Bonding to CAD-CAM Composites: An Interfacial Fracture Toughness Approach

[en] The objective of this study was to evaluate the interfacial fracture toughness (IFT) of composite cement with dispersed filler (DF) versus polymer-infiltrated ceramic network (PICN) computer-aided design and computer-aided manufacturing (CAD-CAM) composite blocks after 2 different surface pretreatments using the notchless triangular prism (NTP) test. Two DFs (Cerasmart [CRT] and Lava Ultimate [LVA]), 2 PICNs (Enamic [ENA] and experimental PICN [EXP]), and e.max CAD lithium disilicate glass-ceramic (EMX, control) prism samples were bonded to their counterparts with Variolink Esthetic DC composite cement after either hydrofluoric acid etching (HF) or gritblasting (GR). Both procedures were followed by silanization. All samples (n = 30 per group) were thermocycled (10,000 cycles) and tested for their IFT in a water bath at 36°C. Moreover, representative samples from each group were subjected to a developed interfacial area ratio (Sdr) measurement by profilometry and scanning electron microscopy (SEM) characterization. EXP-HF gave the highest IFT (1.85 ± 0.39 MPa·m1/2), followed by EMX-HF and ENA-HF, while CRT-HF gave the lowest (0.15 ± 0.22 MPa·m1/2). PICNs gave significantly better results with HF, and DF showed better results with GR. A 2-way analysis of variance indicated that there were significantly higher IFT and Sdr for PICNs than for DF. A positive correlation (r2 = 0.872) was found between IFT and Sdr. SEM characterization showed the specific microstructure of the surface of etched PICNs, indicating the presence of a retentive polymerbased honeycomb structure. Etching of the typical double-network microstructure of PICNs causes an important increase in the Sdr and IFT, while DF should be gritblasted. DF exhibited significantly lower Sdr and IFT values than PICNs. The present results show the important influence of the material class and surface texture, and consequently the micromechanical bond, on the adhesive interface performance of CAD-CAM composites

Research Center/Unit :

d‐BRU - Dental Biomaterials Research Unit - ULiège

Disciplines :

Dentistry & oral medicine

Author, co-author :

Eldafrawy, Maher ; Université de Liège - ULiège > Doct. sc. dent. (paysage)

Ebroin, Marie ; Université de Liège - ULiège > Département des sciences cliniques > Labo de biologie des tumeurs et du développement

Gailly, Patrick ; Université de Liège - ULiège > CSL (Centre Spatial de Liège)

Nguyen, Jean-Francois

Sadoun, Michael

Mainjot, Amélie ; Université de Liège - ULiège > Département de sciences dentaires > Biomatériaux dentaires

Language :

English

Title :

Bonding to CAD-CAM Composites: An Interfacial Fracture Toughness Approach

Publication date :

2018

Journal title :

Journal of Dental Research

ISSN :

0022-0345

eISSN :

1544-0591

Publisher :

International & American Associations for Dental Research, Alexandria, United States - Virginia

Peer reviewed :

Peer Reviewed verified by ORBi

Available on ORBi :

since 22 September 2017

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