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1H NMR (CDCl3, 500 MHz, δ): 3.5 (2H, t, ClCH2), 2.9 (2H, t, NCH2), 1.9 (2H, m, CH2), 0.75 (4H, S, SiCH2), 0.09 (12H, s, SiCH3). The product was dried over CaH2 and distilled as a colorless liquid, which was directly used for the synthesis of the initiator.
