Applications Of Chromatographic And Spectrometric Techniques To The Study Of Dexamethasone Related-Compounds

Gaignage, P.; Lognay, Georges; Marlier, M.; Severin, M.; Dreze, P.

doi:10.1007/BF02260691

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Article (Scientific journals)

Applications Of Chromatographic And Spectrometric Techniques To The Study Of Dexamethasone Related-Compounds

Gaignage, P.; Lognay, Georges; Marlier, M. et al.

1989 • In Chromatographia, 28 (11-12), p. 623-630

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https://hdl.handle.net/2268/185903

DOI
10.1007/BF02260691

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Keywords :

Thin-layer chromatography; Column liquid chromatography; Dexamethasone related compounds; Mass spectrometry; Illicit drug formulations

Abstract :

[en] A methodology for the analysis of dexamethasone and related compounds is proposed. Nine corticoids (corticosteroids) have been separated by TLC and by normalphase HPLC. The optimization of the HPLC separation is performed on a diol column and with a n-hexane/isopropanol (80:20) mobile phase. Mass spectrometry is used to elucidate the nature of the compounds isolated from illicit drug formulations and to confirm the structure of synthesised derivatives from the parent dexamethasone.

Disciplines :

Chemistry

Author, co-author :

Gaignage, P.

Lognay, Georges ; Université de Liège - ULiège > Gembloux Agro-Bio Tech

Marlier, M.

Severin, M.

Dreze, P.

Language :

English

Title :

Applications Of Chromatographic And Spectrometric Techniques To The Study Of Dexamethasone Related-Compounds

Publication date :

December 1989

Journal title :

Chromatographia

ISSN :

0009-5893

eISSN :

1612-1112

Publisher :

Elsevier, Netherlands

Volume :

Issue :

11-12

Pages :

623-630
623-630

Peer reviewed :

Peer Reviewed verified by ORBi

Additional URL :

http://www.springer.com/chemistry/analytical+chemistry/journal/10337

Available on ORBi :

since 14 September 2015

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Bibliography

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