesium alloy metal matrix composite J. Mater. Process. Technol. 168 2005 262 269
H.S. Arora, H. Singh, and B.K. Dhindaw Composite fabrication using friction stir processing - a review Int. J. Adv. Manuf. Technol. 61 2012 1043 1055
D. Khayyamin, A. Mostafapour, and R. Keshmiri The effect of process parameters on microstructural characteristics of AZ91/SiO2 composite fabricated by FSP Mater. Sci. Eng. A 539 2013 217 221
F. Delannay, L. Froyen, and A. Deruyttere The wetting of solids by molten metals and its relation in the preparation of metal-matrix composites J. Mater. Sci. 22 1987 1 16
J.C. Viala, G. Claveyrolas, F. Bosselet, and J. Bouix Chemical behaviour of carbon fibres in magnesium base Mg-Al alloys J. Mater. Sci. 35 2000 1813 1825
R.S. Mishra, M.W. Mahoney, S.X. McFadden, N.A. Mara, and A.K. Mukherjee High strain rate superplasticity in a friction stir processed 7075 Al alloy Scr. Mater. 42 2000 163 168
R.S. Mishra, and Z.Y. Ma Friction stir welding and processing Mater. Sci. Eng. R 50 2005 1 78
Z.Y. Ma Friction stir processing technology: a review Metall. Mater. Trans. A 39 2008 642 658
M.-N. Avettand-Fènoël, A. Simar, R. Shabadi, R. Taillard, and B. de Meester Characterization of oxide dispersion strengthened copper based materials developed by friction stir processing Mater. Des. 60 2014 343 357
B. Zahmatkesh, and M.H. Enayati A novel approach for development of surface nanocomposite by friction stir processing Mater. Sci. Eng. A 527 2010 6734 6740
V.C. Gudla, F. Jensen, A. Simar, R. Shabadi, and R. Ambat Friction stir processing Al-TiO2 surface composites: anodising behaviour and optical appearance Appl. Surf. Sci. 324 2015 554 562
M. Yang, C. Xu, C. Wu, K. Lin, Y.J. Chao, and L. An Fabrication of AA6061/Al2O3 nano ceramic particle reinforced composite coating by using friction stir processing J. Mater. Sci. 45 2010 4431 4438
R.M. Miranda, T.G. Santos, J. Gandra, N. Lopes, and R.J.C. Silva Reinforcement strategies for producing functionally graded materials by friction stir processing in aluminium alloys J. Mater. Process. Technol. 213 2013 1609 1615
Y. Huang, T. Wang, W. Guo, L. Wan, and S. Lv Microstructure and surface mechanical property of AZ31 Mg/SiCp surface composite fabricated by direct friction stir processing Mater. Des. 59 2014 274 278
A. Mertens, A. Simar, and F. Delannay C fibres-Mg matrix composites produced by squeeze casting and friction stir processing: microstructures & mechanical behaviour Mater. Sci. Forum 706-709 2012 1221 1226
A. Mertens, A. Simar, H.-M. Montrieux, J. Halleux, F. Delannay, and J. Lecomte-Beckers Friction stir processing of magnesium matrix composites reinforced with carbon fibres: influence of the matrix characteristics and of the processing parameters on the microstructural developments W.J. Poole, K.U. Kainer, Proc. of the 9th Int. Conf. on Magnesium Alloys and Their Applications 2012 845 850
W. Yuan, S.K. Panigrahi, and R.S. Mishra Achieving high strength and high ductility in friction stir-processed cast magnesium alloy Metall. Mater. Trans. A 44 2013 3675 3684
I.J. Polmear Light Alloys: From Traditional Alloys to Nanocrystals 4th ed. 2006 Elsevier/Butterworth-Heinemann Oxford, Burlington, MA 239
C. Salmon, F. Boland, C. Colin, C. Leroy, and F. Delannay Properties of lead anodes reinforced by carbon or glass creep fibers Intérêts technologiques et marchés potentiels des composites à matrice métallique - Actes du colloque franco-canadien de septembre 1995 1997 Les Presses de l'Ecole des Mines Paris 170 189
C. Jonckheere, B. de Meester, A. Denquin, and A. Simar Torque, temperature and hardening precipitation evolution in dissimilar friction stir welds between 6061-T6 and 2014-T6 aluminum alloys J. Mater. Process. Technol. 213 2013 826 837
Y.H. Yin, N. Sun, T.H. North, and S.S. Hu Hook formation and mechanical properties in AZ31 friction stir spot welds J. Mater. Process. Technol. 210 2012 2062 2070
J.-Y. Buffiere, E. Maire, J. Adrien, J.-P. Masse, and E. Boller In situ experiments with X ray tomography: an attractive tool for experimental mechanics Exp. Mech. 50 2010 289 305
C. Landron, E. Maire, O. Bouaziz, J. Adrien, L. Lecarme, and A. Bareggi Validation of void growth model using X ray microtomography characterization of damage in dual phase steels Acta Mater. 59 2011 7564 7673
A. Razal Rose, K. Manisekar, and V. Balasubramanian Influences of welding speed on tensile properties of friction stir welded AZ61A magnesium alloy J. Mater. Eng. Perform. 21 2012 257 265
F.J. Humphrey, and M. Hatherly Recrystallization and Related Annealing Phenomena 2nd ed. 2004 Elsevier Oxford 285 319
A. Wójcicka, K. Mroczka, P. Kurtyka, M. Binkowski, and Z. Wróbel X ray microtomography analysis of the aluminum alloy composite reinforced by SiC after friction stir processing J. Mater. Eng. Perform. 23 2014 3215 3221
M. Knezevic, A. Levinson, R. Harris, R.K. Mishra, R.D. Doherty, and S.R. Kalidindi Deformation twinning in AZ31: influence on strain hardening and texture evolution Acta Mater. 58 2010 6230 6242
L. Cizek, M. Greger, L. Pawlica, L.A. Dobrzanski, and T. Tanski Study of selected properties of magnesium alloy AZ91 after heat treatment and forming J. Mater. Process. Technol. 157-158 2004 466 471
T.W. Clyne, and P.J. Withers An Introduction to Metal Matrix Composites 1993 Cambridge University Press Cambridge, UK 20 30
S.R. Agnew, J.A. Horton, T.M. Lillo, and D.W. Brown Enhanced ductility in strongly textured magnesium produced by equal channel angular processing Scr. Mater. 50 2004 377 381
W. Yuan, and R.S. Mishra Grain size and texture effects on deformation behavior of AZ31 magnesium alloy Mater. Sci. Eng. A 558 2012 716 724
R. Xin, B. Li, A. Liao, Z. Zhou, and Q. Liu Correlation between texture variation and transverse tensile behavior of friction-stir-processed AZ31 Mg alloy Metall. Mater. Trans. A 43 2012 2500 2508
J. Yang, B.L. Xiao, D. Wang, and Z.Y. Ma Effects of heat input on tensile properties and fracture behavior of friction stir welded Mg-3Al-1Zn alloy Mater. Sci. Eng. A 527 2010 708 714
R. Xin, D. Liu, B. Li, L. Sun, Z. Zhou, and Q. Liu Mechanisms of fracture and inhomogeneous deformation on transverse tensile test of friction-stir-processed AZ31 Mg alloy Mater. Sci. Eng. A 565 2013 333 341
J.A. del Valle, P. Rey, D. Gesto, D. Verdera, J.A. Jimenez, and O.A. Ruano Mechanical properties of ultra-fine grained AZ91 magnesium alloy processed by friction stir processing Mater. Sci. Eng. A 628 2015 198 206
S.H. Park, S.G. Hong, and C.S. Lee Activation mode dependent {10-12} twinning characteristics in a polycristalline magnesium alloy Scr. Mater. 62 2010 202 205
S. Kalpakjian, and S.R. Schmid Manufacturing Engineering and Technology 6th ed. 2010 Pearson Singapore 72