Influence of synthesis methods with low annealing temperature on the structural and magnetic properties of CoFe2O4 nanopowders for permanent magnet application

Abraime, B.; El Maalam, Khadija; Fkhar, L.; Mahmoud, Abdelfattah; Boschini, Frédéric; Tamerd, M. Ait; Benyoussef, Abdelillah Ilah; Hamedoun, Mohammed; Hlil, Elkebir; Ait Ali, Mustapha; El Kenz, Abdallah; Mounkachi, Omar

doi:10.1016/j.jmmm.2020.166416

Article (Scientific journals)

Influence of synthesis methods with low annealing temperature on the structural and magnetic properties of CoFe2O4 nanopowders for permanent magnet application

Abraime, B.; El Maalam, Khadija; Fkhar, L. et al.

2020 • In Journal of Magnetism and Magnetic Materials, 500, p. 166416

Peer Reviewed verified by ORBi

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https://hdl.handle.net/2268/243172

DOI
10.1016/j.jmmm.2020.166416

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Keywords :

Cobalt ferrite; Maximum energy product; Permanent magnet; Synthesis methods

Abstract :

[en] Cobalt ferrite nanopowders were prepared with low annealing temperatures (400 °C and 600 °C) using four different synthesis methods: co-precipitation, sol-gel, sol-gel autocombustion and microemulsion. The pure phase is obtained in all the samples and confirmed using the XRD diffraction. The crystallite size is calculated based on the XRD patterns and ranged between ~9 nm and ~26 nm. The SEM micrographs show an agglomeration with an increase of grain size between 400 °C and 600 °C samples for all the used methods. The magnetic properties are given. The best obtained values are MS = 80,319 emu/g, HC = 2057,97 Oe and (BH)max = 0.3313 MGOe for co-precipitation, sol-gel and sol-gel autocombustion, respectively. An improvement of 89% in (BH)max value is observed in the case of sol-gel auto-combustion when we go from 400 °C to 600 °C.

Research Center/Unit :

GreenMat

Disciplines :

Physics

Author, co-author :

Abraime, B.

El Maalam, Khadija

Fkhar, L.

Mahmoud, Abdelfattah ; Université de Liège - ULiège > Département de chimie (sciences) > LCIS - GreenMAT

Boschini, Frédéric ; Université de Liège - ULiège > Plateforme APTIS

Tamerd, M. Ait

Benyoussef, Abdelillah Ilah

Hamedoun, Mohammed

Hlil, Elkebir

Ait Ali, Mustapha

El Kenz, Abdallah

Mounkachi, Omar

Language :

English

Title :

Influence of synthesis methods with low annealing temperature on the structural and magnetic properties of CoFe2O4 nanopowders for permanent magnet application

Publication date :

15 April 2020

Journal title :

Journal of Magnetism and Magnetic Materials

ISSN :

0304-8853

eISSN :

1873-4766

Publisher :

Elsevier, Amsterdam, Netherlands

Volume :

500

Pages :

166416

Peer reviewed :

Peer Reviewed verified by ORBi

Additional URL :

http://www.sciencedirect.com/science/article/pii/S0304885319339836

Funders :

Walloon region

Available on ORBi :

since 15 January 2020

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