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See detailChemical composition and antibacterial activitiy of the essential oils of Algerian Myrtus communis L.
Hennia, Aïcha; Brada, Moussa; Nemmiche, Saïd et al

in Journal of Essential Oil Research (2015)

Myrtus communis L. leaf essential oils from Algeria were analyzed by gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS). A total of thirty-four components were identified accounting ... [more ▼]

Myrtus communis L. leaf essential oils from Algeria were analyzed by gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS). A total of thirty-four components were identified accounting for 95% of the oil. The main compounds were limonene (23.4%), linalool (15.4%), geranyl acetate (10.9%), α-pinene (10.7%), linalyl acetate (8.2%) and 1,8-cineole (6.6%).The antimicrobial evaluation showed that myrtle oil exhibited good antibacterial activity against Staphylococcus aureus, Proteus mirabilis and Kleibsiella pneumonia, but differed according to the strains. Conversely, it was not active against Pseudomonas aeruginosa. [less ▲]

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See detailChemical Composition and Antimicrobial Activity of Essential Oil of Thyme (Thymus vulgaris) from Eastern Morocco
Imelouane, B.; Amhamdi, H.; Wathelet, Jean-Paul ULiege et al

in International Journal of Agriculture and Biology (2009)

The essential oil from flowering Thyme (Thymis vulgaris L.) an aromatic member of the Lamiaceae family, from Morocco, obtained by hydrodistillation, was analysed by GC/FID and GC/MS. The constituents were ... [more ▼]

The essential oil from flowering Thyme (Thymis vulgaris L.) an aromatic member of the Lamiaceae family, from Morocco, obtained by hydrodistillation, was analysed by GC/FID and GC/MS. The constituents were identified by their mass spectra and Kovats’ indices. Forty three compounds consisting 97.85% of the total components were identified from the oil obtained with 1% yield. Among those, camphor (38.54%), camphene (17.19%), α-pinene (9.35%), 1, 8-cineole (5.44%), borneol (4.91%) and β-pinene (3.90%) were the major oil components. Essential oil of Thyme was evaluated for its antibacterial activities against six Gram-positive and Gram negative pathogenic bacteria: Staphylococcus aureus, S. epidermidis, Streptococcus sp., Pantoa sp. and Escherichia coli. [less ▲]

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See detailChemical composition and antimicrobial activity of essential oils of Ocimum basilicum, Ocimum canum and Ocimum gratissimum in function of harvesting time
Mith, Hasika; Yayi, Éléonore; Bokossa, Innocent et al

in Journal of Essential Oil-Bearing Plants [=JEOBP] (2014)

BACKGROUND: The aim of present the study was to investigate the chemical composition and the antimicrobial activity of essential oils of Ocimum basilicum, Ocimum canum and Ocimum gratissimum from Benin as ... [more ▼]

BACKGROUND: The aim of present the study was to investigate the chemical composition and the antimicrobial activity of essential oils of Ocimum basilicum, Ocimum canum and Ocimum gratissimum from Benin as affected by harvesting time. The chemical composition of hydrodistillated essential oils were analyzed by GC-FID (gas chromatography – flame ionization detector) and GC-MS (gas chromatography-mass spectrometry). Disc diffusion and broth microdilution assays were used to evaluate the antibacterial activity of essential oils against two foodborne pathogens. RESULTS: Based on the composition analysis, major components were as follows: estragol (43.0 -44.7 %) and linalool (24.6 -29.8 %) in O. basilicum oils; carvacrol (12.0 -30.8 %) and p-cymene (19.5 -26.2 %) in O. canum oils; thymol (28.3 -37.7 %) and γ-terpinene (12.5 -19.3 %) in O. gratissimum oils. The tested oils and their components exhibited notable antimicrobial activities against Listeria monocytogenes and Salmonella typhimurium. The O. canum and O. gratissimum oils collected at 7h and 19h showed significant higher activities against L. monocytogenes and S. typhimurium (MICs and MBCs 0.34 – 2.5 µL/mL) (p < 0.05), whereas O. basilicum showed lower activity (MICs and MBCs 2.0 – 8.0 µL/mL) at any daytime of harvest, the weakest being at 19h (MIC and MBC 12.0 – 32.0 µL/mL). CONCLUSION: The daytime of harvest can influence the composition of oils and their activities on bacteria. [less ▲]

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See detailChemical composition and antimicrobial activity of essential oils of Ocimum basilicum, Ocimum canum and Ocimum gratissimum in function of harvesting time
Mith, Hasika; Yayi-Ladékan, Eléonore; Dosso Sika Kpoviessi, Salomé et al

in Journal of Essential Oil-Bearing Plants [=JEOBP] (2016), 19(6), 1413-1425

The chemical composition of essential oils obtained by hydrodistillation from aerial parts of Ocimum basilicum, Ocimum canum and Ocimum gratissimum from Benin as affected by harvesting time, were analyzed ... [more ▼]

The chemical composition of essential oils obtained by hydrodistillation from aerial parts of Ocimum basilicum, Ocimum canum and Ocimum gratissimum from Benin as affected by harvesting time, were analyzed by GC-FID (Gas chromatography-Flame ionization detector) and GC-MS (Gas chromatography-Mass spectrometry). Based on the composition analysis, major components were as follows: estragol (43.0-44.7%) and linalool (24.6 29.8%) in O. basilicum oils; carvacrol (12.0-30.8%) and p-cymene (19.5-26.2%) in O. canum oils; thymol (28.3-37.7%) and γ-terpinene (12.5-19.3 %) in O. gratissimum oils. Disc diffusion and broth microdilution assays were used to evaluate the antibacterial activity of essential oils and their main components against two foodborne bacteria, Listeria monocytogenes and Salmonella enterica serotype Typhimurium. The tested oils and their components exhibited notable antimicrobial activities against L. monocytogenes and S. Typhimurium. The O. canum and O. gratissimum oils collected at 7h and 19h showed significant higher activities against L. monocytogenes and S. Typhimurium (MICs and MBCs 0.34 - 2.5 μL/mL) (p < 0.05), whereas O. basilicum showed lower activity (MICs and MBCs 2.0 - 8.0 μL/mL) at any daytime of harvest, the weakest being at 19h (MIC and MBC 12.0 - 32.0 μL/mL). The daytime of harvest can influence the composition of oils and their activities on bacteria. [less ▲]

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See detailChemical Composition and Antimicrobial Activity of the Essential Oil of Myrtus communis L. from Algeria
Brada, M.; Hennia, A.; Nemmiche, S. et al

Poster (2010)

This study deals with the valorisation of medicinal and aromatic plants of the Algerian flora, in order to find new bioactive natural products. Myrtus communis essential oil obtained by hydrodistillation ... [more ▼]

This study deals with the valorisation of medicinal and aromatic plants of the Algerian flora, in order to find new bioactive natural products. Myrtus communis essential oil obtained by hydrodistillation was investigated by capillary gas chromatography and gas chromatography/mass spectrometry. Twenty-seven volatile compounds were identified in the leaves essential oil; the major components were: -pinene (23.5 %), limonene (22.9 %), 1,8-cineole (16.1 %), linalool (13.0%), linalyl acetate (10.9%) and geranyl acetate (4.6%). The antibacterial activity of essential oils extracts was evaluated by the diffusion method and by the dilution method in liquid medium on pathogenic bacteria (Staphylococcus aureus, Escherichia coli, Salmonella sp, Proteus sp and Klebsiella sp). [less ▲]

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See detailChemical Composition and Antioxidant Activity of Essential Oil of Ocimum basilicum Leaves from the Northern Region of Algeria
Hadj Khelifa, L.; Brada, Moussa; Brahmi, F. et al

in Topclass Journal of Herbal Medicine (2012), 1(2), 53-58

Ocimum basilicum essential oil (Algerian species), which is extracted from dried leaves with an output of 1.98 ± 0.01%, is yellow pale. Its chemical composition has been investigated by GC/MS and GC/FID ... [more ▼]

Ocimum basilicum essential oil (Algerian species), which is extracted from dried leaves with an output of 1.98 ± 0.01%, is yellow pale. Its chemical composition has been investigated by GC/MS and GC/FID. Fourty compounds have been identified accounting for 97.4%. The major compounds were: Linalool (32.83%), linalyl acetate (16%), elemol (7.44%), geranyl acetate (6.18%), myrcene (6.12%), allo-ocimene (5.02%), α-terpineol (4.9%), (E)-β-ocimene (3.68%) and neryl acetate (3.45%). O. basilicum essential oil was screened for its in vitro antioxidant activity using DPPH assay. The results showed that the concentration of the essential oil needed to scavenge 50% of DPPH, was 83.54 mg/ml lower than that of vitamin E (22.0 mg/ml) and therefore acts as a natural antioxidant agent. [less ▲]

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See detailChemical composition and antioxidant activity of essentiel oil, various organic extracts of Cistus ladanifer and Cistus libanotis growing in Eastern Morocco
Zidane, H; Elmiz, M; Aouinti, F et al

in African Journal of Biotechnology (2013), 12(34)

In the present work, we studied the chemical composition of the essential oil of Cistus ladanifer and Cistus libanotis growing in Eastern Morocco. Camphene, borneol, cyclohexanol-2, 2, 6 tremethyl ... [more ▼]

In the present work, we studied the chemical composition of the essential oil of Cistus ladanifer and Cistus libanotis growing in Eastern Morocco. Camphene, borneol, cyclohexanol-2, 2, 6 tremethyl, terpineol-4 and α-pinene were the main constituents of the essential oil of C. ladanifer, while in the essential oil of C. libanotis we obtained terpineol-4, γ-terpinene, camphene, sabinene, α-terpinene and α-pinene. The result show that C. ladanifer of the leaves of methanol: water (50:50) extract had the highest value of total phenolic content and the lowest was present in ethanol: water (50:50) extract of the stem and acetonitrile extract of the flowers of C. libanotis. From our experimental results, the extract of flowers, fruit, stem and leaves of those plants showed highest potential as free radical scavengers [less ▲]

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See detailChemical Composition and Antioxidant Activity of seeds oils and fruit juice of Opuntia Ficus Indica and Opuntia Dillenii from Morocco
Ghazi, Z.; Ramdani, M.; Tahri, M. et al

in Journal of Materials and Environmental Science (2015), 6(8), 2338-2345

This study provides basic information on the mineral composition of the seeds and antioxidant activity in seeds oils and fruit juices of cactus belonging to two species Opuntia ficus indica and Opuntia ... [more ▼]

This study provides basic information on the mineral composition of the seeds and antioxidant activity in seeds oils and fruit juices of cactus belonging to two species Opuntia ficus indica and Opuntia dillenii, from Morocco (Oujda), in order to evaluate the nutritional value of the Opuntia extracts. Minerals determined from dry seeds of Opuntia ficus indica and Opuntia dillenii were: calcium 480.93 and 408.28; phosphorus 1417.59 and 970.15; potassium 304.51 and 201.96; magnesium: 316.59 and 240.30; sodium: 48.33 and 18.18; zinc: 70.77 and 78.26 mg/100g respectively. The main fatty acids of Opuntia ficus indica and Opuntia dillenii seed oil were respectively: linoleic acid: 58.79 and 79.83%, Palmitic acid: 11.18 and 13.52%. The antioxidant activity of Opuntia ficus indica and Opuntia dillenii seed oils and fruit juices were assessed by means of 2, 2-diphenyl-1-picrylhydrazyl (DPPH) radical-scavenging assay and ascorbic acid test. The results showed that the antioxidant activities of Opuntia ficus indica and Opuntia dillenii seed oil (IC50 = 19.79 ± 0.023 and 27.21 ± 0.075 μL/mL) are higher than that of the reference ascorbic acid (IC50 = 16.56 ± 0.019 μg/mL). However, the Opuntia dillenii juice presents antioxidant activity more important than this of Opuntia seed oil and ascorbic acid. It possessed strong antioxidant activity (IC50 = 8.18 μL/mL). The antioxidant activity of the seed oil and juice were also found to be concentration-dependent. [less ▲]

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See detailChemical Composition and Antioxydant Activity of Laurus nobilis Floral Buds Essential Oil
Bouzouita, N.; El Omri, A.; Kachouri, F. et al

in Journal of Essential Oil Research (2009)

The essential oil of Laurus nobilis floral buds (FB) collected in Tunisia was obtained by hydrodistillation and analysed by GC-MS. Twenty three constituents were identified. The main components of this ... [more ▼]

The essential oil of Laurus nobilis floral buds (FB) collected in Tunisia was obtained by hydrodistillation and analysed by GC-MS. Twenty three constituents were identified. The main components of this oil were α-terpinyl acetate (28.43 %), methyl eugenol (19.57 %), eugenol (7.42 %) and elemicin (4.41 %). The antioxidant activity of the oil of Laurus nobilis FB was evaluated by two methods, β-carotene bleaching (BCB) test and 2.2-diphenyl-β-picrylhydrazyl (DPPH) assay using respectively butylated hydroxytoluene (BHT), trolox, gallic acid, caffeic acid and δ-tocopherol as standards. It was found that the Laurus nobilis FB oil have a significant antioxidant effect when tested by each method respectively. The antioxidant activity of this oil is more effective than the synthetic antioxidant (BHT) at 200 ppm and can be attributed to the active compounds eugenol, elemicin and methyl eugenol present in this essential oil. [less ▲]

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See detailChemical composition and functional properties of dietary fibre extracted by Englyst and Prosky methods from the alga Ulva lactuca collected in Tunisia
Yaich, Hela; Garna, Haikel; Bchir, Brahim et al

in Algal Research (2015), 9

Nowadays there is a growing trend to find new sources of dietary fibre (DF), such as marine algae by-products that have traditionally been undervalued. In this respect, the aim of the present ... [more ▼]

Nowadays there is a growing trend to find new sources of dietary fibre (DF), such as marine algae by-products that have traditionally been undervalued. In this respect, the aim of the present investigation was firstly to compare two methods of dietary fibre quantification (Englyst and Prosky) and secondly to determine the chemical composition and some of the functional properties of total and insoluble fibres extracted in accordance with the Englyst method. The dietary fibres of dried Ulva lactuca collected from the Tunisian littoral were determined by the Prosky (gravimetric method) and Englyst (enzymatic-chemical method) methods. The two extraction methods (Englyst–Prosky) provided approximately the same values in total fibres (~54%). However, they had different insoluble and soluble fibre contents. U. lactuca contained 20.53% and 31.55% of soluble fibres and 34.37% and 21.54% of insoluble fibres using the Prosky and Englyst methods, respectively. The fractionation of the insoluble dietary fibre concentrate revealed that hemicellulose was the most abundant fraction (32.49%), followed by cellulose (16.59%) and “lignin-like” compounds (1.53%). For both fibre concentrates, the main neutral sugar was glucose (20.70%–27.59%), which corresponded to hemicellulose and cellulose. The water holding capacity of insoluble fibre concentrate was relatively high. It varied between 9.32 g and 10.3 g of water/g of dry fibre at 25 °C and 80 °C, respectively. Nevertheless, the oil holding capacity of the insoluble fibre concentrate was not affected by temperature. It was about 1.08 and 1.01 g of oil/g of dry fibre at 25 °C and 80 °C. Despite the significant functional properties of fibre concentrate, the presence of lead limits its use as an ingredient in the food industry. [less ▲]

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See detailChemical composition and functional properties of Ulva lactuca seaweed collected in Tunisia
Yaich, H.; Garna, H.; Besbes, S. et al

in Food Chemistry (2011), 128(4), 895-901

The chemical composition and some functional properties of the dried "Ulva lactuca" algae, collected from the littoral between the Taboulba and Sayada area, were determined. The dried "U. lactuca" algae ... [more ▼]

The chemical composition and some functional properties of the dried "Ulva lactuca" algae, collected from the littoral between the Taboulba and Sayada area, were determined. The dried "U. lactuca" algae were investigated for their soluble, insoluble and total dietary fibre content, mineral amount, amino acid and fatty acid profiles, swelling capacity (SWC), water holding capacity (WHC) and oil holding capacity (OHC). Results showed that "U. lactuca" alga powder was characterised by a high content of fibres (54.0%), minerals (19.6%), proteins (8.5%) and lipids (7.9%). The neutral fibres contain hemicellulose (20.6%), cellulose (9.0%) and lignin (1.7%). The proteinic fraction analysis indicated the presence of essential amino acids, which represent 42.0% of the total amino acids. The fatty acids profile was dominated by the palmitic acid, which represents about 60.0% of the total fatty acids, followed by oleic acid (16.0%). The study of the functional properties proved that SWC, WHC and OHC of this alga varied with temperatures and that were comparable to those of some commercial fibre rich products. (C) 2011 Elsevier Ltd. All rights reserved. [less ▲]

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See detailChemical composition and insecticidal activity of Xylopia aethiopica (Dunal) A. Rich (Annonaceae) essential oil on Callosobruchus maculatus
Etse, Koffi Senam ULiege

in Journal de la Société Ouest-Africaine de Chimie (2012), 34

Steam distillation of Xylopa aethiopica (Annonaceae) dried fruits collected at Badou in Akposso region (Togo) gave a colourless essential oil with an overall yield of 3.5% (dry matter). From GC and GC/MS ... [more ▼]

Steam distillation of Xylopa aethiopica (Annonaceae) dried fruits collected at Badou in Akposso region (Togo) gave a colourless essential oil with an overall yield of 3.5% (dry matter). From GC and GC/MS analysis 43 components were identified which represented more than 95% of the essential oil composition. The major components are found to be β-pinene (31.92%), germacrene-D (13.04%), α-pinene (10.28%), sabinene (7.88%), 1,8-cineole (4.87%). Xylopa aethiopica essential oil had a strong and interesting insecticidal activity against Callosobruchus maculatus a major cowpea stored products pest. With dose of 7µL/L of essential oil, more than 98% mortality of weevil was observed after 24 hours of application. [less ▲]

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See detailChemical composition and lipid fraction characteristics of aleppo pine (Pinus halepensis Mill.) seeds cultivated in Tunisia
Cheikh-Rouhou, S.; Hentati, B.; Besbes, S. et al

in Food Science & Technology International (2006), 12(5), 407-415

The proximate composition of Aleppo pine (Pinus halepensis Mill.) seeds cultivated in Bizerta (Tunisia) were investigated for their fatty acid composition, and their thermal and physical properties of ... [more ▼]

The proximate composition of Aleppo pine (Pinus halepensis Mill.) seeds cultivated in Bizerta (Tunisia) were investigated for their fatty acid composition, and their thermal and physical properties of lipid fraction. The proximate analysis of pine seeds showed the following composition (on a dry-weight basis): protein 22.7%, oil 43.3%, ash 8.3% and total carbohydrate 25.7%. Potassium, magnesium and calcium were the predominant mineral elements present in the seeds and reached, together, about 1%. Oleic and linoleic acids were the major unsaturated fatty acids (27.3 and 48.8%, respectively), while the main saturated one was palmitic acid (8.75%). Myristic, myristoleic, palmitoleic, margaric, margaroleic, stearic, linolenic, arachidic, eicosenoic, eicosadienoic eicosatrienoic behenic and lignoceric acids were also detected. Thermal profile of Pinus halepensis Mill. seed oil, determined by its DSC melting curve, showed that the entire liquefaction of the Aleppo pine seed oil occurs at -8 degrees C. GeLab colour parameters (L*, a*, b*), oxidative stability by Rancimat test and viscosity were also determined. Physicochemical properties of the oil include: saponification number 190, peroxide value 3.18, iodine index 117, and a low acidity of 0.61%. Results suggested that the production of oil from Pinus halepensis seeds could provide a potential use in food, pharmaceutical, cosmetics and other non-food industries. [less ▲]

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See detailChemical composition and lipid fraction characteristics of aleppo pine (Pinus halepensis Mill.) seeds cultivated in Tunisia
Cheikh-Rouhou, S.; Besbes, S.; Hentati, B. et al

Poster (2006, September)

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See detailChemical composition and Microbial Quality of dates grown in Figuig oasis of Marocco
Hasnaoui, Amina; ElHoumaizi, Mohamed Aziz; Asehraou, Abdeslam et al

in International Journal of Agriculture and Biology (2010), 12(2), 311-314

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See detailChemical composition and physicochemical characteristics of fixed oils from Algerian Nigella sativa seeds
Benkaci, Ali; Wathelet, Jean-Paul ULiege

in Chemistry of Natural Compounds (2012), 47(6), 925-931

The fatty acids, sterols, and polyphenols from the fixed oils of Nigella sativa seeds originating from four locations were determined. The seeds contained respectively 30.63–34.27% and 25.66–32.77% of ... [more ▼]

The fatty acids, sterols, and polyphenols from the fixed oils of Nigella sativa seeds originating from four locations were determined. The seeds contained respectively 30.63–34.27% and 25.66–32.77% of fixed oils using hexane and isopropyl alcohol in solvent extraction. Linoleic, oleic, and palmitic acids formed the main proportion using the two solvents, respectively: hexane 54.47–61.28%, isopropanol 56.98–67.30%; hexane 19.62–22.94%, isopropanol 18.85–21.96%, and hexane 11.17–13.60%, isopropanol 9.20–14.18%. Other minor unsaturated fatty acids were identified. Eight phytosterols were isolated and identified in the fixed oils by GC and GC/MS analysis, wherein -sitosterol was the dominating compound that inhibits the absorption of dietary cholesterol, followed by stigmasterol, campesterol, and 5-avenasterol. [less ▲]

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See detailThe Chemical Composition of B-type Pulsators: Some Unexpected Results
Morel, Thierry ULiege; Briquet, Maryline ULiege; Aerts, C.

in Precision Spectroscopy in Astrophysics (2008)

We present a project aimed at self-consistently deriving the physical parameters and chemical composition of massive pulsators (β, Cephei stars, Slowly Pulsating B stars) based on high-resolution optical ... [more ▼]

We present a project aimed at self-consistently deriving the physical parameters and chemical composition of massive pulsators (β, Cephei stars, Slowly Pulsating B stars) based on high-resolution optical spectra. Such data will be essential for a proper theoretical interpretation of their oscillation spectrum, but may also contribute in a broader context to our understanding of mixing and diffusion processes in B-type stars. As an illustration, our first results reveal the existence of core-processed material at the surface of some slowly-rotating β, Cephei stars which is not predicted by current evolutionary models including rotation. [less ▲]

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See detailChemical composition of colostrum from Azawak cow in Niger compared with meta-analytical data
Abdou, Harouna; Marichatou, Hamani; Beckers, Jean-François ULiege et al

in Animal Genetic Resources Information = Bulletin d'Information sur les Ressources Génétiques Animales = Boletin de Informacion sobre Recursos Geneticos Animales (2014), 55

This study aimed at comparing data obtained from Azawak zebu colostrum with literature data. The comparison was performed by a meta-analytical approach. Colostrum samples were hand-collected after 5 h ... [more ▼]

This study aimed at comparing data obtained from Azawak zebu colostrum with literature data. The comparison was performed by a meta-analytical approach. Colostrum samples were hand-collected after 5 h from 7 Azawak cows at calving between August 27, to September 10, 2009 in the Sahel. For data from literature, twenty one (21) references were identified in the following analytical databases: PubMed, Science Direct, Google scholar, Collection from University of Liege. The references were selected according to the following two criteria: i) only studies reported on bovine colostrum were used irrespective of breeds, and ii) among the selected studies, those not providing complete information to allow meta-analytical calculation were excluded. Samples were analyzed for immunoglobulins (IgG, IgM, IgA), lactoferrin, and chemical composition (dry mater, protein, fat, lactose, ash, Ca, P, NA, K, Mg). The mean levels of IgG, IgM, dry matter, protein and fat for Azawak cows were lower (P ˂ 0.001) than those obtained in other breeds; however colostrum from the Azawak was higher in IgA but the difference was not significant. For lactose and ash, mean values for Azawak cows were higher (P ˂ 0.001) than those from the literature. Contents of Ca, P, Na and Mg in Azawak bovine colostrum were significantly higher (P ˂ 0.001) than the mean levels in form the literature data. In conclusion, the colostrum from Azawak cows appears to be lower in most immunoglobulins, in fat and in protein than the values reported in the literature, but higher in lactose and minerals. This could be an adaptation to sahelian contraints. [less ▲]

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See detailChemical Composition of Distilled Essential Oils and Hydrosols of Four Senegalese Citrus and Enantiomeric Characterization of Chiral Compounds
Ndiaye, El Hadji Barka; Gueye, Momar Talla; Ndiaye, Ibrahima et al

in Journal of Essential Oil-Bearing Plants [=JEOBP] (2017), 20(3), 820-834

Peels of four local Citrus species (Citrus sinensis L. Obsbeck, Citrus reticulata Blanco, Citrus maxima Burm. and Citrus aurantifolia christm.) grown in a same locality under the same climatic conditions ... [more ▼]

Peels of four local Citrus species (Citrus sinensis L. Obsbeck, Citrus reticulata Blanco, Citrus maxima Burm. and Citrus aurantifolia christm.) grown in a same locality under the same climatic conditions were subjected to steam distillation. The essential oils and floral waters obtained were analyzed by gas chromatography coupled with a flame ionization detector (CPG-FID) and by gas chromatography coupled to a mass spectrometer (CPG-MS). The essential oils yields were ranged between 0.2 and 0.7 %. The qualitative and quantitative analyses show 74 compounds in all oils samples. The oils were largely dominated by hydrocarbon monoterpenes with limonene as major compound (91.5-94.0 %; 90.4-93.4 %; 77.7-93.7 % and 34.8-51.2 %) in oils from Citrus sinensis, Citrus reticulata, Citrus maxima and Citrus aurantifolia, respectively. In addition to limonene, oils of Citrus aurantifolia contained high amounts of β-pinene (6.8-14.4 %), pcymene (5.8-12.2 %), γ-terpinene (0.3 -7.4 %), neral (1.5-9.4 %), geraniol (1.9-12.7 %). Although presenting the same major compound (limonene), the oils had compositions that were qualitatively and quantitatively different. The enantiomeric analyses showed that the chiral major compounds were (R) - (+) - limonene, (S) - (-) – limonene, (1S) - (-) -β-pinene, (1R)-(+)-β-pinene and (S) - (+) - carvone. The hydrosols analyzed were composed of oxygenated compounds and did not have the same major compound. A qualitative and quantitative difference in chemical composition was noted between the Hydrosols. [less ▲]

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See detailChemical composition of essential oils and floral waters of Mentha longifolia (L.) Huds. from Senegal
Diop, Serigne Mbacké; Guèye, Momar Talla; Ndiaye, Ibrahima et al

in American Journal of Essential Oils and Natural Products (2016), 4(1), 46-49

Essential oils of Mentha longifolia from Senegal were extracted from fresh plants and dried plants in the shade for 7 days. The yields were of 0.39 and 0.32% in the fresh and dried plants respectively ... [more ▼]

Essential oils of Mentha longifolia from Senegal were extracted from fresh plants and dried plants in the shade for 7 days. The yields were of 0.39 and 0.32% in the fresh and dried plants respectively. Analysis of the essential oils, floral waters and the assay of pulegone were carried out by GC/FID and GC/MS. The major compounds identified in the oils were pulegone (52.0 and 42.4%), menthone (14.3 and 21.2%), 1, 8-cineole (13.1 and 11.4%) and isomenthone (9.0 and 13.2%) in the fresh and dried plants, respectively. Analyses revealed that floral waters were also characterized by the same major compounds as essential oils but at different rates. In these floral waters, pulegone constituted 60.2 and 47.0%, 1,8- cineole 7.9 and 19.6%, isomenthone 7.2 and 10.7%, menthone 6.4 and 9.2%, chrysanthenone 6.4 and 3.2% and α-terpineol 3.0 and 2.7% in the fresh and dried plants, respectively. The assay results of pulegone, a hepatotoxic compound, have shown very high levels (444.6 and 393.3mg/g) in both fresh and dried plants. [less ▲]

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