On the L-PBF Fabrication of a Novel Medium Carbon, High Silicon Nanostructured Bainitic Steel with and Without Substrate Pre-heating: Density and Microstructural Investigation - 2025
On the L-PBF Fabrication of a Novel Medium Carbon, High Silicon Nanostructured Bainitic Steel with and Without Substrate Pre-heating: Density and Microstructural Investigation
[en] Laser powder bed fusion (L-PBF) metals are often characterized by fabrication defects, such as lack of fusion and stress-induced cracks, which significantly impact the mechanical behavior and structural integrity of the produced components. Substrate pre-heating has emerged as an effective strategy to enhance part density and reduce defect formation. During the fabrication of advanced high-strength steels (AHSS), the combination of high hardenability and rapid cooling rates typically results in untempered martensitic microstructures, necessitating post-fabrication heat treatments, increasing the manufacturing process's complexity, duration, and cost. In this study, the effects of substrate pre-heating and in situ heat treatment were investigated using a nanostructured bainitic steel with a composition of 0.38C-3.2Si-2.8Mn-0.1Al (wt.%). Substrate pre-heating at 320°C, combined with a 1.5-h isothermal holding following fabrication, resulted in improved specimen density and a significant reduction in process-induced cracks. Furthermore, an in situ isothermal heat treatment during fabrication facilitated the development of the desired nanostructured-bainitic microstructure, eliminating additional post-fabrication heat treatments. A comprehensive specimen characterization was conducted using optical microscopy (OM), SEM, TEM, XRD, and nano-hardness measurements. The results demonstrate the potential of combining substrate pre-heating with in situ heat treatment to optimize the microstructure of AHSS fabricated via L-PBF while streamlining the manufacturing process.
Disciplines :
Materials science & engineering
Author, co-author :
Franceschi, Mattia ; Department of Engineering and Management, University of Padova, Vicenza, Italy
Saggionetto, Enrico ; Université de Liège - ULiège > Aérospatiale et Mécanique (A&M)
Yazdanpanah, Arshad; Department of Industrial Engineering, University of Padova, Padua, Italy
Pezzato, Luca; Institute of Condensed Matter Chemistry and Energy Technologies (ICMATE) National Research Council of ItalyC.so Stati Uniti 4, Padua, Italy
Mertens, Anne ; Université de Liège - ULiège > Aérospatiale et Mécanique (A&M)
Dabalà, Manuele; Department of Industrial Engineering, University of Padova, Padua, Italy
Language :
English
Title :
On the L-PBF Fabrication of a Novel Medium Carbon, High Silicon Nanostructured Bainitic Steel with and Without Substrate Pre-heating: Density and Microstructural Investigation
Publication date :
20 August 2025
Journal title :
JOM : the journal of the Minerals, Metals and Materials Society
EU - European Union F.R.S.-FNRS - Fonds de la Recherche Scientifique
Funding text :
M. Franceschi thanks the European Union-NextGenerationEU, in the frame of the project iNEST-Interconnected Nord-Est Innovation Ecosystem (iNEST ECS00000043\u2013Spoke 5*). E. Saggionetto and A. Mertens acknowledge the support of the FNRS (Fonds National de la Recherche Scientifique of Belgium, under PDR no. 35298295).
A. Gisario M. Kazarian F. Martina M. Mehrpouya J. Manuf. Syst. 53 124 149 10.1016/j.jmsy.2019.08.005
K. Kosiba T. Gustmann J.T. Kim J. Seok J. Jung L. Beyer S. Scudino L. Giebeler J. Han J.K. Hufenbach J. Alloys Compd. 967 1:CAS:528:DC%2BB3sXhslCkur3M 10.1016/j.jallcom.2023.171773 171773
S. Cooke K. Ahmadi S. Willerth R. Herring J. Manuf. Process. 57 978 1003 10.1016/j.jmapro.2020.07.025
C.Y. Yap C.K. Chua Z.L. Dong Z.H. Liu D.Q. Zhang L.E. Loh S.L. Sing Appl. Phys. Rev. 10.1063/1.4935926
W.E. King A.T. Anderson R.M. Ferencz N.E. Hodge C. Kamath S.A. Khairallah A.M. Rubenchik Appl. Phys. Rev. 10.1063/1.4937809
J. Zhang B. Song Q. Wei D. Bourell Y. Shi J. Mater. Sci. Technol. 35 270 284 1:CAS:528:DC%2BB38XhtV2ktrfF 10.1016/j.jmst.2018.09.004
L. Pezzato, C. Gennari, M. Franceschi, K. Brunelli, Sci. Rep. (2022).
T. Wegener J. Koopmann J. Richter P. Krooß T. Niendorf Fatigue Fract. Eng. Mater. Struct. 44 2570 2590 1:CAS:528:DC%2BB3MXhtlGlsLbN 10.1111/ffe.13527
C. Wallis B. Buchmayr Mater. Sci. Eng. A 744 215 223 1:CAS:528:DC%2BC1cXisFWrurzK 10.1016/j.msea.2018.12.017
A. Yazdanpanah M. Franceschi R.I. Revilla S. Khademzadeh I. De Graeve M. Dabalà Corros. Sci. 10.1016/j.corsci.2022.110642
A. Yazdanpanah, R.I. Revilla, M. Franceschi, A. Fabrizi, S. Khademzadeh, M. Khodabakhshi, I. Graeve-, and Dabal M, Electrochim. Acta. https://doi.org/10.1016/j.electacta.2023.143723 (2024).
S. Khademzadeh, Prog. Addit. Manuf. (2021).
A. Girotto M. Ballan P. Rebesan R. Dima A. Monetti I. Bodini D. Paderno V. Villa A. Pepato M. Manzolaro J. Phys. Conf. Ser. 10.1088/1742-6596/2687/8/082047
P. Rebesan M. Ballan M. Bonesso A. Campagnolo S. Corradetti R. Dima C. Gennari G.A. Longo S. Mancin M. Manzolaro et al. Addit. Manuf. 47 1:CAS:528:DC%2BB3MXitVyrsr7L 10.1016/j.addma.2021.102277 102277
C. Zitelli P. Folgarait A. Di Schino Metals 10.3390/met9070731
L. Wu S. Das W. Gridin S. Leuders M. Kahlert M. Vollmer T. Niendorf Adv. Eng. Mater. 10.1002/adem.202100049
L. Zai C. Zhang Y. Wang W. Guo D. Wellmann X. Tong Y. Tian Metals 10 1 25 1:CAS:528:DC%2BB3cXht1Kqtb%2FK 10.3390/met10020255
B. Mooney K.I. Kourousis Metals 10 1 22 1:CAS:528:DC%2BB3MXhslCrs7c%3D 10.3390/met10091273
A. Santana A. Eres-Castellanos J.A. Jimenez R. Rementeria C.G. Capdevila F. Caballero J. Mater. Res. Technol. 25 6898 6912 1:CAS:528:DC%2BB3sXhsFeisrnI 10.1016/j.jmrt.2023.07.114
A. Yazdanpanah M. Franceschi G. Bergamo M. Bonesso M. Dabalà Eng. Fail. Anal. 10.1016/j.engfailanal.2022.106192
F. Deirmina N. Peghini B. AlMangour D. Grzesiak M. Pellizzari Mater. Sci. Eng. A 753 109 121 1:CAS:528:DC%2BC1MXltVSnur4%3D 10.1016/j.msea.2019.03.027
C. Lesch N. Kwiaton F.B. Klose Steel Res. Int. 88 1 21 1:CAS:528:DC%2BC2sXhtlyiu7fK 10.1002/srin.201700210
D. Raabe, et al. Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 51, 5517–5586, https://doi.org/10.1007/s11661-020-05947-2 (2020).
J. Zhao Z. Jiang Prog. Mater. Sci. 94 174 242 1:CAS:528:DC%2BC1cXis1agsLY%3D 10.1016/j.pmatsci.2018.01.006
B.C. De Cooman Y. Estrin S.K. Kim Twinning-induced plasticity (TWIP) steels Acta Mater. 142 283 362 1:CAS:528:DC%2BC2sXht1Ols7zL 10.1016/j.actamat.2017.06.046
W. Zhang J. Xu Mater. Des. 221 1:CAS:528:DC%2BB38XitlCrt7zE 10.1016/j.matdes.2022.110994 110994
C. García-Mateo F.G. Caballero H.K.D.H. Bhadeshia Mater. Sci. Forum 500 495 502 10.4028/www.scientific.net/msf.500-501.495
C. Garcia-Mateo F.G. Caballero H.K.D.H. Bhadeshia J. Phys. IV Fr. 112 255 288 10.1051/jp4
C. Garcia-Mateo T. Sourmail F.G. Caballero V. Smanio M. Kuntz C. Ziegler A. Leiro E. Vuorinen R. Elvira T. Teeri Mater. Sci. Technol. 30 1071 1078 1:CAS:528:DC%2BC2cXoslyhtb8%3D 10.1179/1743284713Y.0000000428
L. Morales-Rivas C. Garcia-Mateo T. Sourmail M. Kuntz R. Rementeria F.G. Caballero Metals 10.3390/met6120302
H.K.D.H. Bhadeshia, Bainite in steels: theory and practice; maney publishing, vol. 19; ISBN 9781909662742 (2006).
M. Franceschi C. Soffritti A. Fortini L. Pezzato G.L. Garagnani M. Dabalà Tribol. Int. 10.1016/j.triboint.2022.108071
M. Franceschi, A. Miotti Bettanini, L. Pezzato, M. Dabalà, and P.J. Jacques. Metals. https://doi.org/10.3390/met11122055 (2021).
M. Franceschi R. Bertolini A. Fabrizi M. Dabalà L. Pezzato Mater. Sci. Eng. A 10.1016/j.msea.2022.144553
A. Królicka A.M. Żak F.G. Caballero Mater. Des. 10.1016/j.matdes.2021.110143
K.S. Kim Y.K. Kim K.A. Lee Addit. Manuf. 60 1:CAS:528:DC%2BB38XivV2ht7%2FL 10.1016/j.addma.2022.103262 103262
M. Franceschi A. Yazdanpanah D. Leone L. Pezzato M. Dabalà Metals 10.3390/met14010113
A. Królicka J. Malawska Materials 10.3390/ma17194699 39410271 11478015
L. Caprio A.G. Demir G. Chiari B. Previtali J. Phys. Photonics 10.1088/2515-7647/ab7080
M. Franceschi L. Morales-Rivas E. Cordova-Tapia J.A. Jimenez M. Dabalà C. Garcia-Mateo J. Mater. Res. Technol. 32 2931 2944 1:CAS:528:DC%2BB2cXhvVCnurjO 10.1016/j.jmrt.2024.08.141
M. Franceschi, L. Pezzato, C. Gennari, D. Hanoz, R. Bertolini, A. Fabrizi, M. Polyakova, K. Brunelli, F. Bonollo, and M. Dabalà, Influence of Austempering temperature on microstructure and mechanical properties of high silicon carbide free Bainitic steel. Steel Res. Int. (2023).
Corporation, O. Origin(Pro) (2022).
L. Lutterotti Acta Crystallogr. Sect. A Found. Crystallogr. 56 s54 s54 10.1107/s0108767300021954
N. Ahmed I. Barsoum G. Haidemenopoulos R.K.A. Al-Rub J. Manuf. Process. 75 415 434 10.1016/j.jmapro.2021.12.064
K. Sun W. Peng L. Yang L. Fang Metals 10.3390/met10020292
U. Scipioni Bertoli G. Guss S. Wu M.J. Matthews J.M. Schoenung Mater. Des. 135 385 396 1:CAS:528:DC%2BC2sXhsFyltrfF 10.1016/j.matdes.2017.09.044
Q. Shi D. Gu M. Xia S. Cao T. Rong Opt. Laser Technol. 84 9 22 1:CAS:528:DC%2BC28XmsFyhur8%3D 10.1016/j.optlastec.2016.04.009
J. Platl S. Bodner C. Hofer A. Landefeld H. Leitner C. Turk M.A. Nielsen A.G. Demir B. Previtali J. Keckes et al. Acta Mater. 225 1:CAS:528:DC%2BB38XisFSntA%3D%3D 10.1016/j.actamat.2021.117570 117570
C. García de Andrés F.G. Caballero C. Capdevila L.F. Álvarez Mater. Charact. 48 101 111 10.1016/S1044-5803(02)00259-0
C. Chen S. Chang J. Zhu Z. Xiao H. Zhu X. Zeng J. Manuf. Process. 59 621 628 10.1016/j.jmapro.2020.10.009
M. Franceschi L. Pezzato C. Gennari A. Fabrizi M. Polyakova D. Konstantinov K. Brunelli M. Dabalà M. Dabal Metals 10 1 19 1:CAS:528:DC%2BB3MXksFymu78%3D 10.3390/met10111448
D. Kotzem T. Arold T. Niendorf F. Walther Mater. Sci. Eng. A 772 1:CAS:528:DC%2BC1MXisVSksbzO 10.1016/j.msea.2019.138785 138785
Z.C. Oter Y. Gencer M. Tarakci Optik (Stuttg) 202 1:CAS:528:DC%2BC1MXitVylsbnJ 10.1016/j.ijleo.2019.163568 163568
B. Ferrar L. Mullen E. Jones R. Stamp C.J. Sutcliffe J. Mater. Process. Technol. 212 355 364 10.1016/j.jmatprotec.2011.09.020
Z. Chen X. Wu D. Tomus C.H.J. Davies Addit. Manuf. 21 91 103 1:CAS:528:DC%2BC1cXpsFOnsLY%3D 10.1016/j.addma.2018.02.009
T.P. Moran D.H. Warner A. Soltani-Tehrani N. Shamsaei N. Phan Addit. Manuf. 47 1:CAS:528:DC%2BB3MXit1als73P 10.1016/j.addma.2021.102333 102333
J. Boes A. Röttger C. Mutke C. Escher W. Theisen Addit. Manuf. 23 170 180 1:CAS:528:DC%2BC1cXitlWnsL7P 10.1016/j.addma.2018.08.005
K. Kempen B. Vrancken S. Buls L. Thijs J. Van Humbeeck J.P. Kruth J. Manuf. Sci. Eng. 136 1 7 10.1115/1.4028513
L. Zhou J. Sun J. Chen W. Chen Y. Ren Y. Niu C. Li W. Qiu J. Alloys Compd. 928 1:CAS:528:DC%2BB38Xitlyrtr3N 10.1016/j.jallcom.2022.167130 167130
J.H. Park G.B. Bang K.A. Lee Y. Son Y.H. Song B.S. Lee W.R. Kim H.G. Kim Met. Mater. Int. 28 2836 2848 1:CAS:528:DC%2BB38XhsVKitLzI 10.1007/s12540-022-01169-w
L. Cordova T. Bor M. de Smit M. Campos T. Tinga Addit. Manuf. 32 1:CAS:528:DC%2BB3cXns1ajtbw%3D 10.1016/j.addma.2020.101082 101082
L. Cheng A. Bottger T.H. de Keijser E.J. Mittemeijer Scr. Metall. Mater. 24 509 514 1:CAS:528:DyaK3cXhs1aktrw%3D
R. Rementeria J.D. Poplawsky M.M. Aranda W. Guo J.A. Jimenez C. Garcia-Mateo F.G. Caballero Acta Mater. 125 359 368 1:CAS:528:DC%2BC28XitFWnurbI 10.1016/j.actamat.2016.12.013