Article (Scientific journals)
Interlaboratory studies on two high-performance liquid chromatographic assays for tylosin (tartrate)
Vander Heyden, Y.; Saevels, J.; Roets, E. et al.
1999In Journal of Chromatography. A, 830 (1), p. 3-28
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Keywords :
tutorial; interlaboratory study; ISO guidelines; tylosin
Abstract :
[en] An interlaboratory study was performed on two high-performance liquid chromatographic methods to determine tylosin. The first method is a reversed-phase HPLC on a C-18 column, while the second is a method using a polymeric stationary phase. The first method is described in several pharmacopoeia monographs on tylosin, to determine the composition of a tylosin mixture, while the second method is recently proposed to determine both the composition and the contents in such a mixture. The interlaboratory studies were set-up and interpreted according to ISO guidelines. This paper is written as a tutorial type of article explaining the principles and methods of these guidelines. The results of both methods were compared. Both were found to have disadvantages but in general the old method is still preferred, both for composition determination and to assay the components. (C) 1999 Elsevier Science B.V. All rights reserved.
Disciplines :
Chemistry
Pharmacy, pharmacology & toxicology
Author, co-author :
Vander Heyden, Y.
Saevels, J.
Roets, E.
Hoogmartens, J.
Decolin, D.
Quaglia, M. G.
Van den Bossche, W.
Leemans, R.
Smeets, O.
Van de Vaart, F.
Mason, B.
Taylor, G. C.
Underberg, W.
Bult, A.
Chiap, Patrice ;  Université de Liège - ULiège > Département de pharmacie > Département de pharmacie
Crommen, Jacques ;  Université de Liège - ULiège > Département de pharmacie > Analyse des médicaments
De Beer, J.
Hansen, S. H.
Massart, D. L.
More authors (9 more) Less
Language :
English
Title :
Interlaboratory studies on two high-performance liquid chromatographic assays for tylosin (tartrate)
Publication date :
1999
Journal title :
Journal of Chromatography. A
ISSN :
0021-9673
eISSN :
1873-3778
Publisher :
Elsevier Science, Amsterdam, Netherlands
Volume :
830
Issue :
1
Pages :
3-28
Peer reviewed :
Peer Reviewed verified by ORBi
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