Ferrara, D., Albendea, P., & Purcaro, G. (19 September 2024). Comparison of microwave-assisted saponification and extraction methods for MOH determination in meat [Poster presentation]. 3rd European Sample Preparation Conference (EuSP2024) and the 2nd Green and Sustainable Analytical Chemistry Conference (GSAC2024), Chania, Greece. |
Ferrara, D., Beccaria, M., Chiara Cordero, & Purcaro, G. (2024). Advantages of the use of Microwave-assisted technology for lipid analysis. In D. Ferrara, M. Beccaria, Cordero Chiara, ... G. Purcaro, Book of Abstracts – 3rd European Sample Preparation Conference and 2nd Green and Sustainable Analytical Chemistry Conference. Chania, Greece: 3rd European Sample Preparation Conference (EuSP2024) and the 2nd Green and Sustainable Analytical Chemistry Conference (GSAC2024). |
Eggermont, D., Pardi Francesca, & Purcaro, G. (2024). Vacuum-Assisted SPME-GC×GC-MS for Accurate 5-HMF Determination and Volatile Profiling of Honey. In Elefteria Psillakis, Book of Abstracts – 3rd European Sample Preparation Conference and 2nd Green and Sustainable Analytical Chemistry ConferenceBook of abstract. Greece: Elefteria Psillakis. |
Purcaro, G. (2024). Sample Preparation and GC×GC: Fundamental Allies to Unravel MOSH and MOAH Contamination. In Book of abstract: the 3rd European Sample Preparation Conference (EuSP2024) and the 2nd Green and Sustainable Analytical Chemistry Conference (GSAC2024). Chania, Greece: the 3rd European Sample Preparation Conference (EuSP2024) and the 2nd Green and Sustainable Analytical Chemistry Conference (GSAC2024). |
Schincaglia, A., Pasti, L., Cavazzini, A., Purcaro, G., & Beccaria, M. (2024). Optimization and Validation of a Cheaper, Safer, and More Sustainable Methodology for Aflatoxins Determination in Rich-Lipidic Matrices (Pistachio Nuts) Using Deep Eutectic Solvent Extraction and UHPLC-FLD Analysis. Journal of Agricultural and Food Chemistry. doi:10.1021/acs.jafc.4c05094 |
Gorska, A., Pierret, D., Bauwens, G., Albendea, P., & Purcaro, G. (2024). Multidimensional Gas Chromatography Techniques and Sameple Preparation: Crucial Aspects in Mineral Oil Hydrocarbons Routine Analysis. LCGC international. |
Schincaglia, A., Franchina, F. A., Cavazzini, A., Purcaro, G., & Beccaria, M. (26 August 2024). Sustainability in Food Safety: Deep Eutectic Solvents for Aflatoxin Extraction in Pistachios [Poster presentation]. XXVIII Congresso Nazionale della Società Chimica Italiana, Milan, Italy. |
Farková, V., Křížová, L., Dadáková, K., Farka, Z., Mascrez, S., Eggermont, D., Purcaro, G., & Kašparovský, T. (August 2024). Changes in the fatty acid profiles and health indexes of bovine colostrum during the first days of lactation and their impact on human health. Food Chemistry, 448, 139042. doi:10.1016/j.foodchem.2024.139042 |
Ferrara, D., Beccaria, M., Cordero, C. E., & Purcaro, G. (August 2024). Comprehensive comparison of fatty acid methyl ester profile in different food matrices using microwave-assisted extraction and derivatization methods and comprehensive two-dimensional gas chromatography coupled with flame ionization detection. Advances in Sample Preparation, 11, 100124. doi:10.1016/j.sampre.2024.100124 |
Lazzari, E., Mase, C., Dayton, D. C., Marceau, S., Purcaro, G., Focant, J.-F., Piparo, M., & Giusti, P. (August 2024). Exploring molecular composition of upgraded pyrolysis bio-oil using GC×GC-(EI/PI)-TOF MS with different column set-ups. Journal of Analytical and Applied Pyrolysis, 181, 106569. doi:10.1016/j.jaap.2024.106569 |
Kouassi, K. A., Alabi, T., Purcaro, G., Blecker, C., & Danthine, S. (31 July 2024). Assessment of the Impact of Annual Growing Conditions on the Physicochemical Properties of Mango Kernel Fat. Horticulturae, 10 (8), 814. doi:10.3390/horticulturae10080814 |
Schincaglia, A., Pasti, L., Cavazzini, A., Purcaro, G., & Beccaria, M. (31 July 2024). Optimization of headspace high-capacity tool coupled to two-dimensional gas chromatography–mass spectrometry for mapping the volatile organic compounds of raw pistachios. A proof-of-concept on the classification ability by geographic origin. Food Chemistry, 460, 140702. doi:10.1016/j.foodchem.2024.140702 |
Bauwens, G., & Purcaro, G. (11 July 2024). Improved microwave-assisted saponification to reduce the variability of MOAH determination in edible oils. Analytica Chimica Acta, 1312, 342788. doi:10.1016/j.aca.2024.342788 |
Gorska, A., Danthine, S., Jacquet, N., & Purcaro, G. (2024). Impact of deodorisation time and temperature on the removal of different MOAH structures: a lab-scale study on spiked coconut oil. Food Additives and Contaminants. Part A. Chemistry, Analysis, Control, Exposure and Risk Assessment, 1 - 14. doi:10.1080/19440049.2024.2371925 |
Purcaro, G. (31 May 2024). LC-GC×GC: A POWERFUL HYPHENATED TECHNIQUE TO ENHANCE CHROMATOGRAPHIC SEPARATION AND SIMPLIFY SAMPLE PREPARATION FOR ROUTINE APPLICATIONS [Paper presentation]. 18th International Symposium onHyphenated Techniques inChromatography and Separationtechnology (HTC), Leuven, Belgium. |
Beccaria, M., Schincaglia, A., Cavazzini, A., & Purcaro, G. (06 May 2024). Extraction and determination of aflatoxins in rich-lipidic matrices using deep eutectic solvent as the extraction medium and UHPLC-FLD analysis [Paper presentation]. 2024 AOCS Annual Meeting & Expo, Montreal, Canada. |
Danthine, S., Karra, S., Vionne, A., Filocco, S., Mascrez, S., Purcaro, G., & Gibon, V. (May 2024). Impact of experimental conditions on DAK formation during interesterification [Poster presentation]. AOCS Annual meeting and expo, Montréal, Canada. |
Gorska, A., Bauwens, G., & Purcaro, G. (May 2024). Reducing the variability of the saponification step for MOSH&MOAH analysis using microwave-assisted extraction [Poster presentation]. AOCS Annual Meeting & Expo 2024, Montréal, Canada. |
Gorska, A., Bauwens, G., & Purcaro, G. (01 May 2024). New strategy for removing biogenic interferences from mineral oil aromatic hydrocarbons in vegetable oils [Paper presentation]. AOCS Annual Meeting & Expo 2024, Montréal, Canada. |
Kouassi, K. A., Blecker, C., Purcaro, G., Alabi, T., & Danthine, S. (01 May 2024). Potentialities of Ivorian mango (Mangifera indica. L) kernel fat fractions produced by solvent fractionation [Poster presentation]. 2024 AOCS Annual Meeting & Expo, Montréal, Québec, Canada. |
Schincaglia, A., Flavio Antonio Franchinca, Alberto Cavazzini, Purcaro, G., & Beccaria, M. (May 2024). Aflatoxin determination in food: a greener DES-based extraction followed by SPE-UHPLC-FLD analysis [Paper presentation]. 18th International Symposium on Hyphenated Techniques in Chromatography and Separation Technology (HTC-18), Leuven, Belgium. |
Schincaglia, A., Franchina Flavio Antonio, Cavazzini Alberto, Purcaro, G., & Beccaria, M. (May 2024). In-depth analysis of pistachio aroma compounds utilizing high-capacity concentration tools coupled with GC×GC-MS [Poster presentation]. 18th International Symposium on Hyphenated Techniques in Chromatography and Separation Technology (HTC-18), Leuven, Belgium. |
Ferrara, D., & Purcaro, G. (30 April 2024). Microwave-assisted processes for Fatty Acids Methyl Esters analysis in food matrix: A comparative study [Paper presentation]. AOCS annual meeting & expo 2024, Montréal, Canada. |
Mascrez, S., Purcaro, G., & Ferrara, D. (Other coll.). (29 April 2024). Vacuum-assisted and multi-cumulative trapping coupled with GC×GC for highly informative virgin olive oil volatile profiling [Poster presentation]. AOCS annual meeting & expo 2024, Montréal, Canada. |
Purcaro, G. (29 April 2024). MOSH & MOAH IN FOOD: STATE-OF-THE-ART AND RECENT ADVANCEMENTS [Paper presentation]. 2024 AOCS Annual Meeting & Expo, Montreal, Canada. |
Ferrara, D., Cescon, M., Giacoppo, G., Costa, V., Purcaro, G., Spadafora, N. D., Cordero, C., Pasti, L., Cavazzini, A., & Beccaria, M. (01 April 2024). Composition and nutritional values of fatty acids in marine organisms by one-step microwave-assisted extraction/derivatization and comprehensive two-dimensional gas chromatography -flame ionization detector. Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences, 1236, 124074. doi:10.1016/j.jchromb.2024.124074 |
Wang, J., Yang, P., Liu, J., Yang, W., Qiang, Y., Jia:, W., Han, D., Zhang, C., Purcaro, G., & Fauconnier, M.-L. (30 March 2024). Study of the flavor dissipation mechanism of soy-sauce-marinated beef using flavor matrices. Food Chemistry, 437 (1), 137890. doi:10.1016/j.foodchem.2023.137890 |
Mascrez, S., Aspromonte, J., Spadafora, N. D., & Purcaro, G. (12 January 2024). Vacuum-assisted and multi-cumulative trapping in headspace solid-phase microextraction combined with comprehensive multidimensional chromatography-mass spectrometry for profiling virgin olive oil aroma. Food Chemistry, 442, 138409. doi:10.1016/j.foodchem.2024.138409 |
Ferrara, D., Beccaria Marco, & Purcaro, G. (2024). Comparative evaluation of Microwave-assisted processes for fatty acid methyl esters analysis in food matrices [Poster presentation]. 18th International Symposium on hyphenated techniquest in chromatography and separation technology. |
Ferrara, D., Cescon Mirco, Giacoppo Giulia, Costa Valentina, Purcaro, G., Spadafora Natasha Damiana, Cordero chiara, Pasti Luisa, Cavazzini Alberto, & Beccaria, M. (2024). One-step microwave-assisted extraction and derivatization for the evaluation of fatty acid methyl esters composition in marine organisms and their nutritional value [Poster presentation]. AOCS annual meeting & expo 2024, Montréal, Canada. |
Kouassi, K. A., Alabi, T., Cissé, M., Purcaro, G., Moret, S., Moret, E., Blecker, C., & Danthine, S. (2024). Assessment of composition, color, and oxidative stability of mango (Mangifera indica L.) kernel fats from various Ivorian varieties. Journal of the American Oil Chemists' Society. doi:10.1002/aocs.12758 |
Kouassi, K. A., Alabi, T., N’guessan, E. A., Purcaro, G., Moret, S., Cissé, M., Blecker, C., & Danthine, S. (2024). Comparative study of thermal behavior of mango kernel fat from seven Ivorian varieties related to their chemical composition. European Food Research and Technology. doi:10.1007/s00217-024-04538-4 |
Kouassi, K. A., Alabi, T., Purcaro, G., Moret, E., Blecker, C., & Danthine, S. (2024). Thermal and structural behavior of mango (Mangifera indica L) kernel fat from three Ivorian varieties. Journal of the American Oil Chemists' Society, 101 (1), 67 - 78. doi:10.1002/aocs.12781 |
Piparo M, Mase, C., Purcaro, G., Dayton, D., Lazzari, E., Focant, J.-F., & Giusti, P. (2024). Exploring molecular composition of upgraded pyrolysis bio-oil by using GC×GC-(EI/PI)-TOF MS [Paper presentation]. HTC-18. |
Di Mario, M., Bauwens, G., Peltier, F., Goscinny, S., Focant, J.-F., Purcaro, G., & Van Hoeck, E. (30 November 2023). Investigation of potential migratables from paper and board food contact materials. Frontiers in Chemistry, 11. doi:10.3389/fchem.2023.1322811 |
Aspromonte, J., Mascrez, S., Eggermont, D., & Purcaro, G. (2023). Solid-phase microextraction coupled to comprehensive multidimensional gas chromatography for food analysis. Analytical and Bioanalytical Chemistry. doi:10.1007/s00216-023-05048-0 |
Lazzari, E., Piparo, M., Mase, C., Levacher, L., Stefanuto, P.-H., Purcaro, G., Focant, J.-F., & Giusti, P. (November 2023). Chemical elucidation of recycled plastic pyrolysis oils by means of GC×GC-PI-TOF-MS and GC-VUV. Journal of Analytical and Applied Pyrolysis, 176, 106224. doi:10.1016/j.jaap.2023.106224 |
Purcaro, G. (19 October 2023). Tackling the Challenge of MOSH and MOAH Analysis in Food using Advanced Chromatographic Technique [Paper presentation]. 19th Euro Fed Lipid Congress and Expo, Poznan, Poland. |
Bauwens, G., & Purcaro, G. (18 September 2023). Evaluation of a new microwave assisted saponification/extraction method for mineral oil analysis in food [Poster presentation]. 19th Euro Fed Lipid congress and expo, Poznan, Poland. |
Danthine, S., Vionne, A., Filocco, S., Mascrez, S., Purcaro, G., & Gibon, V. (September 2023). Assessment of DAK formation during interesterification of edible oils and fats [Poster presentation]. EuroFedLipid Congress, Poland. |
Ferrara, D., Beccaria, M., Cordero, C. E., & Purcaro, G. (2023). Microwave-assisted extraction in closed vessel in food analysis. Journal of Separation Science, 2300390. doi:10.1002/jssc.202300390 |
Bauwens, G., Gorska, A., & Purcaro, G. (02 August 2023). Towards the Use of Multidimensional Gas Chromatography Techniques in Routine Analysis: The Mineral Oil Case. LC GC North America, 41 (s5), 6-10. |
Gorska, A., Salgarella, N., Calaminici, R., Forte, E., Beccaria, M., & Purcaro, G. (02 August 2023). Impact of column temperature on triacylglycerol regioisomers separation in silver ion liquid chromatography using heptane-based mobile phases. Journal of Chromatography. A, 1702, 464095. doi:10.1016/j.chroma.2023.464095 |
Purcaro, G. (21 July 2023). Sample preparation and GC×GC a powerful marriage in food analysis [Paper presentation]. 25th International Symposium on Advances in Extraction Technologies (ExTech), Tenerife, Spain. |
Purcaro, G. (20 July 2023). Microwave-assisted sample preparation in food analysis: A highly valuable ally [Paper presentation]. 25th International Symposium on Advances in Extraction Technologies (ExTech), Tenerife, Spain. |
Bauwens, G., Ferrara, D., & Purcaro, G. (19 July 2023). Improvement of the saponification process for mineral oil analysis using microwave assisted saponification/extraction [Poster presentation]. 25th International Symposium on Advances in Extraction Technologies (ExTech 2023), Tenerife, Spain. |
Ferrara, D., Fina Angelica, Chiara Emilia Cordero, & Purcaro, G. (19 July 2023). A new microwave-assisted extraction technology for the profiling of fatty acids in food matrices [Paper presentation]. 25th International Symposium on Advances in Extraction Technologies (ExTech 2023). |
Schincaglia, A., Purcaro, G., & Beccaria, M. (18 July 2023). Introducing an environmentally friendly method for detecting aflatoxins in pistachios: an innovative approach utilizing deep eutectic solvents [Poster presentation]. ExTech 2023, Tenerife, Spain. |
Qiao, Y., Chen, Q., Gou, M., Liu, Z., Purcaro, G., Jin, X., Wu, X., Lyu, J., & Bi, J. (July 2023). Elucidation of baking induced changes in key odorants of Red Jujube (Ziziphus jujuba Mill. cv.‘Junzao’). Journal of Food Composition and Analysis, 120, 105320. doi:10.1016/j.jfca.2023.105320 |
Schincaglia, A., Purcaro, G., & Beccaria, M. (29 June 2023). To a greener way in aflatoxins determination: a deep eutectic solvent–based approach [Paper presentation]. Advances in Separation Science, Gembloux, Belgium. |
Bauwens, G., & Purcaro, G. (28 June 2023). Exploration of the saponification conditions for mineral oil analysis through the utilization of microwave-assisted saponification/extraction [Poster presentation]. 2nd ADVANCES IN SEPARATION SCIENCE From Extraction to Chromatographic Applications, Gembloux, Belgium. |
Eggermont, D., Mascrez, S., & Purcaro, G. (28 June 2023). Potentialities of High-Capacity-Headspace-Extraction followed by GC×GC-qMS to better appreciate coffee brew note [Poster presentation]. 2nd ADVANCES IN SEPARATION SCIENCE: from extraction to chromatographic separation, Gembloux, Belgium. |
Mascrez, S., & Purcaro, G. (28 June 2023). Coupling vacuum assisted headspace and multi cumulative trapping SPME with GC × GC MS to enhance the chromatographic profiling [Paper presentation]. Advances in Separation Sciences 2nd Edition. |
Purcaro, G. (28 June 2023). The role of GC×GC in mineral oil analysis. Application of a complete LC-HC×GC-FID/ToFMS platform [Paper presentation]. 2nd Advances in Separation Science, Gembloux, Belgium. |
Schincaglia, A., Purcaro, G., & Beccaria, M. (28 June 2023). Unlocking the aroma compounds of pistachios using the power of multi-dimensional gas chromatography [Poster presentation]. Advances in Separation Science, Gembloux, Belgium. |
Schincaglia, A., Purcaro, G., & Beccaria, M. (31 May 2023). Multi-dimensional gas chromatography: a powerful tool to unwrap the aroma compounds of pistachios [Paper presentation]. Chimali 2023 - XIII Italian Food Chemistry Congress, Marsala, Italy. |
Spadafora, N. D., Eggermont, D., Křešťáková, V., Chenet, T., Van Rossum, F., & Purcaro, G. (10 May 2023). COMPREHENSIVE ANALYSIS OF FLORAL SCENT AND FATTY ACIDS IN NECTAR OF SILENE NUTANS THROUGH MODERN ANALYTICAL GAS CHROMATOGRAPHY TECHNIQUES. Journal of Chromatography. A, 1696, 463977. doi:10.1016/j.chroma.2023.463977 |
Bauwens, G.* , Gorska, A.* , & Purcaro, G. (2023). The role of comprehensive two-dimensional gas chromatography in mineral oil determination. Analytical and Bioanalytical Chemistry. doi:10.1007/s00216-023-04718-3 * These authors have contributed equally to this work. |
Danthine, S., Closset, S., Maes, J., Mascrez, S., Blecker, C., Purcaro, G., & Gibon, V. (03 May 2023). Enzymatic Interesterification to produce rapeseed oil-based zero-trans and dialkylketones-free fats [Paper presentation]. 2023 Annual Meeting & Expo, Denver, United States. |
Kouassi, K. A., Blecker, C., Purcaro, G., Moret, S., Alabi, T., & Danthine, S. (03 May 2023). Polymorphic Behaviour of three Ivorian Mango (Mangifera indica L) Kernel Fat varieties [Poster presentation]. 2023 AOCS Annual Meeting & Expo, Denver, United States. |
Purcaro, G., & Bauwens, G. (03 May 2023). MOSH AND MOAH IN FOOD: A LONG LASTING ANALYTICAL CHALLENGE [Paper presentation]. AOCS Annual Meeting, Denver, United States. |
Purcaro, G., Bauwens, G., & Gorska, A. (03 May 2023). LC GC × GC TOF MS/FID: A COMPREHENSIVE APPROACH TO TACKLE THE COMPLEXITY OF MINERAL OIL [Paper presentation]. AOCS Annual Meeting, Denver, United States. |
Eggermont, D., Spadafora, N. D., Aspromonte, J., Pellegrino, R., & Purcaro, G. (2023). Exploring different high-capacity tools and extraction modes to characterize the aroma of brewed coffee. Analytical and Bioanalytical Chemistry. doi:10.1007/s00216-023-04654-2 |
Bhatt, K., Beccaria, M., Zou, Y., Stefanuto, P.-H., Purcaro, G., Anna Luiza Mendes Siqueira, Adrien Maniquet, Marco Piparo, Pierre Giusti, & Focant, J.-F. (April 2023). In-depth characterization of complex molecules using GC×GC-TOFMS [Poster presentation]. European R&D Days, Brussels, Belgium. |
Mascrez, S., Eggermont, D., & Purcaro, G. (2023). SPME and Chromatographic Fingerprints in Food Analysis. In Evolution of Solid Phase Microextraction Technology. The Royal Society of Chemistry. doi:10.1039/bk9781839167300-00494 |
Purcaro, G. (20 March 2023). SPME-GC×GC a powerful tool in food analysis [Paper presentation]. Pittcon, Philadelphia, United States. |
Bauwens, G., Barp, L., & Purcaro, G. (March 2023). Validation of the liquid chromatography-comprehensive multidimensional gas chromatography-time-of-flight mass spectrometer/flame ionization detector platform for mineral oil analysis exploiting interlaboratory comparison data. Green Analytical Chemistry, 4, 100047. doi:10.1016/j.greeac.2022.100047 |
Eggermont, D., Mascrez, S., Spadafora, N. D., Aspromonte, J., & Purcaro, G. (01 February 2023). Exploring the cup of coffee using GC×GC-MS combined with multiple combination of headspace extractions [Paper presentation]. 14th Multidimensional Chromatography Workshop, Liège, Belgium. |
Mascrez, S., & Purcaro, G. (01 February 2023). Bursting the chromatographic fingerprint by combining vacuum assisted headspace, multi cumulative trapping SPME, and GC × GC [Paper presentation]. 14th Multidimensional Chromatography Workshop. |
Bauwens, G., Barp, L., & Purcaro, G. (31 January 2023). Validation of the LC-GC×GC–MS/FID platform for mineral oil analysis through the comparison with the result of interlaboratory trials [Poster presentation]. 14th multidimensional chromatographic workshop, Liege, Belgium. |
Schincaglia, A., Purcaro, G., & Beccaria, M. (31 January 2023). Chromatographic fingerprint of Pistacia vera fruits: an aromatic tour around the world [Paper presentation]. 14th Multidimensional Chromatography Workshop, Liège, Belgium. |
Purcaro, G. (30 January 2023). LC-GC×GC-TOF MS/FID: A POWERFUL MULTIDIMENSIONAL TECHNIQUE FOR AUTOMATED AND RELIABLE CHARACTERIZATION OF COMPLEX SAMPLES [Paper presentation]. Multidimensional Chromatography Workshop, Liege, Belgium. |
Schincaglia, A., Aspromonte, J., Franchina, F., Chenet, T., Pasti, L., Cavazzini, A., Purcaro, G., & Beccaria, M. (24 January 2023). Current Developments of Analytical Methodologies for Aflatoxins' Determination in Food during the Last Decade (2013-2022), with a Particular Focus on Nuts and Nut Products. Foods, 12 (3), 527. doi:10.3390/foods12030527 |
Beccaria, M., Piparo, M., Zou, Y., Stefanuto, P.-H., Purcaro, G., Mendes Siqueira, A. L., Maniquet, A., Giusti, P., & Focant, J.-F. (15 January 2023). Analysis of mixed plastic pyrolysis oil by comprehensive two-dimensional gas chromatography coupled with low- and high-resolution time-of-flight mass spectrometry with the support of soft ionization. Talanta, 252, 123799. doi:10.1016/j.talanta.2022.123799 |
Bauwens, G., Cavaco Soares, A., Lacoste, F., Ribera, D., Blomsma, C., Berg, I., Campos, F., Coenradie, A., Creanga, A., Zwagerman, R., & Purcaro, G. (2023). Investigation of the effect of refining on the presence of targeted mineral oil aromatic hydrocarbons in coconut oil. Food Additives and Contaminants. Part A. Chemistry, Analysis, Control, Exposure and Risk Assessment, 1 - 12. doi:10.1080/19440049.2022.2164621 |
Ferrara, D., Giacoppo, G., Beccaria, M., & Purcaro, G. (2023). Comparison of different extraction methods for the determination of fatty acid methyl esters in mussles samples [Poster presentation]. 2nd Advance in Separation Science, Gembloux, Belgium. |
Focant, J.-F., Lazzari, E., Beccaria, M., Piparo, M., Stefanuto, P.-H., Purcaro, G., Mendes Siqueira, A., Maniquet, A., & Giusti, P. (2023). Chemical investigation of plastic pyrolysis oils. In Sep proceedings. Paris, France: SEP. |
Franchina, F., Zanella, D., Henin, A., Mascrez, S., Stefanuto, P.-H., Purcaro, G., & Focant, J.-F. (2023). METHOD DEVELOPMENT AND OPTIMIZATION FOR MONITORING PROBE EXHALED BREATH METABOLITES USING PARALLEL MS-BASED ANALYTICAL PLATFORMS [Paper presentation]. 14th Multidimensional Chromatography Workshop. |
Lazzari, E., Piparo, P., Marceau, S., Purcaro, G., Focant, J.-F., & Giusti, P. (2023). QUALITATIVE SCREENING OF CATALYTIC PYROLYSIS WOOD-OIL BY MEANS OF GC×GC-TOFMS AND SOFT IONIZATION [Paper presentation]. 14th Multidimensional Chromatography Workshop. |
Eggermont, D., Spadafora, N. D., Aspromonte, J., & Purcaro, G. (08 December 2022). Unraveling the impact of the capsule material on the aroma of brewed coffee by headspace analysis using a HiSorb probe followed by reverse fill/flush flow modulation GC×GC-MS. Analytical and Bioanalytical Chemistry, 45, 2511-2521. doi:10.1007/s00216-022-04457-x |
Aspromonte, J., Lancioni, C., & Purcaro, G. (17 October 2022). Solid-Phase Microextraction—Gas Chromatography Analytical Strategies for Pesticide Analysis. Methods and Protocols, 5 (5), 82. doi:10.3390/mps5050082 |
Fina, A., Mascrez, S., Beccaria, M., De Luca, C., Aspromonte, J., Cordero, C., & Purcaro, G. (October 2022). A high throughput method for fatty acid profiling using simultaneous microwave-assisted extraction and derivatization followed by reversed fill/flush flow modulation comprehensive multidimensional gas chromatography. Advances in Sample Preparation, 4, 100039. doi:10.1016/j.sampre.2022.100039 |
Kouassi, K. A., Danthine, S., Alabi, T., Blecker, C. (Other coll.), Purcaro, G. (Other coll.), & Moret, S. (Other coll.). (26 September 2022). Triacylglycerol composition and Thermal Behavior of Mango (Mangifera indica L) Kernel Fat from Various Ivorian Varieties [Poster presentation]. Berlin Symposium on Structured Lipid Phases, Berlin, Germany. |
Bauwens, G., & Purcaro, G. (16 September 2022). STUDY OF COCONUT OIL SPIKED WITH NAPHTHALENES AND BENZO[A]PYRENES COMPOUNDS BEFORE AND AFTER REFINING BY LC-GC×GC–TOFMS/FID [Poster presentation]. ADVANCES IN SEPARATION SCIENCE from extraction to chromatographic applications 1st workshop, Gembloux, Belgium. |
Purcaro, G., Mascrez, S., & Eggermont, D. (16 September 2022). NOVEL APPROACH FOR VOLATILE PROFILING IN FOOD ANALYSIS [Paper presentation]. ADVANCES IN SEPARATION SCIENCE FROM EXTRACTION TO CHROMATOGRAPHIC APPLICATIONS. |
Barp, L., Moret, S., & Purcaro, G. (06 September 2022). Monitoring and Occurrence of Heavy PAHs in Pomace Oil Supply Chain Using a Double-Step Solid-Phase Purification and HPLC-FLD Determination. Foods, 11 (18), 2737. doi:10.3390/foods11182737 |
Křešťáková, V., Křížová, L., Mascrez, S., Eggermont, D., Purcaro, G., & Kašparovský, T. (06 September 2022). Changes in the Profile of Hypercholesterolemic Fatty Acids in Cow Colostrum During the First Days of Lactation [Poster presentation]. RAFA (RECENT ADVANCES IN FOOD ANALYSIS), Prague, Czechia. |
Purcaro, G., Mascrez, S., Bauwens, G., & Eggermont, D. (06 September 2022). ENHANCED FOOD SAFETY AND QUALITY ASSESSMENT THROUGH HYPHENATED AND AUTOMATED SAMPLE INTRODUCTION COUPLED TO GC×GC [Paper presentation]. RAFA_RECENT ADVANCES IN FOOD ANALYSIS, Prague, Czechia. |
Zanella, D., Henin, A., Mascrez, S., Stefanuto, P.-H., Franchina, F., Focant, J.-F., & Purcaro, G. (September 2022). Comprehensive two-dimensional gas chromatographic platforms comparison for exhaled breath metabolites analysis. Journal of Separation Science, 45 (18), 3542 - 3555. doi:10.1002/jssc.202200164 |
Spadafora, N. D., Mascrez, S., McGregor, L., & Purcaro, G. (30 July 2022). Exploring multiple-cumulative trapping solid-phase microextraction coupled to gas chromatography-mass spectrometry for quality and authenticity assessment of olive oil. Food Chemistry, 383, 132438. doi:10.1016/j.foodchem.2022.132438 |
Kouassi, K. A.* , Danthine, S.* , Blecker, C., Purcaro, G., ALABI TAOFIC* , & MORET Sabrina. (08 July 2022). Physicochemical and Thermal properties of Mango (Mangifera indica L) Seed Kernel Fats from Various Ivorian Varieties [Paper presentation]. 26th National Symposium For Applied Biological Sciences, Anvers, Belgium. * These authors have contributed equally to this work. |
Bauwens, G., Conchione, C., Sdrigotti, N., Moret, S., & Purcaro, G. (2022). Quantification and characterization of mineral oil in fish feed by liquid chromatography-gas chromatography-flame ionization detector and liquid chromatography-comprehensive multidimensional gas chromatography-time-of-flight mass spectrometer/flame ionization detector. Journal of Chromatography. A, 463208. doi:10.1016/j.chroma.2022.463208 |
Eggermont, D., Mascrez, S., & Purcaro, G. (31 May 2022). The Versatility Of HiSorb-GC×GC-qMS To Explore Brewed Coffee Volatiles [Poster presentation]. 19th International GC×GC Symposium. |
Purcaro, G., Eggermont, D., & Mascrez, S. (30 May 2022). Adding an extra dimension to GC×GC by tuning the sample introduction parameters [Paper presentation]. 19th International GC×GC Symposium, virtual, United States. |
Eggermont, D., Mascrez, S., & Purcaro, G. (19 May 2022). Comparison Of High Concentration Capacity Headspace Technique For Brewed Coffee Characterization Follow By GC×GC-MS [Poster presentation]. 17th International Symposium on Hyphenated Techniques in Chromatography and Separation Technology (HTC-17), Ghent, Belgium. |
Eggermont, D., Křešťáková, V., Mascrez, S., Spadafora, N., Van Rossum, F., & Purcaro, G. (17 May 2022). Comprehensive analysis of floral scent and fatty acids in nectar of Silene nutans through modern analytical gas chromatography techniques [Paper presentation]. Silene 2022. |
Giusti, P., Freije-Carrelo, L., Burnens, G., Piparo, M., Garcia-Bellido, J., Redondo-Velasco, M., Moldovan, M., Ruiz-Encinar, J., Bouyssiere, B., Lazzari, E., Focant, J.-F., Purcaro, G., Takamasa, S., Takechi, R., Hiraoka, T., & Miyagawa, H. (May 2022). GC and GC×GC based approaches for the molecular characterization of complex matrices related to alternative energy sources [Paper presentation]. 19th International GCxGC Symposium, Canada. |
Giusti, P., Freije-Carrelo, L., García-Bellido, J., Lazzari, E., Piparo, M., Burnens, G., Focant, J.-F., Purcaro, G., Moldovan, M., Takamas, S., Takeshi, R., Hiraoka, T., Miyagawa, H., Bouyssiere, B., & Ruiz-Encinar, J. (May 2022). GC and GC×GC based approaches for the molecular characterization of complex matrices related to alternative energy sources [Paper presentation]. Colloquium Spectroscopicum Internationale XLII (CSI XLII), Gijon, Spain. |
Qiao, Y., Bi, J., Chen, Q., Wu, X., Jin, X., Gou, M., Yang, X., & Purcaro, G. (May 2022). Rapid and sensitive quantitation of DDMP (2,3-dihydro-3,5-dihydroxy-6-methyl-4H-pyran-4-one) in baked red jujubes by HS-SPME-GC-MS/MS. Food Control, 135, 108820. doi:10.1016/j.foodcont.2022.108820 |
Purcaro, G., Eggermont, D., & Mascrez, S. (15 March 2022). High-Concentration Capacity Headspace Extraction Coupled with Comprehensive Multidimensional Gas Chromatography for Enhanced Chromatographic Fingerprint of Food [Paper presentation]. 2nd European Sample Preparation (EuSP2022) and 1st Green and Sustainable Analytical Chemistry (GSAC2022) e-conferences. |
Eggermont, D., Mascrez, S., & Purcaro, G. (14 March 2022). HS HCC Techniques In Combination With Multi Cumulative Trapping and GC × GC qMS Followed by Machine Learning to Explore the Impact Of Packaging On Coffee Brew Aroma [Poster presentation]. 2nd European Sample Preparation (EuSP2022) and 1st Green and Sustainable Analytical Chemistry (GSAC2022) e-conferences. |
Bauwens, G., & Purcaro, G. (01 February 2022). UTILISATION OF REVERSE COLUMN SET FOR MINERAL OIL QUANTIFICATION IN FOOD [Poster presentation]. 13th multidimensionnal chromatography workshop, On-line Liège, Belgium. |
Beccaria, M., Stefanuto, P.-H., Purcaro, G., & Franchina, F. (2022). The diagnostic purpose of odorant patterns for clinical applications using GC×GC. In C. E. I. Cordero (Ed.), Characterization of Odorant Patterns by Comprehensive Two-Dimensional Gas Chromatography (pp. 367-409). San Diego, United States - California: Elsevier. doi:10.1016/bs.coac.2021.11.004 |
Delbecque, N., Mascrez, S., Psillakis, E., & Purcaro, G. (01 February 2022). Sub-ambient temperature sampling of fish volatiles using vacuum-assisted headspace solid phase microextraction: Theoretical considerations and proof of concept. Analytica Chimica Acta, 1192, 339365. doi:10.1016/j.aca.2021.339365 |
Eggermont, D., Mascrez, S., & Purcaro, G. (01 February 2022). HISORB-GC×GC-QMS A POWERFUL MARRIAGE TO EXPLORE BREWED COFFEE VOLATILES [Poster presentation]. 13th Multidimensional Chromatography Workshop. |
Eggermont, D., Mascrez, S., Spadafora, N., Van Rossum, F., & Purcaro, G. (01 February 2022). EXPLORING THE SCENT OF SILENE BY TD-GC×GC-MS [Poster presentation]. 13th Multidimensional Chromatography Workshop. |
Qiao, Y., Chen, Q., Bi, J., Wu, X., Jin, X., Gou, M., Yang, X., & Purcaro, G. (31 January 2022). Investigation of the Volatile Profile of Red Jujube by Using GC-IMS, Multivariate Data Analysis, and Descriptive Sensory Analysis. Foods, 11 (3), 421. doi:10.3390/foods11030421 |
Bauwens, G., & Purcaro, G. (2022). Thoughtful optimization of microwave-assisted saponification and extraction of MOSH&MOAH in edible oil [Poster presentation]. 2022 AOCS Annual Meeting & Expo, Atlanta, United States - Georgia. |
Bauwens, G., & Purcaro, G. (2022). Elucidation of fish feed MOSH&MOAH contamination by LC-GC×GC-FID [Poster presentation]. 2nd European Sample Preparation e-Conference (EuSP2022) and the 1st Green and Sustainable Analytical Chemistry-Conference (GSAC2022). |
Beccaria, M., Zou, Y., Stefanuto, P.-H., Mendes Siqueria, A., Maniquet, A., Piparo, M., Giusti, P., Purcaro, G., & Focant, J.-F. (2022). Deeper investigation of oxygen-containing compounds in oleaginous feedstock (animal fat) by preparative column chromatography and comprehensive two-dimensional gas chromatography coupled with high-resolution time-of-flight mass spectrometry. Talanta, 238. doi:10.1016/j.talanta.2021.123019 |
Beccaria, M., Zou, Y., Stefanuto, P.-H., Mendes-Siquiera, A., Maniquet, A., Giusti, P., Pipro, M., Purcaro, G., & Focant, J.-F. (2022). Advanced analytical tools based on GC×GC-MS for the characterization of biomass and biofuel samples [Paper presentation]. HTC-17, Belgium. |
Beccaria, M., Zou, Y., Stefanuto, P.-H., Purcaro, G., Focant, J.-F., Piparo, M., Mendes Siqueira, A., Maniquet, A., & Giusti, P. (2022). ADVANCED ANALYTICAL TOOLS BASED ON GC×GC-MS FOR THE CHARACTERIZATION OF BIOMASS AND PLASTIC WASTE SAMPLES [Paper presentation]. 19th International GCxGC Symposium, Canada. |
Danthine, S., Closset, S., Maes, J., Mascrez, S., Blecker, C., Purcaro, G., & Gibon, V. (2022). Enzymatic interesterification to produce zero- trans and dialkylketones-free fats from rapeseed oil. Oilseeds and Fats, Crops and Lipids, 29 (7), 36. doi:10.1051/ocl/2022029 |
Eggermont, D., Mascrez, S., & Purcaro, G. (2022). HS-HCC Techniques In Combination With Multi Cumulative Trapping and GC×GC-qMS Followed by Machine Learning to Explore the Impact Of Packaging On Coffee Brew Aroma [Poster presentation]. 2nd European Sample Preparation e-Conference (EuSP2022) and the 1st Green and Sustainable Analytical Chemistry-Conference (GSAC2022). |
Franchina, F., & Purcaro, G. (2022). Sample preparation strategies for comprehensive volatile fingerprinting. In C. E. I. Cordero (Ed.), Characterization of Odorant Patterns by Comprehensive Two-Dimensional Gas Chromatography. Elsevier B.V. doi:10.1016/bs.coac.2022.02.001 |
Giusti P, Freije-Carrelo, L., Garcia-Bellido, J., Redondo-Velasco, M., Lazzari, E., Piparo, M., Burnens, G., Focant, J.-F., Purcaro, G., Moldovan, M., Suzuki, T., Ryo, T., Takaaki, H., Haruhiko, M., Bouyssiere, B., & Ruiz-Encinar, J. (2022). GC and GC×GC based approaches for the molecular characterization of complex matrices related to alternative energy sources [Poster presentation]. Analytics Nates 2022, Nantes, France. |
Glineur, A., Nott, K., Carbonelle, P., & Purcaro, G. (2022). Dual SPE purification, followed by offline derivatization and HPLC-ESI-MS/MS analysis for the quantification of estrogenic compounds at ultra-trace level: method development, validation, and screening of Belgian surface water [Poster presentation]. 2nd European Sample Preparation e-Conference (EuSP2022) and the 1st Green and Sustainable Analytical Chemistry e-Conference (GSAC2022). |
Lazzari, E., Beccaria, M., Zou, Y., Luiza Mendes Siqueira, A., Maniquet, A., Piparo, M., Giusti, P., Purcaro, G., Giri, A., Stefanuto, P.-H., & Focant, J.-F. (2022). Keynote Letcture-GC×GC-TOFMS to support the transition from fossil-based to bio-based energy sources [Paper presentation]. PEFTEC 2022, Rotterdam, Netherlands. |
Lazzari, E., Beccaria, M., Zou, Y., Mendes Siqueira, A., Maniquet, A., Piparo, M., Giusti, P., Purcaro, G., Giri, A., Stefanuto, P.-H., & Focant, J.-F. (2022). GC×GC-TOFMS to Support the Transition from Geological to Renewable Fuels [Paper presentation]. ADVANCES IN SEPARATION SCIENCE from extraction to chromatographic applications, Gembloux, Belgium. |
Lazzari, E., Beccaria, M., Zou, Y., Mendes Siqueira, A., Maniquet, A., Piparo, M., Giusti, P., Purcaro, G., Giri, A., Stefanuto, P.-H., & Focant, J.-F. (2022). GC×GC-TOFMS to Support the Transition from Fossil-based to Bio-based Energy Sources [Paper presentation]. PEFTEC 2022, Netherlands. |
Lazzari, E., Piparo, M., Purcaro, G., Focant, J.-F., & Giusti, P. (2022). Screening of pyrolysis oils from plastic by GC×GC-PI-TOFMS and GC-VUV [Paper presentation]. PEFTEC 2022, Netherlands. |
Mascrez, S., Fina, A., & Purcaro, G. (2022). Increase the throughput and reliability of fatty acid characterization in food by using a rapid single step microwave-assisted extraction and derivatization method followed by GC×GC-FID [Poster presentation]. 2022 AOCS Annual Meeting & Expo, Atlanta, United States - Georgia. |
Mascrez, S., Fina, A., & Purcaro, G. (2022). A rapid single step microwave-assisted extraction and derivatization method for the analysis of fatty acid in food by GC×GC-FID [Poster presentation]. 2nd European Sample Preparation e-Conference (EuSP2022) and the 1st Green and Sustainable Analytical Chemistry-Conference (GSAC2022). |
Mascrez, S., & Purcaro, G. (2022). Enhancing the olive oil fingerprint by combining vacuum-assisted and multi-cumulative trapping SPME [Poster presentation]. 19th International GC×GC Symposium, virtual, United States. |
Purcaro, G. (2022). Reverse fill/flush flow modulator in various GC×GC applications: a versatile tool to optimize your lab activities [Paper presentation]. International Day of Women and Girls in Science. |
Purcaro, G. (2022). LC-GC×GC-TOFMS/FID: a strategic tool to unravel the complexity of mineral oil contamination [Paper presentation]. Analytica. |
Purcaro, G., & Bauwens, G. (2022). LC-GC×GC-TOFMS/FID: extra dimensionality to untangle mineral oil contamination: a particular look into the MOAH fraction [Paper presentation]. 2022 AOCS Annual Meeting & Expo, Atlanta, United States. |
Purcaro, G., & Bauwens, G. (2022). A fully automated LC-GC×GC-TOF MS/FID platform for mosh and moah determination in food [Paper presentation]. 17th International Symposium on Hyphenated Techniques in Chromatography and Separation Technology (HTC&HTCS), Gent, Belgium. |
Agbohessou, P. S., Mandiki, S. N. M., Gougbédji, A., Megido, R. C., Lima, L.-M. W., Cornet, V., Lambert, J., Purcaro, G., Francis, F., Lalèyè, P. A., & Kestemont, P. (15 December 2021). Efficiency of fatty acid-enriched dipteran-based meal on husbandry, digestive activity and immunological responses of Nile tilapia Oreochromis niloticus juveniles. Aquaculture, 545, 737193. doi:10.1016/j.aquaculture.2021.737193 |
Mascrez, S., Eggermont, D., & Purcaro, G. (02 November 2021). Multiple-Cumulative Trapping: A Fascinating Option to Enhance Headspace Profile. LCGC Supplements, 39 (s11), 11-14. |
Bauwens, G., Conchione, C., Moret, S., & Purcaro, G. (21 October 2021). quantification and characterization of mineral oil in fish feed BY LC-GC-FID and LC-GC×GC-TOFMS/FID [Paper presentation]. 18th Euro Fed Lipid Congress and Expo (On-line Meeting). |
Bauwens, G., & Purcaro, G. (21 October 2021). MICROWAVE ASSISTED SAPONIFICATION FOLLOW BY LC-GC-FID AND LC-GC × GC TOFMS/FID FOR MOSH AND MOAH DETERMINATION IN DIFFERENT DRY SAMPLES [Poster presentation]. 18th Euro Fed Lipid Congress and Expo (On-line Meeting). |
Purcaro, G. (21 October 2021). Mineral Oil Contamination in Food: A Comprehensive Journey beyond the Hump [Paper presentation]. 18th Euro Fed Lipid Congress, virtual, Germany. |
Selecky, T., Losa, S., Panto, S., Bauwens, G., & Purcaro, G. (21 October 2021). FOOD CONTAMINATION WITH MINERAL OILS DETERMINED BY GC×GC-TOFMS/FID [Poster presentation]. 18th Euro Fed Lipid Congress and Expo (On-line Meeting). |
Purcaro, G. (14 October 2021). Hyphenated chromatographic techniques and miniaturized sample preparation: powerful tools for food quality, authenticity, and safety [Paper presentation]. Utilisation de techniques séparatives avancées pour la caractérisation d’échantillons complexes, Lyon, France. |
Purcaro, G., Spadafora, N., Mascrez, S., & McGregor, L. (October 2021). Multi-Cumulative Trapping HS-SPME-GC-MS in combination of with a novel data handling software for quality and geographical origin classification of virgin olive oil [Poster presentation]. 18th Euro Fed Lipid Congress. |
Glineur, A., Beccaria, M., & Purcaro, G. (30 August 2021). Exploring 20 eV electron impact ionization in gas chromatography-tandem mass spectrometry for the determination of estrogenic compounds. Journal of Chromatography. A, 1652, 462359. doi:10.1016/j.chroma.2021.462359 |
Beccaria, M., Franchina, F., Nasir, M., Mellors, T., Hill, J. E., & Purcaro, G. (29 July 2021). Investigating Bacterial Volatilome for the Classification and Identification of Mycobacterial Species by HS-SPME-GC-MS and Machine Learning. Molecules, 26 (15), 4600. doi:10.3390/molecules26154600 |
Bauwens, G., Conchione, C., Moret, S., & Purcaro, G. (02 July 2021). QUANTIFICATION AND CHARACTERIZATION OF MINERAL OIL IN FISH FEED BY LC-GC-FID AND LC-GC×GC-TOFMS/FID [Poster presentation]. EXTECH XXIII. |
Bauwens, G., & Purcaro, G. (02 July 2021). HYPHENATION AND MULTIDIMENSIONALITY AS SAMPLE PREPARATION ALLEYS IN MOSH AND MOAH ANALYSIS [Poster presentation]. EXTECH XXIII. |
Glineur, A., Nott, K., & Purcaro, G. (30 June 2021). Development and validation of methods using solid-phase extraction, offline derivatization and UHPLC-ESI(+)-MS/MS for the quantification of estrogenic compounds at ultra-trace levels in different types of water [Poster presentation]. Symposium on Advances in Extraction Technologies (Extech2021). |
Mascrez, S., Eggermont, D., & Purcaro, G. (June 2021). Exploring the capability of the HiSorb probe for characterization of volatile and semi-volatile compounds in brewed coffee by GCxGC-qMS [Poster presentation]. XXIII International Symposium on Advances in Extraction Technologies (Extech 2021). |
Mascrez, S., Psillakis, E., & Purcaro, G. (June 2021). Enhancing the volatile profile at sub-ambient temperature by using vacuum-assisted HS-SPME. Case study on fish spoilage [Poster presentation]. XXIII International Symposium on Advances in Extraction Technologies (Extech 2021). |
Purcaro, G. (June 2021). LC-GCxGC-ToFMS/FID platform for MOSH and MOAH determination: a quantitative and confirmative approach [Paper presentation]. Mineral Oil Contaminants in Food (Hybrid-Event). |
Purcaro, G., & Mascrez, S. (June 2021). Multi-cumulative trapping HS-SPME: a novel approach to enhance volatile fingerprinting [Paper presentation]. 23rd International Symposium on Advances in Extraction Technologies (Extech). |
Spadafora, N., Mascrez, S., McGregor, L., & Purcaro, G. (June 2021). Classification of olive oil and geographical origin by using a multi-cumulative trapping HS-SPME-GC-MS follow by a novel data handling software [Poster presentation]. XXIII International Symposium on Advances in Extraction Technologies (Extech 2021). |
Purcaro, G., & Beccaria, M. (21 May 2021). Advanced Analytical Techniques in Food Analysis. Journal of AOAC International, 104 (2), 251 - 252. doi:10.1093/jaoacint/qsaa159 |
Purcaro, G., Bauwens, G., Collard, M., & Panto, S. (11 May 2021). A fully integrated LC-GCxGC-ToFMS/FID platform for MOSH&MOAH determination in food. Qualitative and quantitative considerations [Paper presentation]. 2021 AOCS Annual Meeting & Expo. |
Mascrez, S., Danthine, S., & Purcaro, G. (May 2021). A rapid and efficient method for dialkyl ketones and sterols determination in fat [Poster presentation]. AOCS Annual Meeting & Expo 2021. |
Mascrez, S., & Purcaro, G. (May 2021). Multi-Cumulative Trapping HS-SPME to enhance the volatile profile of extra-virgin olive oil [Poster presentation]. AOCS Annual Meeting & Expo 2021. |
Bauwens, G., Panto, S., & Purcaro, G. (26 April 2021). Mineral oil saturated and aromatic hydrocarbons quantification: Mono- and two-dimensional approaches. Journal of Chromatography. A, 1643, 462044. doi:10.1016/j.chroma.2021.462044 |
Hochegger, A., Moret, S., Geurts, L., Gude, T., Leitner, E., Mertens, B., O'Hagan, S., Poças, F., Simat, T., & Purcaro, G. (20 April 2021). Mineral oil risk assessment: Knowledge gaps and roadmap. Outcome of a multi-stakeholders workshop. Trends in Food Science and Technology, 113, 151-166. doi:10.1016/j.tifs.2021.03.021 |
Hoc, B., Francis, F., Carpentier, J., Mostade, L., Blecker, C., Purcaro, G., & Caparros Megido, R. (April 2021). ω3-enrichment of Hermetia illucens (L. 1758) prepupae from oilseed byproducts. Journal of the Saudi Society of Agricultural Sciences, 20. doi:10.1016/j.jssas.2021.01.001 |
Ciale Rosso, M., Stilo, F., Mascrez, S., Bicchi, C., Purcaro, G., & Cordero, C. (23 March 2021). Shelf-Life Evolution of the Fatty Acid Fingerprint in High-Quality Hazelnuts (Corylus avellana L.) Harvested in Different Geographical Regions. Foods, 10 (3), 685. doi:10.3390/foods10030685 |
Bauwens, G., & Purcaro, G. (12 March 2021). LC-GC×GC-ToFMS/FID: a powerful technique for MOSH and MOAH quantification and characterization [Poster presentation]. 1st European Sample Preparation e-Conference. |
Purcaro, G. (11 March 2021). Sample Introduction And Multidimensionality As Part Of Sample Preparation [Paper presentation]. 1st European Sample Preparation e-Conference. |
Mascrez, S., Danthine, S., & Purcaro, G. (March 2021). Microwave-assisted saponification and SPE for the simultaneous or alternative analysis of dialkyl ketones and sterols in fats [Poster presentation]. 1st European Sample Preparation e-Conference. |
Mascrez, S., Psillakis, E., & Purcaro, G. (March 2021). Vacuum-assisted headspace SPME under sub-ambient temperature for the analysis of fish samples [Poster presentation]. 1st European Sample Preparation e-Conference. |
Mascrez, S., Psillakis, E., & Purcaro, G. (March 2021). Vacuum-assisted headspace SPME: A powerful tool for extra virgin olive oil profiling enhancement [Poster presentation]. 1st European Sample Preparation e-Conference. |
Mascrez, S., & Purcaro, G. (March 2021). Multi-Cumulative Trapping HSSPME to enhance the volatile profile of extra virgin olive oil [Poster presentation]. 1st European Sample Preparation e-Conference. |
Mascrez, S., & Purcaro, G. (February 2021). Enhanced fingerprinting of extra virgin olive oil by multiple-cumulative SPME and GCxGC [Poster presentation]. 12th Multidimensional Chromatography Virtual Workshop. |
Purcaro, G. (01 February 2021). LC-GC×GC-TOFMS/FID, a powerful platform for MOSH/MOAH Determination [Paper presentation]. Mineralölanalytik in Lebensmitteln & Bedarfsgegenständen – Praxisworkshop. |
Purcaro, G., & Bauwens, G. (01 February 2021). Advancement on the validation of the integrated LC-GC×GC-TOF MS/FID platform for mosh and moah determination [Paper presentation]. 12th Multidimensional Chromatography Workshop. |
Sdrigotti, N., Bauwens, G., & Purcaro, G. (February 2021). A Review of MOSH and MOAH Analysis in Food. LCGC Europe, 34 (2), 1-19. |
Bertoz, V., Purcaro, G., Conchione, C., & Moret, S. (2021). A Review on the Occurrence and Analytical Determination of PAHs in Olive Oils. Foods, 10, 324. doi:10.3390/foods10020324 |
Hoc, B., Tomson, T., Malumba Kamba, P., Blecker, C., Jijakli, H., Purcaro, G., Francis, F., & Caparros Megido, R. (2021). Production of rainbow trout (Oncorhynchus mykiss) using black soldier fly (Hermetia illucens) prepupae-based formulations with differentiated fatty acid profiles. Science of the Total Environment, 794. doi:10.1016/j.scitotenv.2021.148647 |
Mascrez, S., Danthine, S., & Purcaro, G. (2021). Microwave-Assisted Saponification Method Followed by Solid-Phase Extraction for the Characterization of Sterols and Dialkyl Ketones in Fats. Foods, 10, 445. doi:10.3390/foods10020445 |
Mascrez, S., & Purcaro, G. (2021). Multiple-cumulative trapping non-saturated headspace SPME: A powerful tool to increase volatile fingerprints [Poster presentation]. 2021 AOCS Annual Meeting & Expo (virtual). |
Mtibaa, I., Zouari, A., Purcaro, G., Attia, H., Ayadi, M. A., & Danthine, S. (2021). Crystallization mechanisms in camel milk cream during physical ripening: Effect of temperature and ripening duration. Transactions of the Institution of Chemical Engineers. Part C, Food and Bioproducts Processing, 127, 435–442. doi:10.1016/j.fbp.2021.03.016 |
Purcaro, G. (2021). The power of multidimensionality in the analysis of MOSH and MOAH in foods [Vendor seminar LECO] [Paper presentation]. Recent Advances in Food Analysis (RAFA). |
Purcaro, G. (2021). Microwave assisted extraction and saponification for food quality and safety [Vendor seminar Milestone] [Paper presentation]. Recent Advances in food analysis (RAFA). |
Purcaro, G. (2021). LC-GCxGC-ToFMS/FID platform for MOSH and MOAH determination: a quantitative and confirmative approach [Paper presentation]. Deutsche Gesellschaft für Fettwissenschaft e.V., Mineral Oil Contaminants in Food (Hybrid-Event), Berlin, Germany. |
Purcaro, G. (2021). LC-GC×GC-ToFMS/FID for MOSH and MOAH analysis of complex food matrices [Vendor seminar Restek] [Paper presentation]. Recent Advances in food analysis (RAFA). |
Purcaro, G., & Bauwens, G. (2021). Multidimensionality as a Powerful Alley for the Improvement of Sample Preparation and Data Accuracy for MOSH and MOAH Analysis [Paper presentation]. 18th GC×GC Symposium. |
Purcaro, G., & Bauwens, G. (2021). LC-GC×GC-TOFMS/FID: Multidimensionality as a Powerful Alley for th Improvement of Sample Preparation and Data Accuracy for MOSH and MOAH Analysis [Paper presentation]. 18th GCxGC Symposium. |
Purcaro, G., & Bauwens, G. (2021). Advancement on the validation of the integrated LC-GC×GC-TOF MS/FID platform for MOSH and MOAH determination [Paper presentation]. 12th Multidimensional Chromatography Workshop. |
Purcaro, G., & Fina, A. (2021). One-step microwave-assisted extraction and derivatization followed by flow-modulation GC×GC-FID for rapid determination of fatty acid in a variety of food samples [Paper presentation]. 18th Euro Fed Lipid Congress. |
Qiao, Y., Bi, J., Chen, Q., Wu, X., Gou, M., Hou, H., Jin, X., & Purcaro, G. (2021). Volatile Profile Characterization of Winter Jujube from Different Regions via HS-SPME-GC/MS and GC-IMS. Journal of Food Quality, 2021, 1-15. doi:10.1155/2021/9958414 |
Sdrigotti, N.* , Collard, M.* , & Purcaro, G.*. (2021). Evolution of hyphenated techniques for mineral oil analysis in food. Journal of Separation Science, 44 (1), 464-482. doi:10.1002/jssc.202000901 * These authors have contributed equally to this work. |
Uerlings, J., Arevalo Sureda, E., Schroyen, M., Kroeske, K., Tanghe, S., De Vos, M., Bruggeman, G., Wavreille, J., Bindelle, J., Purcaro, G., & Everaert, N. (2021). Impact of Citrus Pulp or Inulin on Intestinal Microbiota and Metabolites, Barrier, and Immune Function of Weaned Piglets. Frontiers in Nutrition, 8, 650211. doi:10.3389/fnut.2021.650211 |
Mascrez, S., & Purcaro, G. (29 June 2020). Enhancing the performance of SPME for the fingerprinting of olive oil volatiles [Poster presentation]. 2020 AOCS Annual Meeting & Expo, United States. |
Purcaro, G., & Panto, S. (29 June 2020). Towards a fully integrated LC-GC×GC-ToFMS/FID platform to unravel the MOSH&MOAH hump in food [Paper presentation]. 2020 AOCS Annual Meeting & Expo. |
Mtibaa, I., Purcaro, G., Attia, H., Ayadi, M. A., & Danthine, S. (June 2020). Characteristics and processing challenges of camel milk cream. Inform magazine, 31 (6), 24-26. doi:10.21748/inform.06.2020.24 |
Mascrez, S., & Purcaro, G. (May 2020). Exploring multiple-cumulative trapping solid-phase microextraction for olive oil aroma profiling. Journal of Separation Science, 43, 1934-1941. doi:10.1002/jssc.202000098 |
Purcaro, G. (16 March 2020). Vacuum-Assisted HSSPME for food analysis [Paper presentation]. PortASAP. |
Mascrez, S., & Purcaro, G. (2020). Vacuum Assisted Headspace Solid-Phase Microextraction: A Powerful Tool for Olive Oil Analysis. Chromatography Today. |
Collard, M., & Purcaro, G. (31 January 2020). Comprehensive multidimensional gas chromatography coupled with ms and fid (GC×GC-MS/FID) for mosh&moah determination in food [Poster presentation]. 25th National Symposium for Applied Biological Sciences (NSABS), Liege, Belgium. |
Glineur, A., Nott, K., & Purcaro, G. (31 January 2020). Development and validation of a UHPLC-ESI-MS/MS method for determining estrogenic compounds in surface water at the ultra-trace level [Poster presentation]. National Symposium for Applied Biological Sciences (NSABS). |
Goumbri, W. B., Somé, T. I., Marini Djang'Eing'A, R., Purcaro, G., & Danthine, S. (31 January 2020). Evaluation of some quality parameters of crude shea butter produced in Burkina Faso [Poster presentation]. 25th National Symposium for Applied Biological Sciences, Gembloux, Belgium. |
Hoc, B., Francis, F., carpentier, J., Mostade, L., Blecker, C., Purcaro, G., & Caparros Megido, R. (27 January 2020). Enrichment in omega3 of Hermetia illucens (L. 1758) prepupae from oilseed co products [Poster presentation]. NSABS, Gembloux, Belgium. |
Glineur, A., Nott, K., Carbonelle, P., Ronkart, S., & Purcaro, G. (2020). Development and validation of a method for determining estrogenic compounds in surface water at the ultra-trace level required by the EU Water Framework Directive Watch List. Journal of Chromatography. A, 1624, 461242. doi:10.1016/j.chroma.2020.461242 |
Mascrez, S., Psikallis, E., & Purcaro, G. (2020). Vacuum-Assisted HSSPME, An Innovative Sampling Approach, For Food Applications [Poster presentation]. National Symposium for Applied Biological Science. |
Mascrez, S., Psillakis, E., & Purcaro, G. (2020). A Multifaceted investigation of the effect of reduced pressure condition on the headspace-solid phase microextraction of extra-virgin olive oil. Analytica Chimica Acta, 1103, 106-114. doi:10.1016/j.aca.2019.12.053 |
Mascrez, S., & Purcaro, G. (2020). Enhancement of volatile profiling using multiple-cumulative trapping solid-phase microextraction. consideration on sample volume. Analytica Chimica Acta, 1122, 89-96. doi:10.1016/j.aca.2020.05.007 |
Panto', S., Collard, M., & Purcaro, G. (2020). Comprehensive gas chromatography coupled to simultaneous dual detection (ToFMS/FID) as a confirmatory method for MOSH&MOAH determination in food. Current Trend in Mass spectrometry, 18 (3), 15-20. |
Purcaro, G. (2020). Classical and comprehensive 2D LC-GC. In P. Q. Tranchida & L. Mondello, Hyphenations of Capillary Chromatography with Mass Spectrometry (pp. 227-275). Amsterdam, Netherlands: Elsevier. |
Purcaro, G., Mascrez, S., & Psillakis, E. (2020). Vacuum-Assisted HSSPME for food analysis [Paper presentation]. PortASAP Meeting (virtual). |
Goumbri, W. B., Somé, T. I., Marini Djang'Eing'A, R., Purcaro, G., & Danthine, S. (11 December 2019). Evaluation of some quality parameters of crude shea butter produced in Burkina Faso [Poster presentation]. 2nd CIRM Day, Liège, Belgium. |
Glineur, A., Nott, K., Ronkart, S., & Purcaro, G. (14 November 2019). Development and validation of methods using UHPLC ESI MS/MS for the quantification of estrogenic compounds at ultra trace levels in different types of water [Poster presentation]. Seminar on Process-Related Compounds and Natural Toxins, Gembloux, Belgium. |
Purcaro, G. (14 November 2019). Presentation on the topic of the Mineral oil group [Paper presentation]. Seminar on Process-Related Compounds and Natural Toxins, Gembloux, Belgium. |
Purcaro, G., & Panto, S. (05 November 2019). Comprehensive gas chromatography coupled to simultaneous dual detection (ToFMS/FID) as the confirmatory method for mineral oil determination in food [Paper presentation]. 9th International Symposium on Recent Advances in Food Analysis (RAFA 2019), Prague, Czechia. |
Mascrez, S., Collard, M., Panto, S., & Purcaro, G. (September 2019). Comprehensive Multidimensional Gas Chromatography Coupled With Dual Detection For MOSH&MOAH Determination In Food [Poster presentation]. EuroAnalysis 2019. |
Mascrez, S., Psillakis, E., & Purcaro, G. (September 2019). A comprehensive study on the effect of vacuum of targeted volatile compounds on HSSPME in a complex matrix: A softer efficient method to profile olive oil aromas [Paper presentation]. EuroAnalysis 2019. |
Glineur, A., Nott, K., & Purcaro, G. (May 2019). Quantification of estrogenic compounds as pyridine-3-sulfonyl derivatives by UHPLC-ESI-MS/MS at trace level in different aqueous matrices [Poster presentation]. The 43th International Symposium on Capillary Chromatography (ISCC) & The 16th GC×GC Symposium, Fort Worth, Texas, United States. |
Mascrez, S., Psillakis, E., & Purcaro, G. (May 2019). A comparative study on the effect of vacuum on HS-SPME of olive oil volatiles [Poster presentation]. The 43th International Symposium on Capillary Chromatography (ISCC) & The 16th GC×GC Symposium, Fort Worth, Texas, United States. |
Purcaro, G., Collard, M., & Pantó, S. (May 2019). Towards a regulatory method using multidimensional techniques. The mineral oil case [Paper presentation]. The 43th International Symposium on Capillary Chromatography (ISCC) & The 16th GC×GC Symposium, Fort Worth, Texas, United States. |
Stefanuto, P.-H., & Purcaro, G. (May 2019). GCxGC Discusssion Panel: The GCxGC Report Card - Method Development/Workflow [Paper presentation]. International Symposium on Capillary Chromatography and GCxGC, Fort Worth, United States. |
Zanella, D., Franchina, F., Stefanuto, P.-H., Focant, J.-F., Purcaro, G., Burklund, A., Beccaria, M., & Hill, J. (March 2019). Importance du type d'absorbant pour l'échantillonnage des volatils : application sur les cultures bactériennes et l'haleine [Poster presentation]. 13ème congrès francophone sur les sciences séparatives et les couplages de l'AFSEP, Paris, France. |
Beccaria, M., Bobak, C., Maitshotlo, B., Mellors, T. R., Purcaro, G., Franchina, F., Rees, C. A., Nasir, M., Black, A., & Hill, J. E. (2019). Exhaled human breath analysis in active pulmonary tuberculosis diagnostics by comprehensive gas chromatography-mass spectrometry and chemometric techniques. Journal of Breath Research, 13 (1), 016005. doi:10.1088/1752-7163/aae80e |
Franchina, F., Purcaro, G., Burklund, A., Beccaria, M., & Hill, J. E. (2019). Evaluation of different adsorbent materials for the untargeted and targeted bacterial VOC analysis using GC×GC-MS. Analytica Chimica Acta, 1066, 146-153. doi:10.1016/j.aca.2019.03.027 |
Mascrez, S., Psillakis, E., & Purcaro, G. (2019). Exploring the performance of vacuum-HS-SPME for volatile profiling of olive oil [Poster presentation]. International Symposium on Recent Advances In Food Analysis. |
Mascrez, S., & Purcaro, G. (2019). Determination of dialkyl ketones (DAK) in interesterified lipids by GC-FID and GC-MS [Paper presentation]. ILSI seminar. |
Purcaro, G. (2019). Towards a regulatory method using multidimensional techniques. The mineral oil case [Paper presentation]. GCxGC Symposium & Workshop, Forth worth, United States - Texas. |
Purcaro, G. (2019). GC×GC-ToFMS/FID: a journey beyond the MOSH&MOAH hump in food determination [Paper presentation]. 9th International Symposium on Recent Advances in Food Analysis (RAFA 2019), Prague, Czechia. |
Purcaro, G., Nasir, M., Franchina, F., Rees, C. A., Aliyeva, M., Daphtary, N., Wargo, M. J., Lundblad, L. K. A., & Hill, J. E. (2019). Breath metabolome of mice infected with Pseudomonas aeruginosa. Metabolomics, 15 (1). doi:10.1007/s11306-018-1461-6 |
Rees, C. A., Beccaria, M., Franchina, F., Hill, J. E., & Purcaro, G. (2019). Fatty acid methyl ester (FAME) profiling identifies carbapenemase-producing Klebsiella pneumoniae belonging to clonal complex 258. Separations, 6 (2). doi:10.3390/separations6020032 |
Franchina, F., Zanella, D., Stefanuto, P.-H., Purcaro, G., Burklund, A., Beccaria, M., Jane, H., & Focant, J.-F. (08 November 2018). Importance of sorbent material selection for VOCs sampling: application on bacterial cultures and breath [Paper presentation]. Breath Biopsy Conference 2018, Cambridge, United Kingdom. |
Kormuth, K., Franchina, F., Le Sage, V., Nturibi, E., Lakdawala, S. S., Hill, J. E., & Purcaro, G. (08 November 2018). A breathprint of influenza a virus infection in the ferret model [Poster presentation]. Breath Biopsy Conference, Cambridge, United Kingdom. |
Purcaro, G. (November 2018). Analytical techniques for MOSH and MOAH quantification and identification [Paper presentation]. MOSH/MOAH-Mineral Oil Contamination of Foodstuff, Berlin, Germany. |
Franchina, F., Beccaria, M., Nasir, M., Hill, J. E., & Purcaro, G. (13 May 2018). Exploring different ionization energy for bacterial fatty acid analysis in GC-MS [Poster presentation]. The 42th International Symposium on Capillary Chromatography (ISCC) & The 15th GC×GC Symposium, Riva del Garda, Italy. |
Purcaro, G., Kormuth, K. A., Lakdawala, S. S., Franchina, F., Rees, C. A., Nasir, M., & Hill, J. E. (13 May 2018). Viral infection signature using GC×GC TOF MS [Paper presentation]. The 42th International Symposium on Capillary Chromatography (ISCC) & The 15th GC×GC Symposium, Riva del Garda, Italy. |
Purcaro, G.* , Stefanuto, P.-H.* , Flavio, F., Marco, B., Wieland-Alter, W., Wright, P., & Hill, J. (2018). SPME-GC×GC-TOF MS fingerprint of virally-infected cell culture: Sample preparation optimization and data processing evaluation. Analytica Chimica Acta. doi:10.1016/j.aca.2018.03.037 * These authors have contributed equally to this work. |
Beccaria, M., Franchina, F., Nasir, M., Mellors, T., Hill, J. E., & Purcaro, G. (2018). Investigation of mycobacteria fatty acid profile using different ionization energies in GC–MS. Analytical and Bioanalytical Chemistry, 410 (30), 7987-7996. doi:10.1007/s00216-018-1421-z |
Franchina, F., Nasir, M., Beccaria, M., Mellors, T., Hill, J. E., & Purcaro, G. (2018). Investigating bacterial volatilome for the classification and identification of mycobacterial species [Poster presentation]. The 42th International Symposium on Capillary Chromatography (ISCC) & The 15th GC×GC Symposium, Riva del Garda, Italy. |
Purcaro, G. (2018). Raymond P. W. Scott: Introduction to analytical gas chromatography, 2nd ed. Analytical and Bioanalytical Chemistry. doi:10.1007/s00216-018-1207-3 |
Purcaro, G., Rees, C. A., Melvin, J. A., Bomberger, J. M., & Hill, J. E. (2018). Volatile fingerprinting of Pseudomonas aeruginosa and respiratory syncytial virus infection in an in vitro cystic fibrosis co-infection model. Journal of Breath Research, 12 (4), 046001. doi:10.1088/1752-7163/aac2f1 |
Vita, F., Franchina, F., Taiti, C., Locato, V., Pennazza, G., Santonico, M., Purcaro, G., De Gara, L., Mancuso, S., Mondello, L., & Alpi, A. (2018). Environmental conditions influence the biochemical properties of the fruiting bodies of Tuber magnatum Pico. Scientific Reports, 8 (1). doi:10.1038/s41598-018-25520-7 |
Purcaro, G., Rees, C., Wieland-Alter, W., Schneider, M., Wang, X., Stefanuto, P.-H., Wright, P., Enelow, R., & Hill, J. (December 2017). Volatile fingerprinting of human respiratory viruses from cell culture. Journal of Breath Research, 12 (2). doi:10.1088/1752-7163/aa9eef |
Purcaro, G., Wang, D., Rees, C. A., Franchina, F., & Hill, J. E. (May 2017). Towards a rapid non-invasive detection method for viral and bacterial respiratory infections using GC×GC TOF MS [Paper presentation]. The 41th International Symposium on Capillary Chromatography (ISCC) & The 14th GC×GC Symposium, Fort Worth, United States. |
Barp, L.* , Franchina, F.* , Purcaro, G., Tranchida, P. Q., & Mondello, L. (2017). In-pipette solid-phase extraction prior to flow-modulation comprehensive two-dimensional gas chromatography with dual detection for the determination of minor components in vegetable oils. Talanta, 165, 598-603. doi:10.1016/j.talanta.2017.01.009 * These authors have contributed equally to this work. |
Beccaria, M., Inferrera, V., Rigano, F., Gorynski, K., Purcaro, G., Pawliszyn, J., Dugo, P., & Mondello, L. (2017). Highly informative multiclass profiling of lipids by ultra-high performance liquid chromatography – Low resolution (quadrupole) mass spectrometry by using electrospray ionization and atmospheric pressure chemical ionization interfaces. Journal of Chromatography. A, 1509, 69-82. doi:10.1016/j.chroma.2017.06.017 |
Purcaro, G., Tranchida, P. Q., & Mondello, L. (2017). Comprehensive 2D GC Methodologies for the Analysis of Lipids. In Handbook of Advanced Chromatography /Mass Spectrometry Techniques. AOCS Press. |
Zoccali, M., Purcaro, G., Schepis, A., Tranchida, P. Q., & Mondello, L. (2017). Miniaturization of the QuEChERS Method in the Fast Gas Chromatography-Tandem Mass Spectrometry Analysis of Pesticide Residues in Vegetables. Food Analytical Methods, 10 (8), 2636-2645. doi:10.1007/s12161-017-0826-1 |
Zoccali, M., Purcaro, G., Barp, L., Beccaria, M., Sciarrone, D., & Mondello, L. (August 2016). Improvement in the determination of mineral oil contamination in vegetable oils: efficient removal of olefin interferences by LC-LC-GC [Poster presentation]. 31th International Symposium on Chromatography, Cork, Ireland. |
Purcaro, G. (May 2016). Multidimensional techniques for quality assessment of lipids [Paper presentation]. 107th AOCS Annual Meeting and Expo, Salt Lake City, United States. |
Tranchida, P. Q., Franchina, F., Purcaro, G., Maimone, M., & Mondello, L. (May 2016). Hyphenations of (low-)flow modulation comprehensive 2D GC with single quadrupole, triple quadrupole and high-resolution time-of-flight mass spectrometry [Paper presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Aguennouz, M., Beccaria, M., Purcaro, G., Oteri, M., Micalizzi, G., Musumesci, O., Ciranni, A., Di Giorgio, R. M., Toscano, A., Dugo, P., & Mondello, L. (2016). Analysis of lipid profile in lipid storage myopathy. Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences, 1029-1030, 157-168. doi:10.1016/j.jchromb.2016.06.039 |
Albergamo, A., Rigano, F., Purcaro, G., Mauceri, A., Fasulo, S., & Mondello, L. (2016). Free fatty acid profiling of marine sentinels by nanoLC-EI-MS for the assessment of environmental pollution effects. Science of the Total Environment, 571, 955-962. doi:10.1016/j.scitotenv.2016.07.082 |
Beccaria, M., Inferrera, V., Rigano, F., Dugo, P., Purcaro, G., & Mondello, L. (2016). Lipidomics-type analysis of human plasma by UHPLC-qMS [Poster presentation]. 107th AOCS Annual Meeting and Expo, Salt Lake City, United States. |
Beccaria, M., Inferrera, V., Rigano, F., Purcaro, G., Dugo, P., & Mondello, L. (2016). Lipidomics-type analysis by UHPLC-Q-MS with ESI and APCI interfaces [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Beccaria, M., Moret, E., Purcaro, G., Pizzale, L., Cotroneo, A., Dugo, P., Mondello, L., & Conte, L. S. (2016). Reliability of the ΔeCN42 limit and global method for extra virgin olive oil purity assessment using different analytical approaches. Food Chemistry, 190, 216-225. doi:10.1016/j.foodchem.2015.05.075 |
Beccaria, M., Oteri, M., Micalizzi, G., Bonaccorsi, I. L., Purcaro, G., Dugo, P., & Mondello, L. (2016). Reuse of Dairy Product: Evaluation of the Lipid Profile Evolution During and After Their Shelf-Life. Food Analytical Methods, 9 (11), 3143-3154. doi:10.1007/s12161-016-0466-x |
Beccaria, M., Purcaro, G., Oteri, M., Micalizzi, G., Dugo, P., & Mondello, L. (2016). Analysis of lipid profile in human lipid storage myopathies [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Bjerk, T. R., Maimone, M., Franchina, F., Purcaro, G., Sciarrone, D., Zini, C., Tranchida, P. Q., & Mondello, L. (2016). (Low-)flow modulation comprehensive two-dimensional gas chromatography experiments under different outlet pressure conditions [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Dugo, P., Donato, P., Cacciola, F., Beccaria, M., Inferrera, V., Rigano, F., Purcaro, G., & Mondello, L. (January 2016). Hyphenated LC-MS and LC×LC-MS techniques reduce the need for extensive sample preparation for accurate analysis of target compounds [Paper presentation]. HTC-14, 14th International Symposium on Hyphenated Techniques in Chromatography and Separation Technology, Ghent, Belgium. |
Franchina, F., Barp, L., Zoccali, M., Purcaro, G., Sciarrone, D., TRanchida, P. Q., & Mondello, L. (2016). Phthalic acid esters determination in vegetable oils by using SPME followed by fast GC coupled with triple quadrupole MS [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Franchina, F., Purcaro, G., Maimone, M., Tranchida, P. Q., & Mondello, L. (2016). Recent evolution of flow-modulation comprehensive gas chromatography within the context of mass spectrometry hyphenation. Chimica Oggi, 34 (2), 6-10. |
Franchina, F., Purcaro, G., Tranchida, P. Q., & Mondello, L. (January 2016). Novel Ultra-Fast Quad and Triple Quad Detectors for GC×GC [Paper presentation]. 7th Multidimensional chromatography workshop, Toronto, Canada. |
Maimone, M., Franchina, F., Purcaro, G., Tranchida, P. Q., & Mondello, L. (2016). (Low-)flow modulation comprehensive two-dimensional gas chromatography for the determination of suspected allergens in fragrances [Poster presentation]. HTC-14, 14th International Symposium on Hyphenated Techniques in Chromatography and Separation Technology, Ghent, Belgium. |
Micalizzi, G., Utzcas, M., Purcaro, G., Sciarrone, D., & Mondello, L. (2016). Exploitation of different techniques for a reliable identification of unknown compounds to be added into a dedicated database fro the flavor and fragrance field [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Moret, S., Scolaro, M., Barp, L., Purcaro, G., & Conte, L. S. (2016). Microwave assisted saponification (MAS) followed by on-line liquid chromatography (LC)-gas chromatography (GC) for high-throughput and high-sensitivity determination of mineral oil in different cereal-based foodstuffs. Food Chemistry, 196, 50-57. doi:10.1016/j.foodchem.2015.09.032 |
Oteri, M., Beccaria, M., Purcaro, G., Micalizzi, G., Bonaccorsi, I. L., Cacciola, F., Dugo, P., & Mondello, L. (2016). Evaluation of the lipid profile of diary products during and after their shelf-life [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Purcaro, G., Barp, L., Beccaria, M., & Conte, L. S. (2016). Characterisation of minor components in vegetable oil by comprehensive gas chromatography with dual detection. Food Chemistry, 212, 730-738. doi:10.1016/j.foodchem.2016.06.048 |
Purcaro, G., Barp, L., & Moret, S. (2016). Determination of hydrocarbon contamination in foods. A review. Analytical Methods, 8 (29), 5755-5772. doi:10.1039/c6ay00655h |
Purcaro, G., Franchina, F., Barp, L., Tranchida, P. Q., & Mondello, L. (2016). Optimization of in-pipette solid-phase extraction for determination of minor components in vegetable oils by GC×GC-FID/MS [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Purcaro, G., Franchina, F., Barp, L., Tranchida, P. Q., & Mondello, L. (2016). Elucidation of minor components in vegetable oils by using comprehensive two-dimensional gas chromatography: A “green” evolution [Poster presentation]. 107th AOCS Annual Meeting and Expo, Salt Lake City, United States. |
Rigano, F., Albergamo, A., Sciarrone, D., Beccaria, M., Purcaro, G., & Mondello, L. (2016). Nano Liquid Chromatography Directly Coupled to Electron Ionization Mass Spectrometry for Free Fatty Acid Elucidation in Mussel. Analytical Chemistry, 88 (7), 4021-4028. doi:10.1021/acs.analchem.6b00328 |
Rigano, F., Albergamo, A., Sciarrone, D., Beccaria, M., Purcaro, G., & Mondello, L. (2016). Characterization of free fatty acid profile in mussels by Nano-LC directly coupled to electron ionization mass spectrometry [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Russo, M., Zoccali, M., Purcaro, G., Dugo, P., Funada, Y., HAttori, T., Nishimura, M., & Mondello, L. (2016). Pesticides determination by means of a green unified analytical tool [Poster presentation]. 44th HPLC, San Francisco, United States. |
Schepis, A., Zoccali, M., Purcaro, G., Tranchida, P. Q., & Mondello, L. (2016). Quantification of pesticides in food samples by means of miniaturized QuEChERS approach coupled to fast GC-QqQ MS [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Tranchida, P. Q., Maimone, M., Franchina, F., Bjerk, T. R., Zini, C. A., Purcaro, G., & Mondello, L. (2016). Four-stage (low-)flow modulation comprehensive gas chromatography-quadrupole mass spectrometry for the determination of recently-highlighted cosmetic allergens. Journal of Chromatography. A, 1439, 144-151. doi:10.1016/j.chroma.2015.12.002 |
Tranchida, P. Q., Purcaro, G., Maimone, M., & Mondello, L. (2016). Impact of comprehensive two-dimensional gas chromatography with mass spectrometry on food analysis. Journal of Separation Science, 39 (1), 149-161. doi:10.1002/jssc.201500379 |
Utczas, M., Micalizzi, G., Purcaro, G., & Mondello, L. (2016). Linear retention indices: added value to a dedicated MS spectra database for the reliable identification of complex samples in the flavour and fragrance field [Poster presentation]. 18th ExTech & 22th ISSS, Torun, Poland. |
Utczas, M., Zoccali, M., Micalizz, G., Purcaro, G., & Mondello, L. (2016). MS Spectra Database Of Flavours And Fragrances Coupled With Linear Retention Index Approach: Reliable Identification Of Complex Essential Oil Samples [Poster presentation]. 31th International Symposium on Chromatography, Cork, Ireland. |
Utzcas, M., Micalizzi, G., Purcaro, G., & Mondello, L. (2016). Embedded of the linear retention index information within a dedicated MS spectra database to boost the identification reliability of complex samples in the flavor and fragrance field [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Utzcas, M., Purcaro, G., Cacciola, F., Giuffrida, D., & Mondello, L. (2016). Variation in the volatile and non-volatile fraction in processed and native Arbutus unedo [Poster presentation]. 18th ExTech & 22th ISSS, Torun, Poland. |
Utzcas, M., Zoccali, M., Purcaro, G., Cacciola, F., & Mondello, L. (2016). CHROMATOPLUS SPECTRA and PESTICIDE mass spectral database: a powerful coupling of a unique chromatographic software with integrated automated LRI algorithm function exploiting the PESTICIDE MS database [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Zoccali, M., Barp, L., Beccaria, M., Sciarrone, D., Purcaro, G., & Mondello, L. (2016). Improvement of mineral oil saturated and aromatic hydrocarbons determination in edible oil by liquid-liquid-gas chromatography with dual detection. Journal of Separation Science, 39 (3), 623-631. doi:10.1002/jssc.201501247 |
Zoccali, M., Barp, L., Beccaria, M., Sciarrone, D., Purcaro, G., & Mondello, L. (2016). Efficient on-line liquid chromatography removal of olefin interferences prior to the gas chromatography determination of mineral oil contamination in vegetable oils [Poster presentation]. HTC-14, 14th International Symposium on Hyphenated Techniques in Chromatography and Separation Technology, Ghent, Belgium. |
Zoccali, M., Purcaro, G., Barp, L., Beccaria, M., Sciarrone, D., & Mondello, L. (2016). Efficient removal of olefin interferences by on-line liquid-liquid chromatography prioe to the gas chromatography determination of mineral oil contamination in vegetable oils [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Zoccali, M., Purcaro, G., Nishimura, M., & Mondello, L. (2016). On-line coupling of CO2 supercritical fluid extraction chromatography coupled to triple quadrupole mass spectrometry [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Zoccali, M., Purcaro, G., Nishimura, M., & Mondello, L. (2016). A unified analytical tool for green extraction and determination of both targeted and untargeted analysis [Poster presentation]. 31th International Symposium on Chromatography, Cork, Ireland. |
Zoccali, M., Purcaro, G., Schepis, A., TRanchida, P. Q., Cacciola, F., & Mondello, L. (2016). Miniaturized QuEChERS methodologies coupled to fast gas chromatography-triple quadrupole mass spectrometry fro the determination of pesticides in different vegetables [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Zoccali, M., Purcaro, G., Utczas, M., Nishimura, M., & Mondello, L. (2016). On-line extraction and determination by means CO2 supercritical fluid and triple quadrupole mass spectrometry [Poster presentation]. 18th ExTech & 22th ISSS, Torun, Poland. |
Zoccali, M., Utzcas, M., Purcaro, G., & Mondello, L. (2016). VUV spectra database of fatty acids derivatized coupled with linear retention index approach: reliable identification tool fro complex samples [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Zoccali, M., Utzcas, M., Purcaro, G., Tranchida, P. Q., Schug, K. A. A., & Mondello, L. (2016). Flow-modulated comprehensive 2D gas chromatography combined with vacuum ultraviolet detector for the analysis of complex mixture [Poster presentation]. 40th International Symposium on Capillary Chromatography, and 13th GC×GC Symposium, Riva del Garda, Italy. |
Purcaro, G., Moret, S., & Conte, L. S. (2015). Polycyclic Aromatic Hydrocarbons. In B. Caballero, P. Finglas, ... F. Toldra, Encyclopedia of Food and Health (pp. 406-418). Academic Press. doi:10.1016/B978-0-12-384947-2.00550-X |
Beccaria, M., Costa, R., Oteri, M., Cacciola, F., Purcaro, G., Dugo, P., & Mondello, L. (September 2015). Determination of the Triacylglycerol Fraction in Fish Oil by Ultra Performance and Comprehensive Liquid Chromatography Techniques with the Support of Gas Chromatography and Mass Spectrometry Data [Paper presentation]. Euro Fed Lipid Congress "Fats, Oils and Lipids: New Challenges in Technology, Quality Control and Health, Florence, Italy. |
Purcaro, G., Barp, L., Zoccali, M., Franchina, F., Tranchida, P. Q., Moret, S., Conte, L. S., & Mondello, L. (May 2015). GC×GC: a powerful tool for a comprehensive evaluation of food quality, authenticity, and safety [Paper presentation]. The 39th International Symposium on Capillary Chromatography (ISCC) & The 12th GC×GC Symposium, Fort Worth, United States. |
Barp, L., Purcaro, G., Franchina, F., Zoccali, M., Sciarrone, D., Tranchida, P. Q., & Mondello, L. (2015). Determination of phthalate esters in vegetable oils using direct immersion solid-phase microextraction and fast gas chromatography coupled with triple quadrupole mass spectrometry. Analytica Chimica Acta, 887, 237-244. doi:10.1016/j.aca.2015.06.039 |
Conchione, C., Purcaro, G., Conte, L. S., & Moret, S. (2015). Solid-phase microextraction with gas chromatography and mass spectrometry determination of benzo(a)pyrene in microcrystalline waxes used as food additives. Journal of Separation Science, 38 (10), 1749-1754. doi:10.1002/jssc.201401246 |
Costa, R., Albergamo, A., Oteri, M., Piparo, M., Purcaro, G., Dugo, P., & Mondello, L. (2015). Multidimensional Gas Chromatographic Techniques Applied to the Analysis of Lipids from Marine Species of the Mediterranean Sea [Paper presentation]. 106th AOCS Annual Meeting and Industry Showcases, Orlando, United States. |
Franchina, F., Maimone, M., Sciarrone, D., Purcaro, G., Tranchida, P. Q., & Mondello, L. (2015). Evaluation of a novel helium ionization detector within the context of (low-)flow modulation comprehensive two-dimensional gas chromatography. Journal of Chromatography. A, 1402, 102-109. doi:10.1016/j.chroma.2015.05.013 |
Inferrera, V., Beccaria, M., Donato, P., Purcaro, G., Dugo, P., & Mondello, L. (2015). Lipidomic analysis of biological samples by using one- and multidimensional chromatography coupled to mass spectrometry [Paper presentation]. 21st International Symposium on Separation Science (ISSS 2015), Ljubiana, Slovenia. |
Panto, S., Sciarrone, D., Purcaro, G., & Mondello, L. (2015). LC-GC-GC-GC-prep: a new powerful and versatile system for the collection of highly pure volatile from complex samples [Paper presentation]. 21st International Symposium on Separation Science (ISSS 2015), Ljubiana, Slovenia. |
Purcaro, G., Barp, L., Beccaria, M., & Conte, L. S. (2015). Fingerprinting of vegetable oil minor components by multidimensional comprehensive gas chromatography with dual detection. Analytical and Bioanalytical Chemistry, 407 (1), 309-319. doi:10.1007/s00216-014-8140-x |
Purcaro, G., Barp, L., & Conte, L. (2015). Comparison of different injection modes in edible oil minor components analysis. Journal of Separation Science, 38 (13), 2278-2285. doi:10.1002/jssc.201401242 |
Purcaro, G., Conte, L., & Mondello, L. (2015). Potentiality of the GC×GC Technique for Quality and Authenticity Assessment of Olive Oil [Paper presentation]. 106th AOCS Annual Meeting and Industry Showcases, Orlando, United States. |
Purcaro, G., Rigano, F., Costa, R., Sciarrone, D., & Mondello, L. (2015). NanoLC coupled to an EI-MS system for a fast and reliable identification of lipid components [Paper presentation]. The 39th International Symposium on Capillary Chromatography (ISCC) & The 12th GC×GC Symposium, Fort Worth, United States. |
Tranchida, P. Q., Maimone, M., Purcaro, G., Dugo, P., & Mondello, L. (2015). The penetration of green sample-preparation techniques in comprehensive two-dimensional gas chromatography. TrAC: Trends in Analytical Chemistry, 71, 74-84. doi:10.1016/j.trac.2015.03.011 |
Zoccali, M., Tranchida, P. Q., Dugo, P., Purcaro, G., & Mondello, L. (2015). On-line combination of liquid chromatography-large volume injection-comprehensive two-dimensional gas chromatography-triple quad mass spectrometry: a powerful 5-D separation-science tool [Paper presentation]. The 39th International Symposium on Capillary Chromatography (ISCC) & The 12th GC×GC Symposium, Fort Worth, United States. |
Moret, S., Scolaro, M., Barp, L., Purcaro, G., Sander, M., & Conte, L. S. (2014). Optimisation of pressurised liquid extraction (PLE) for rapid and efficient extraction of superficial and total mineral oil contamination from dry foods. Food Chemistry, 157, 470-475. doi:10.1016/j.foodchem.2014.02.071 |
Purcaro, G., Codony, R., Pizzale, L., Mariani, C., & Conte, L. (2014). Evaluation of total hydroxytyrosol and tyrosol in extra virgin olive oils. European Journal of Lipid Science and Technology, 116 (7), 805-811. doi:10.1002/ejlt.201300420 |
Purcaro, G., & Conte, L. (2014). Fingerprint of vegetable oils: exploring minor compounds by GCxGC with dual detection [Paper presentation]. 38th International Symposium on Capillary Chromatography and 11th GC×GC Symposium, Riva del Garda, Italy. |
Purcaro, G., Cordero, C., Liberto, E., Bicchi, C., & Conte, L. S. (2014). Toward a definition of blueprint of virgin olive oil by comprehensive two-dimensional gas chromatography. Journal of Chromatography. A, 1334, 101-111. doi:10.1016/j.chroma.2014.01.067 |
Barp, L., Purcaro, G., Conte, L., & Moret, S. (2013). Development of rapid extraction methods and hyphenated techniques for determination of mineral oil hydrocarbons: the focus on MOSH and MOAH in foods [Paper presentation]. 8th Rapid Europe Methods, Noordwijkerhout, Netherlands. |
Barp, L., Purcaro, G., Moret, S., & Conte, L. S. (2013). A high-sample-throughput LC-GC method for mineral oil determination. Journal of Separation Science, 36 (18), 3135-3139. doi:10.1002/jssc.201300114 |
Conte, L., Moret, S., & Purcaro, G. (2013). Contaminazione da idrocarburi policiclici aromatici (PAHs) ed oli minerali in prodotti ittici: valutazioni ed approcci analitici [Paper presentation]. I prodotti ittici tra sicurezza e benessere, Marsala, Italy. |
Moret, S., Purcaro, G., Barp, L., & Conte, L. (2013). Mineral Oil saturated Hydrocarbons (MOSH) and mineral oil aromatic hydrocarbon (MOAH) determination in vegetable oils and fats [Paper presentation]. 11th EuroFed Lipid Congress, Antalya, Turkey. |
Moret, S., Sander, M., Purcaro, G., Scolaro, M., Barp, L., & Conte, L. S. (2013). Optimization of pressurized liquid extraction (PLE) for rapid determination of mineral oil saturated (MOSH) and aromatic hydrocarbons (MOAH) in cardboard and paper intended for food contact. Talanta, 115, 246-252. doi:10.1016/j.talanta.2013.04.061 |
Purcaro, G., Cordero, C. I. E., Bicchi, C., & Conte, L. (2013). Iterative approach to define the chemical blueprint of olive oil by GCxGC-MS [Paper presentation]. 3rd MS Food Day, Trento, Italy. |
Purcaro, G., Cordero, C. I. E., Bicchi, C., & Conte, L. (2013). Chemical blueprint of extravergin olive oil [Paper presentation]. 37th International Symposium on Capillary Chromatography and 10th GC×GC Symposium, Palm Spring, United States. |
Purcaro, G., Cordero, C. I. E., Bicchi, C., & COnte, L. (2013). A comprehensive approach to define the chemical blueprint of extra virgin olive oil [Paper presentation]. 6th International Symposium on Recent Advances in Food Analysis (RAFA), Prague, Czechia. |
Purcaro, G., Moret, S., & Conte, L. (2013). Sample pre-fractionation of environmental and food samples using LC-GC multidimensional techniques. TrAC: Trends in Analytical Chemistry, 43, 146-160. doi:10.1016/j.trac.2012.10.007 |
Purcaro, G., Moret, S., & Conte, L. S. (2013). Overview on polycyclic aromatic hydrocarbons: Occurrence, legislation and innovative determination in foods. Talanta, 105, 292-305. doi:10.1016/j.talanta.2012.10.041 |
Purcaro, G., Moret, S., Marega, M., & Conte, L. (2013). Lipid Molecules as Marker of Food Quality. In S. Sforza, Food Authentication Using Biorganic Molecules (pp. 197-220). Lancaster, United States: DEStech Publ. |
Purcaro, G., Picardo, M., Barp, L., Moret, S., & Conte, L. S. (2013). Direct-immersion solid-phase microextraction coupled to fast gas chromatography mass spectrometry as a purification step for polycyclic aromatic hydrocarbons determination in olive oil. Journal of Chromatography. A, 1307, 166-171. doi:10.1016/j.chroma.2013.07.068 |
Purcaro, G., Tranchida, P. Q., Barp, L., Moret, S., Conte, L. S., & Mondello, L. (2013). Detailed elucidation of hydrocarbon contamination in food products by using solid-phase extraction and comprehensive gas chromatography with dual detection. Analytica Chimica Acta, 773, 97-104. doi:10.1016/j.aca.2013.03.002 |
Purcaro, G., Zoccali, M., Tranchida, P. Q., Barp, L., Moret, S., Conte, L., Dugo, P., & Mondello, L. (2013). Comparison of two different multidimensional liquid-gas chromatography interfaces for determination of mineral oil saturated hydrocarbons in foodstuffs. Analytical and Bioanalytical Chemistry, 405 (2-3), 1077-1084. doi:10.1007/s00216-012-6535-0 |
Conte, L., Moret, S., & Purcaro, G. (2012). Vegetable oils contaminants: technological and analytical means to manage their occurrence [Paper presentation]. Indo-Indian Workshop on food biotechnology: industrial processing , safety & health, Patiala, India. |
Mondello, L., Zoccali, M., Purcaro, G., Franchina, F., Sciarrone, D., Moret, S., Conte, L., & Tranchida, P. Q. (2012). Determination of saturated-hydrocarbon contamination in baby foods by using on-line liquid-gas chromatography and off-line liquid chromatography-comprehensive gas chromatography combined with mass spectrometry. Journal of Chromatography. A, 1259, 221-226. doi:10.1016/j.chroma.2012.03.096 |
Moret, S., Barp, L., Purcaro, G., & Conte, L. S. (2012). Rapid and sensitive solid phase extraction-large volume injection-gas chromatography for the analysis of mineral oil saturated and aromatic hydrocarbons in cardboard and dried foods. Journal of Chromatography. A, 1243, 1-5. doi:10.1016/j.chroma.2012.04.040 |
Moret, S., Marega, M., Conte, L. S., & Purcaro, G. (2012). Sample preparation techniques for the determination of some food contaminants (polycyclic aromatic hydrocarbons, mineral oils and phthalates). In Comprehensive Sampling and Sample Preparation (4ed, pp. 313-356). Oxford, United Kingdom: Elsevier Inc. doi:10.1016/B978-0-12-381373-2.00138-1 |
Moret, S., Sander, M., Scolaro, M., Purcaro, G., & Conte, L. (2012). Determination of mineral oil saturated hydrocarbons (MOSH) and mineral oil aromatic hydrocarbon (MOAH) in cardboard and foods [Paper presentation]. 14th International Symposium on Advances in Extraction Technologies (Extech), Messina, Italy. |
Purcaro, G., Modello, L., Tranchida, P. Q., Barp, L., Conte, L., & Moret, S. (2012). Elucidation of hydrocarbon contamination in food products by using off-line solid-phase extraction and comprehensive two-dimensional gas chromatography with dual detection [Paper presentation]. the 36th International Symposium on Capillary Chromatography (ISCC) and the 9th GCxGC Symposium, Riva del Garda, Italy. |
Purcaro, G., Modello, L., Tranchida, P. Q., Moret, S., & Conte, L. (2012). Use of solid phase microextraction (SPME) for determination of mineral oil and polycyclic aromatic hydrocarbons by monodimensional GC or GCxGC [Paper presentation]. 14th International Symposium on Advances in Extraction Technologies (Extech), Messina, Italy. |
Purcaro, G., Moret, S., Bučar-Miklavčič, M., & Conte, L. S. (2012). Ultra-high performance liquid chromatographic method for the determination of polycyclic aromatic hydrocarbons in a passive environmental sampler. Journal of Separation Science, 35 (8), 922-928. doi:10.1002/jssc.201100922 |
Purcaro, G., Moret, S., & Conte, L. (2012). Hyphenated liquid chromatography-gas chromatography technique: Recent evolution and applications. Journal of Chromatography. A, 1255, 100-111. doi:10.1016/j.chroma.2012.02.018 |
Silva, B. J. G., Tranchida, P. Q., Purcaro, G., Queiroz, M. E. C., Mondello, L., & Lanças, F. M. (2012). Evaluation of comprehensive two-dimensional gas chromatography coupled to rapid scanning quadrupole mass spectrometry for quantitative analysis. Journal of Chromatography. A, 1255, 177-183. doi:10.1016/j.chroma.2012.05.035 |
Conte, L., Moret, S., & Purcaro, G. (2011). HPLC in Food Analysis. In D. Corradini (Ed.), Handbook of HPLC (2nd). CRC Press, Taylor & Francis. |
Mondello, L., Tranchida, P. Q., & Purcaro, G. (2011). Potential of comprehensive two-dimensional gas chromatography coupled to a very fast quadrupole mass spectrometer (20,000 amu/sec) [Paper presentation]. Pittcon 2011 Conference & Expo, Atlanta, United States. |
Mondello, L., Tranchida, P. Q., Purcaro, G., Fanali, C., Dugo, P., La Camera, E., Bisignano, C., & Banoub, J. H. (2011). Identification of the bacterial cellular lipid fraction by using fast GC × GC-MS and innovative MS libraries. In J. Banoub (Ed.), Detection of Biological Agents for the prevention of Bioterrorism (pp. 231-244). Springer. doi:10.1007/978-90-481-9815-3_15 |
Moret, S., Barp, L., Purcaro, G., & Conte, L. (2011). Rapid SPE-GC-FID Determination of MOSH (Mineral Oil Saturated Hydrocarbons) and MOAH (Mineral Oil Aromatic Hydrocarbons) in Printing Inks, Recycled Cardboard and in Dried Food as a Consequence of Migration Under Accelerated Test Condition [Paper presentation]. 5th International Symposium on Recent Advance in Food Analisys (RAFA), Prague, Czechia. |
Purcaro, G., Quinto Tranchida, P., Conte, L., Obiedzińska, A., Dugo, P., Dugo, G., & Mondello, L. (2011). Performance evaluation of a rapid-scanning quadrupole mass spectrometer in the comprehensive two-dimensional gas chromatography analysis of pesticides in water. Journal of Separation Science, 34 (18), 2411-2417. doi:10.1002/jssc.201100085 |
Purcaro, G., Tranchida, P. Q., & Mondello, L. (2011). Comprehensive 2D GC Methodologies for the Analysis of Lipids. In W. C. Byrdwell & M. Holcapek (Eds.), Extreme Chromatography – Faster, Hotter, Smaller (1st, pp. 381-430). Urbana, United States: AOCS Press. |
Purcaro, G., Tranchida, P. Q., Zoccali, M., Moret, S., Conte, L., Dugo, P., & Mondello, L. (2011). A Rapid Screening Method for the Detection of Low Levels of Mineral Oil in Vegetable Oils using Comprehensive 2D GC [Paper presentation]. Joint Congress 2011, the 35th International Symposium on Capillary Chromatography (ISCC) and the 8th GCxGC Symposium, San Diego, United States. |
Tranchida, P. Q., Purcaro, G., Dugo, P., & Mondello, L. (2011). Modulators for comprehensive two-dimensional gas chromatography. TrAC: Trends in Analytical Chemistry, 30 (9), 1437-1461. doi:10.1016/j.trac.2011.06.010 |
Tranchida, P. Q., Purcaro, G., Visco, A., Conte, L., Dugo, P., Dawes, P., & Mondello, L. (2011). A flexible loop-type flow modulator for comprehensive two-dimensional gas chromatography. Journal of Chromatography. A, 1218 (21), 3140-3145. doi:10.1016/j.chroma.2010.11.082 |
Tranchida, P. Q., Zoccali, M., Purcaro, G., Moret, S., Conte, L., Beccaria, M., Dugo, P., & Mondello, L. (2011). A rapid multidimensional liquid-gas chromatography method for the analysis of mineral oil saturated hydrocarbons in vegetable oils. Journal of Chromatography. A, 1218 (42), 7476-7480. doi:10.1016/j.chroma.2011.06.089 |
Tranchida, P. Q., Zoccali, M., Purcaro, G., Moret, S., Conte, L., Dugo, P., & Mondello, L. (2011). A Rapid and Sensitive LC/GC (LC×GC) Method for the Determination of Hydrocarbon Contamination in Vegetable Oils [Paper presentation]. Joint Congress 2011, the 35th International Symposium on Capillary Chromatography (ISCC) and the 8th GCxGC Symposium, 26th International symposium on MicroScale Bioseparation, San Diego, United States. |
Mondello, L., Purcaro, G., Tranchida, P. Q., Dugo, P., & Dugo, G. (2010). New frontier in ultra fas-GC/MS rapid quadrupole technology (20000amu/s) for qualitative and quantitative analysis [Paper presentation]. the 34th International Symposium on Capillary Chromatography (ISCC) and the 7th GCxGC Symposium, Riva del Garda, United States. |
Mondello, L., Tranchida, P. Q., Purcaro, G., Dugo, P., & Dugo, G. (2010). Comprehensive chromatography (GCxGC and LCxLC) for the analysis of complex samples [Paper presentation]. International Chemical Congress of Pacific Basin Societies, Honolulu, United States. |
Mondello, L., Tranchida, P. Q., Purcaro, G., Dugo, P., Dugo, G., & Dawes, P. (2010). A Novel Chip-Based Flow Modulator for Comprehensive Two-Dimensional Gas Chromatography [Paper presentation]. 16th International Symposium on Separation Science, ISSS 2010, Rome, Italy. |
Moret, S., Purcaro, G., & Conte, L. S. (2010). Polycyclic aromatic hydrocarbons (PAHs) levels in propolis and propolis-based dietary supplements from the Italian market. Food Chemistry, 122 (1), 333-338. doi:10.1016/j.foodchem.2010.02.041 |
Purcaro, G., Tranchida, P. Q., Conte, L., Dugo, P., Dugo, G., & Mondello, L. (2010). Potential of Very fast Quadruple Mass Spectrometry (20000amu/sec) for Analysis of Perfume Allergens Using Comprehensive Two-Dimensional Gas Chromatography [Paper presentation]. 16th International Symposium on Separation Science, ISSS 2010, Rome, Italy. |
Purcaro, G., Tranchida, P. Q., Conte, L., Dugo, P., Dugo, G., & Mondello, L. (2010). Potential of comprehensive two-dimensional gas chromatography coupled to a very fast quadruple mass spectrometer (20000amu/sec) [Paper presentation]. 28th International Symposium on Chromatography, ISC 2010, Valencia, Spain. |
Purcaro, G., Tranchida, P. Q., Conte, L., Dugo, P., Dugo, G., & Mondello, L. (2010). Characterization of bacterial lipid profiles by using rapid sample preparation and fast comprehensive two-dimensional gas chromatography in combination with mass spectrometry [Paper presentation]. HTC-11, Bruges, Belgium. |
Purcaro, G., Tranchida, P. Q., Dugo, P., Dugo, G., & Mondello, L. (2010). Extending the realm of qualification and quantification in comprehensive two-dimensional chromatography coupled to quadrupole mass spectrometry [Paper presentation]. the 34th International Symposium on Capillary Chromatography (ISCC) and the 7th GCxGC Symposium, Riva del Garda, Italy. |
Purcaro, G., Tranchida, P. Q., Dugo, P., La Camera, E., Bisignano, G., Conte, L., & Mondello, L. (2010). Characterization of bacterial lipid profiles by using rapid sample preparation and fast comprehensive two-dimensional gas chromatography in combination with mass spectrometry. Journal of Separation Science, 33 (15), 2334-2340. doi:10.1002/jssc.201000160 |
Purcaro, G., Tranchida, P. Q., Ragonese, C., Conte, L., Dugo, P., Dugo, G., & Mondello, L. (2010). Evaluation of a rapid-scanning quadrupole mass spectrometer in an apolar × ionic-liquid comprehensive two-dimensional gas chromatography system. Analytical Chemistry, 82 (20), 8583-8590. doi:10.1021/ac101678r |
Sciarrone, D., Purcaro, G., Tranchida, P. Q., Ragonese, C., Dugo, P., Dugo, G., & Mondello, L. (2010). Advanced Gas Chromatographic Techniques for the Quali-Quantitative Analysis of Essential Oils: Fast GC-qMS (20,000 a.m.u./sec) and Multidimensional MDGC-qMS [Paper presentation]. 41th International Symposium on Essential Oils, ISEO 2010, Wroclaw, Poland. |
Tranchida, P. Q., Purcaro, G., Dugo, P., Dugo, G., Dawes, P., & Mondello, L. (2010). Sviluppo di un modulatore pneumatico versatile basato su un chip per gas cromatografia multidimensionale comprehensive di matrici alimentari [Paper presentation]. VIII Congresso Nazionale di Chimica degli Alimenti – Qualità e Tipicità degli Alimenti Mediterranei: Alimentazione e Salute, Marsala, Italy. |
Tranchida, P. Q., Purcaro, G., Dugo, P., Dugo, G., Dawes, P., & Mondello, L. (2010). Development of a flexible chip-based pneumatic modulator for comprehensive two-dimensional gas chromatography [Paper presentation]. the 34th International Symposium on Capillary Chromatography (ISCC) and the 7th GCxGC Symposium, Riva del Garda, Italy. |
Tranchida, P. Q., Purcaro, G., Fanali, C., Dugo, P., Dugo, G., & Mondello, L. (2010). Optimized use of a 50μm ID secondary column in comprehensive two-dimensional gas chromatography-mass spectrometry. Journal of Chromatography. A, 1217 (25), 4160-4166. doi:10.1016/j.chroma.2010.01.040 |
Tranchida, P. Q., Purcaro, G., Sciarrone, D., Dugo, P., Dugo, G., & Mondello, L. (2010). Accurate quadrupole MS peak reconstruction in optimized gas-flow comprehensive two-dimensional gas chromatography. Journal of Separation Science, 33 (17-18), 2791-2795. doi:10.1002/jssc.201000288 |
Tranchida, P. Q., Shellie, R. A., Purcaro, G., Conte, L. S., Dugo, P., Dugo, G., & Mondello, L. (2010). Analysis of fresh and aged tea tree essential oils by using GC×GC-qMS. Journal of Chromatographic Science, 48 (4), 262-266. doi:10.1093/chromsci/48.4.262 |
Akpambang, V. O. E., Purcaro, G., Lajide, L., Amoo, I. A., Conte, L. S., & Moret, S. (2009). Determination of polycyclic aromatic hydrocarbons (PAHs) in commonly consumed Nigerian smoked/grilled fish and meat. Food Additives and Contaminants. Part A. Chemistry, Analysis, Control, Exposure and Risk Assessment, 26 (7), 1096-1103. doi:10.1080/02652030902855406 |
Purcaro, G., Moret, S., & Conte, L. S. (2009). Optimisation of microwave assisted extraction (MAE) for polycyclic aromatic hydrocarbon (PAH) determination in smoked meat. Meat Science, 81 (1), 275-280. doi:10.1016/j.meatsci.2008.08.002 |
Purcaro, G., Tranchida, P. Q., Jacques, R. A., Caramão, E. B., Moret, S., Conte, L., Dugo, P., Dugo, G., & Mondello, L. (2009). Characterization of the yerba mate (Ilex paraguariensis) volatile fraction using solid-phase microextraction-comprehensive 2-D GC-MS. Journal of Separation Science, 32 (21), 3755-3763. doi:10.1002/jssc.200900343 |
Purcaro, G., Tranchida, P. Q., & Mondello, L. (2009). Advantages of using comprehensive 2D GC in the analysis of lipids [Paper presentation]. the 33rd International Symposium on Capillary Chromatography and Electrophoresis (ISCCE) and the 6th GCxGC Symposium, Portland, United States. |
Tranchida, P. Q., Purcaro, G., Conte, L., Dugo, G., & Mondello, L. (2009). Higher resolution comprehensive two-dimensional gas chromatography [Paper presentation]. the 33rd International Symposium on Capillary Chromatography and Electrophoresis (ISCCE) and the 6th GCxGC Symposium, Portland, United States. |
Tranchida, P. Q., Purcaro, G., Conte, L., Dugo, P., Dugo, G., & Mondello, L. (2009). Optimized use of a 50 μm internal diameter secondary column in a comprehensive two-dimensional gas chromatography system. Analytical Chemistry, 81 (20), 8529-8537. doi:10.1021/ac901461y |
Tranchida, P. Q., Purcaro, G., Conte, L., Dugo, P., Dugo, G., & Mondello, L. (2009). Enhanced resolution comprehensive two-dimensional gas chromatography applied to the analysis of roasted coffee volatiles. Journal of Chromatography. A, 1216 (43), 7301-7306. doi:10.1016/j.chroma.2009.06.056 |
Moret, S., Purcaro, G., & Conte, L. S. (2008). Valutazione della presenza di inquinanti, dello stato di ossidazione e caratterizzazione della frazione volatile nei prodotti della filiera della carne suina. Progress in Nutrition, 10 (2), 69-80. |
Purcaro, G., Moret, S., & Conte, L. S. (2008). Rapid SPE-HPLC determination of the 16European priority polycyclic aromatic hydrocarbons in olive oils. Journal of Separation Science, 31 (22), 3936-3944. doi:10.1002/jssc.200800392 |
Purcaro, G., Moret, S., & Conte, L. S. (2008). HS-SPME-GC applied to rancidity assessment in bakery foods. European Food Research and Technology, 227 (1), 1-6. doi:10.1007/s00217-007-0715-8 |
Moret, S., Purcaro, G., & Conte, L. S. (2007). Polycyclic aromatic hydrocarbon (PAH) content of soil and olives collected in areas contaminated with creosote released from old railway ties. Science of the Total Environment, 386 (1-3), 1-8. doi:10.1016/j.scitotenv.2007.07.008 |
Purcaro, G., Moret, S., & Conte, L. S. (2007). Rapid validated method for the analysis of benzo[a]pyrene in vegetable oils by using solid-phase microextraction-gas chromatography-mass spectrometry. Journal of Chromatography. A, 1176 (1-2), 231-235. doi:10.1016/j.chroma.2007.10.070 |
Purcaro, G., Moret, S., & Conte, L. (2007). Prodotti a rischio per la presenza di idrocarburi policiclici aromatici (IPA) [Paper presentation]. Sicurezza alimentare: aggiornamenti per le imprese. Formazione di composti a seguito di trattamenti termici negli alimenti”, Fiera CIBUS, Rome, Italy. |
Purcaro, G., Morrison, P., Moret, S., Conte, L., & Marriott, P. (2007). Determination of polycyclic aromatic hydrocarbons in vegetable oils using solid phase microextraction comprehensive two-dimensional gas chromatography coupled with time of flight mass spectrometry [Paper presentation]. 5th Euro Fed Lipid Congress, Gothenburg, Sweden. |
Purcaro, G., Morrison, P., Moret, S., Conte, L. S., & Marriott, P. J. (2007). Determination of polycyclic aromatic hydrocarbons in vegetable oils using solid-phase microextraction-comprehensive two-dimensional gas chromatography coupled with time-of-flight mass spectrometry. Journal of Chromatography. A, 1161 (1-2), 284-291. doi:10.1016/j.chroma.2007.05.105 |
Tran, T., Amador-Muñoz, O., Purcaro, G., & Marriott, P. (2007). Gas chromatographic analysis of polyaromatic hydrocarbons. In Environmental Impact of Polynuclear Aromatic Hydrocarbons (pp. 331-378). Kerala, India: Research Signpost. |
Purcaro, G., Navas, J. A., Guardiola, F., Conte, L. S., & Moret, S. (2006). Polycyclic aromatic hydrocarbons in frying oils and snacks. Journal of Food Protection, 69 (1), 199-204. doi:10.4315/0362-028X-69.1.199 |
Moret, S., Purcaro, G., & Conte, L. S. (2005). Polycyclic aromatic hydrocarbons in vegetable oils from canned foods. European Journal of Lipid Science and Technology, 107 (7-8), 488-496. doi:10.1002/ejlt.200501060 |