Optimization of settling behavior for an efficient solvent-extraction process for bio-based components

Bednarz, Andreas; Scherübel, Peter; Spieß, Antje C.; Pfennig, Andreas

doi:10.1002/ceat.201700020

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Article (Scientific journals)

Optimization of settling behavior for an efficient solvent-extraction process for bio-based components

Bednarz, Andreas; Scherübel, Peter; Spieß, Antje C. et al.

2017 • In Chemical Engineering and Technology, 40 (10), p. 1852-1860

Peer Reviewed verified by ORBi

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https://hdl.handle.net/2268/212546

DOI
10.1002/ceat.201700020

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Bednarz Scherübel Spieß Pfennig 2017 Optimization of Settling Behavior for an Efficient Solvent-Extraction Process for Biobased Components.pdf

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Keywords :

Biocompatibility; coalescence; phase separation; extraction; fermentation media; settling tests; diamines

Abstract :

[en] Extraction is a downstream-process option in bio-based processes. Since the knowledge of phase-separation behavior is essential for designing efficient separation processes, this study investigates the settling and coalescence behavior of bio-based extraction systems using a standard lab-scale settling cell. The influence of different buffer media as well as of E. coli cells on coalescence was determined for the reactive extraction of hexane-1.6-diamine with isostearic acid and D2EHPA using kerosene and oleyl alcohol as diluents. As a result, an increasing pH value of the buffer significantly increases settling time. The presence of E. coli cells hinders the phase separation of the investigated systems, in particular with dispersed organic phases.

Research Center/Unit :

PEPs, Products, Environment, and Processes, Department of Chemical Engineering

Disciplines :

Chemical engineering

Author, co-author :

Bednarz, Andreas

Scherübel, Peter

Spieß, Antje C.

Pfennig, Andreas ; Université de Liège > Department of Chemical Engineering > PEPs - Products, Environment, and Processes

Language :

English

Title :

Optimization of settling behavior for an efficient solvent-extraction process for bio-based components

Publication date :

2017

Journal title :

Chemical Engineering and Technology

ISSN :

0930-7516

eISSN :

1521-4125

Publisher :

Wiley, New York, United States - New York

Volume :

Issue :

Pages :

1852-1860

Peer reviewed :

Peer Reviewed verified by ORBi

Additional URL :

http://onlinelibrary.wiley.com/doi/10.1002/ceat.201700020/full

Available on ORBi :

since 03 July 2017

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